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Wyniki wyszukiwania dla: BI5TI3FEO15 CERAMICS
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BET adsorption-desorption isotherm of CeO2 prepared using Pechini method
Dane BadawczeThe dataset includes the isotherms of adortion and desorption of N2 at LN2 temperature. The sorption isotherms were obtained using Quatachrome NovaTouch LX1 equippment. The ceramic measured powder was composed of nanometric pure CeO2 prepared using modified Pechini method - citric acid and propylene glycol (2:1)
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Nonlinear impedance of Bi2VO5.5 ceramic of thickness 2.52 mm (after second heat-treatment at 913 K) was measured at high temperature range with impedance spectroscopy method
Dane BadawczeThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 2.52 mm (after second heat-treatment at 913 K) was measured by impedance spectroscopy method.
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Assessment of Trace Metals Leaching During Rainfall Events from Building Rooftops with Different Types of Coverage – Case Study
PublikacjaRunoff water is an important medium transporting various types of pollution originating from the atmosphere and washed out from roofing materials. The study presents a quality assessment of runoff from different roofs in the context of trace metal concentrations. The analysed rooftops were covered with copper, tar paper and ceramic tile. The quality of the rain water collected at the same time satisfies the demands of the first...
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Mn-Co spinel coatings on Crofer 22 APU by electrophoretic deposition: Up scaling, performance in SOFC stack at 850 °C and compositional modifications
PublikacjaCeramic coatings for metallic interconnects play a key role in limiting corrosion and chromium evaporation in solid oxide cells. This study presents the upscaling of the electrophoretic deposition (EPD) technique to process Mn-Co spinels on real-dimension Crofer 22 APU interconnects and the test in a SOFC stack. Area specific resistance of long-term test conducted for 5000 h at 850 °C demonstrated that two-steps sintering has a...
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Krzysztof Zagórski mgr inż.
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CLAY MINERALS – MINERALOGY AND PHENOMENON OF CLAY SWELLING IN OIL & GAS INDUSTRY
PublikacjaAmong the minerals found in the earth's crust, clay minerals are of the widest interest. Due to the specific properties such as plasticity, absorbing and catalytic properties clay minerals are used in many industries (oil & gas, chemistry, pharmacy, refractory technology, ceramics etc.). In drilling, a phenomenon of swelling clays is frequently observed. It has an important impact on the cementing quality. During the last few decades...
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Ocena stanu powierzchni kulek ceramicznych po nagniataniu tocznym stali hartowanej Cf53
PublikacjaW artykule przedstawiono wyniki z badań eksperymentalnych dotyczących przydatności kulek wykonanych z ceramiki technicznej, do nagniatania tocznego, narzędziami z dociskiem hydrostatycznym. W badaniach wykorzystano narzędzie umożliwiające wymianę kulek nagniatających. Badania wykonano poprzez nagniatanie wałków wykonanych ze stali Cf53 w stanie utwardzonym (zahartowanym). Wyniki badań obejmują charakterystyki stanu powierzchni...
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Results of abrasive slurry dosage in lapping process
PublikacjaPrzedstawiono wyniki badań dawkowania zawiesiny ściernej w docieraniu powierzchni płaskich elementów ceramicznych. Analizowano wpływ dawkowania na podstawowe parametry chropowatości powierzchni ceramiki Al2O3 i Al2O3-ZrO2.
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Allergic Reactions as a Defense of the Organism to the Influence of Implants Components Made of Stainless Steel
PublikacjaDue to the increasing number of cases of hypersensitivity caused by direct contact with metals, as well as the increasing demand for implants in humans all ages numerous studies on the effects of the impact of implant components are being carried out. The paper presents the phenomenon of etiology of allergy in general terms and in relation to the biomaterials used in medicine. There have been characterized in terms of impact on...
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Allergic reactions as a defense of the organism to the influence of implants components made of stainless steel
PublikacjaDue to the increasing number of cases of hypersensitivity caused by direct contact with metals, as well as the increasing demand for implants in humans all ages numerous studies on the effects of the impact of implant components are being carried out. The paper presents the phenomenon of etiology of allergy in general terms and in relation to the biomaterials used in medicine. There have been characterized in terms of impact on...
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Development of polyurethanes for bone repair
PublikacjaThe purpose of this paper is to review recent developments on polyurethanes aimed at the design, synthesis, modifications, and biological properties in the field of bone tissue engineering. Different polyurethane systems are presented and discussed in terms of biodegradation, biocompatibility and bioactivity. A comprehensive discussion is provided of the influence of hard to soft segments ratio, catalysts, stiffness and hydrophilicity...
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Novel Low-Loss Substrates for 5G Applications
PublikacjaThis paper presents a feasibility study of a new type of microwave low-loss dielectric substrates for 5G network applications. The new substrate materials are composites of polypropylene and high-dielectric-constant micro-ceramics. This combination is expected to form a very low-loss dielectric material at low fabrication cost. Two substrate samples with different dielectric properties are fabricated and their characteristics at...
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In Vitro Dissolution of Na-Ca-P-Oxynitrides
Publikacja: Sodium-calcium-phosphate based oxynitride glasses and glass-ceramics doped with Mg, Si, and Nb were studied in vitro in simulated body fluid (SBF) under static conditions. The release of ions and pH changes up to 7 days of immersion were investigated. The nitrogen incorporation into phosphate glass matrix was found to notably influence in vitro dissolution only of homogenous glasses. Increasing the nitrogen content in the samples...
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ZUŻYCIE POWIERZCHNI KULEK CERAMICZNYCH W PROCESIE NAGNIATANIA TOCZNEGO STALI HARTOWANEJ
PublikacjaPrzedstawiono wyniki z badań eksperymentalnych dotyczących przydatności kulek wykonanych z ceramiki technicznej, do nagniatania tocznego, narzędziami z dociskiem hydrostatycznym. W przeprowadzonych badaniach zastosowano narzędzie umożliwiające wymianę kulek ceramicznych zastosowanych jako elementów nagniatające. Badania wykonano poprzez nagniatanie próbek - wałków wykonanych ze stali Cf53 w stanie utwardzonym (zahartowanym). Wyniki...
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Linear impedance as a function of A.C. voltage for 50(2Bi2O3-V2O5)-50SrB4O7 glass-ceramic heat-treated at 813 K measured with impedance spectroscopy method at high temperature region
Dane BadawczeThe linear electrcial properties as a function of A.C. voltage of 50(2Bi2O3-V2O5)-50SrB4O7 glass-ceramic heat treated at 813 K was measured by impedance spectroscopy method.
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Electrocatalytic Gas Sensor with Reference Layer
PublikacjaThis paper presents studies of gas sensors prepared in ceramic technology with Nasicon as a solid electrolyte. Sensors work in the voltammetric mode thus based on the excitation of a sensor with a periodic potential signal while current response is recorded. The main aim is to investigate a Bi8Nb2O17 reference layer influence on sensor properties. Sensors I-V characteristics in different concentration of nitrogen dioxide have been...
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Vertical vibration reduction and audible sound analysis in surface grinding with electroplated tools
PublikacjaOne of the first approaches to the development of a grinding process monitoring system based on audible sound sensors is presented in the paper. Electroplated diamond tools (abrasive D64 and D107) were used in a modified single-disc lapping machine configuration for flat grinding of ceramics (Al2O3). The main aim of the machine modification was to reduce the vertical vibration in order to decrease the tool wear and to increase...
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The structure of lead-silicate glasses and nanocomposites doped with iron oxide
Dane BadawczeThe structure of iron-doped glasses and glass-ceramics were studied. Samples has the composition of 50SiO2–(50−x)PbO–xFe2O3, where x=15, 20 and 25 (in mol%). All samples were prepared by the conventional melt quenching technique; the melting was conducted in air at 1623 K in alumina crucibles. The melts were poured on a brass plate preheated to 573...
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The morphology of lead-silicate glasses and nanocomposites doped with iron oxide
Dane BadawczeThe topography of iron-doped glasses and glass-ceramics were studied. Samples has the composition of 50SiO2–(50−x)PbO–xFe2O3, where x=15, 20 and 25 (in mol%). All sampleswere prepared by the conventional melt quenching technique; the melting was conducted in air at 1623 K in alumina crucibles. The melts were poured on a brass plate preheated to 573...
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Wpływ dawkowania zawiesiny ściernej na efekty docierania powierzchni płaskich
PublikacjaPrzedstawiono wyniki badań dawkowania zawiesiny ściernej podczas docierania powierzchni płaskich. Określono wpływ wielkości dawki ścierniwa na wydajność obróbki i podstawowe parametry chropowatości powierzchni. Obrabiano elementy z ceramiki tlenkowej oraz miedziane.
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Analiza czasochłonności docierania technologicznego powierzchni płaskich w operacjach montażowych.
PublikacjaPrzedstawiono wyniki analiz docierania i mikroszlifowania elementów płaskich na docierarce jednotarczowej mikroziarnami węglika krzemu. Obrabiano elementy ze stali 100Cr oraz z tlenkowej ceramiki technicznej Al2O3. Analizowano czas obróbki i koszty operacji.
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Characteristics of La 0.8 Sr 0.2 Ga 0.8 Mg 0.2 O 3-δ -supported micro-tubular solid oxide fuel cells with LaCo 0.4 Ni 0.6-x Cu x O 3-δ cathodes
PublikacjaIn this study, micro-tubular solid oxide fuel cells (T-SOFCs) with extruded La0.8Sr0.2Ga0.8Mg0.2O3-δ (LSGM) electrolyte as the mechanical support and LaCo0.4Ni0.6O3-δ (LCNO) or LaCo0.4Ni0.4Cu0.2O3-δ (LCNCO) as cathodes were prepared and characterized. Partial substitution of Cu for the Ni-ion positions in the LCNO lattices was found to significantly enhance the densification and accelerate the grain growth. The porosity-corrected...
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Correlation between structural and electrical properties in highly porous (Y,Sr)(Ti,Nb)O3-delta SOFC anodes
PublikacjaIn order to find a relationship between structural and electrical properties, niobium and yttrium doped SrTiO3 ceramics were prepared via solid-state reaction. The samples were sintered in hydrogen and air conditions. The samples were also fabricated with a pore-former to obtain highly porous specimens. The electrical properties of Nb-doped SrTiO3 samples and yttrium and niobium co-doped SrTiO3 were compared. The comparable electrical...
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Udział nośny powierzchni elementów ceramicznych i węglików spiekanych po docieraniu.
PublikacjaPrzedstawiono wyniki badań docierania jednotarczowego powierzchni elementów z ceramiki technicznej i węglików spiekanych. Analizowano jakość obróbki i udział nośny powierzchni po docieraniu. Docieranie powierzchni płaskich jest technologią pozwalającą uzyskać duży udział nośny.
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Nonlinear impedance as a function of A.C. voltage and temperature for Bi2VO5.5 ceramic of thickness 2.52 mm (after first heat-treatment at 913 K) was measured at different frequencies with impedance spectroscopy method
Dane BadawczeThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 2.52 mm was measured by impedance spectroscopy method.
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The structure of lead-silicate glasses containing nanocrystallites of iron oxides
Dane BadawczeThe structure of iron-doped glasses and glass-ceramics were studied. Samples has the composition of (50 − 0.5x)SiO2–(50 − 0.5x)PbO–xFe2O3, where x = 2, 5, 10, 15, 20 and 25 (in mol%). All samples were prepared by the conventional melt quenching technique; the melting was conducted in air at 1623 K in alumina crucibles. The melts were poured on a brass...
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The morphology of lead-silicate glasses containing nanocrystallites of iron oxides
Dane BadawczeThe topography of iron-doped glasses and glass-ceramics were studied. Samples has the composition of (50 − 0.5x)SiO2–(50 − 0.5x)PbO–xFe2O3, where x = 2, 5, 10, 15, 20 and 25 (in mol%). All sampleswere prepared by the conventional melt quenching technique; the melting was conducted in air at 1623 K in alumina crucibles. The melts were poured on a brass...
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n/d Silicon Oxycarbide (SiOC) as Anode Materials for Lithium Ion Batteries: Synthesis and Optimization of Ceramics Prepared by Sol-Gel Method
ProjektyProjekt realizowany w Wydział Chemiczny zgodnie z porozumieniem Homing Plus/2012-6/16 z dnia 2013-05-22
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Development of conductive porous media as packing materials for biotrickling filter – microbial fuel cell system (BTF-MFC system)
Dane BadawczeDataset presents values of electrical resistance measured for three developed conductive packimg materials for the application in a BTF-MFC system.
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Ocena czynnej powierzchni narzędzia w mikroszlifowaniu powierzchni płaskich z kinematyką docierania jednotarczowego
PublikacjaPrzedstawiono wyniki badań eksperymentalnych mikroszlifowania z kinematyką docierania w układzie jednotarczowym. Badania miały na celu wyznaczenie okresu trwałości narzędzia i zmieniających się w czasie jego właściwości ściernych. Badania przeprowadzono na próbkach z ceramiki aluminiowej.
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Wpływ zawiesiny ściernej dawkowanej w sposób wymuszony na wydajność docierania jednotarczowego elementów ceramicznych
PublikacjaPrzedstawiono zagadnienia związane z przygotowywaniem zawiesiny ściernej w docieraniu maszynowym powierzchni płaskich. W badaniach zastosowano wymuszony sposób dozowania zawiesiny na docierak żeliwny. Badano docieranie elementów z ceramiki tlenkowej zawiesiną na bazie mikroziaren węglika krzemu.
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Coatings in arthroplasty [online]
PublikacjaThe modern coatings used in arthroplasty for long term implants are reviewed. The phosphate coatingsare the most popular technique to improve the bone-implant interfacial strength and promote theosseointegration. The plasma spraying, electrophoretic precipitation, powder metallurgy, ion beamsputtering, high velocity oxy-fuel (HVOF) combustion spraying, sol-gel technique, biomimeticdeposition are mostly used to obtain the phosphate,...
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KTaO3 a perovskite for water and air treatment
PublikacjaPerovskites are inorganic compounds that exhibit dielectric properties. These minerals belong to the crystal ceramics family. These compounds are described by the formula: ABX3 where, A and B are 2, 3 or 4 valuable metal ions, and X is an ion of oxygen or fluorine. An example of perovskite is the compound KTaO3. There are many methods for producing KTaO3, but the hydrothermal method is most commonly used. Perovskites can be characterized...
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Water uptake kinetics and electrical transport in BaCe0.6Zr0.2Y0.1M0.1O3−δ (M = Tb, Pr, Fe) protonic conductors
PublikacjaBaCe0.6Zr0.2Y0.1M0.1O3−d (M = Fe, Pr, Tb) is a mixed conducting oxide in which three mobile charge carriers – oxygen ion, electron/hole, and protonic defects – are present. These types of materials have gained much interest as electrode materials for protonic ceramic fuel cells (PCFCs) and protonic ceramic electrolysis cells (PCECs). In this study, the water uptake and oxygen transport properties of different BaCe0.6Zr0.2Y0.1M0.1O3−d...
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Analiza gniazda docierarek dwutarczowych do płaszczyzn - studium przypadku.
PublikacjaPrzedstawiono analizę gniazda trzech docierarek dwutarczowych do płaszczyzn. Analizowano przypadki obróbki pierścieni stalowych i krążków z ceramiki technicznej. Badano czasy główne docierania oraz składowe czasów pomocniczych w analizowanych operacjach obróbki wstępnej, dokładnej i bardzo dokładnej.
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The morphology of lead-borate glasses and nanocomposites doped with iron oxide
Dane BadawczeThe topography of iron-doped borate glasses and glass-ceramics were studied. Samples of composition of xFe2O3–(100 − x)(B2O3–2PbO) (2.5 < x < 37 in mol%) were prepared by the conventional meltquenching technique. The melting was conducted in alumina crucibles at the temperature of 1523 K. The melts were poured on a preheated (573 K) brass plate...
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The structure of lead-borate glasses containing nanocrystallites of iron oxides
Dane BadawczeThe structure of iron-doped glasses and glass-ceramics were studied. Glass samples of composition of xFe2O3–(100 − x)(B2O3–2PbO) (2.5 b x b 37, in mol%) were prepared by the conventional melt quenching technique. The melting was conducted in alumina crucibles at the temperature of 1523 K. The melts were poured on a preheated (573 K) brass plate and...
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Oxygen deficient YBa2Cu3O7-r: two superconducting phases
PublikacjaZestaw próbek ceramiki YBa2Cu3O7-r w postaci pudru i granulatupoddawano stopniowemu odtlenianiu i badano za pomocątermograwimetrii oraz absorbcji mikrofalowej. Stosowanie tychmetod pokazało, że występująca faza $Trm_c=60$~K w związkuYBa2Cu3O7-r, powstała poprzez odtlenianie jest niestabilna.
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Recent advances on spinel-based protective coatings for solid oxide cell metallic interconnects produced by electrophoretic deposition
PublikacjaThe application of ceramic protective coatings to the metallic interconnects in solid oxide cells (SOCs) is a viable and effective method to limit interconnect degradation issues. This featured letter provides a critical overview of the main outcomes of current research on the use of the electrophoretic deposition (EPD) technique to produce protective coatings for SOC metallic interconnects, specifically focusing on different approaches...
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Optical monitoring of thin oil film thickness in extrusion processes
PublikacjaPraca porusza problem pomiaru grubości cienkiej warstwy przyściennej -oleju, podczas procesu wyciskania ceramiki modelowej. Szczegółowo opisuje zjawiska fizyczne zachodzące w warstwie przyściennej oraz dynamiczne parametry wykorzystywane do oceny grubości. Autorzy opisują także metodę pomiaru oraz konstrukcję układów pomiarowych.
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Fabrication of solid oxide fuel cell supported on speciallyperformed ferrite-based perovskite cathode
PublikacjaW pracy przedstawiono warunki technologiczne niezbedne do wytworzenia tlenkowego ogniwa paliwowego na elencie nośnym z materiału perowskitowego LSF. Jako elektrolit stosowana była ceramika z tlenku ceru. Między innymi badany były właściwości elektryczne zarówno materiału katodowego jak i ogniwa.
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Autogenous Fiber Laser Welding of 316L Austenitic and 2304 Lean Duplex Stainless Steels
PublikacjaThis study presents results of experimental tests on quality of dissimilar welded joints between 316L austenitic and 2304 lean duplex stainless steels, welded without ceramic backing. Fiber laser welded butt joints at a thickness of 8 mm were subjected to non‐destructive testing (visual and penetrant), destructive testing (static tensile test, bending test, and microhardness measurements) and structure observations (macro‐ and...
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Material Design and Optimisation of Electrochemical Li-Ion Storage Properties of Ternary Silicon Oxycarbide/Graphite/Tin Nanocomposites
PublikacjaIn this work, we present the characterization and electrochemical performance of various ternary silicon oxycarbide/graphite/tin (SiOC/C/Sn) nanocomposites as anodes for lithium-ion batteries. In binary SiOC/Sn composites, tin nanoparticles may be produced in situ via carbothermal reduction of SnO2 to metallic Sn, which consumes free carbon from the SiOC ceramic phase, thereby limiting the carbon content in the final ceramic nanocomposite....
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Wykorzystanie metody sztucznych baz w badaniach wydajności docierania elementów ceramicznych.
PublikacjaPrzedstawiono metodę pomiaru ubytku liniowego docieranych elementów z ceramiki tlenkowej. W badaniach wykorzystano bazowe odciski Vickersa wykonane na stalowych próbkach kontrolnych. Pomiary przekątnych odcisków przeprowadzono przy pomocy mikroskopu stereoskopowego i kamery CCD, sprzężonej z programem komputerowym MultiScan v 6.08.
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Nanotechnologia, chemia i medycyna
PublikacjaKsiążka przedstawia chemiczne metody otrzymywania nanomateriałów oraz metody ich funkcjonalizacji. Opisano struktury zero, jedno i dwuwymiarowe zbudowane z różnych materiałów (metale, ceramika, związki organiczne, alotropowe odmiany węgla, chalkogenki metali). Podano wybrane przykłady zastosowania nanostruktur w medycynie i naukach pokrewnych.
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Kształtowanie jakości powierzchni w procesach docierania niekonwencjonalnego.
PublikacjaPrzedstawiono wyniki badań jakości docierania powierzchni płaskich niekonwencjonalnymi narzędziami ścierno-metalowymi na docierarce jednotarczowej o standardowym układzie kinematycznym. Analizowano obróbkę żeliwa oraz ceramiki tlenkowej. Tabletki ścierne wykonano z mikroziaren węglika boru. Badania przeprowadzono w ramach projektu KBN T07D 041 10.
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Optyczna tomografia niskokoherentna w badaniach obiektów technicznych
PublikacjaW pracy przedstawiono polaryzacyjny system OCT pracujący w dziedzinie czasu z detekcją zrównoważoną do badań obiektów technicznych. Obiektem badań z wykorzystaniem tego systemu były warstwy wykonane z ceramiki PLZT 9/65/35. Mierzone były grubości tych warstw i ich jednorodność.
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An insight into craft activities in rural areas of Dalmatia province - first data on iron working at the Roman settlement in Lopar (Island of Rab)
PublikacjaWithin multidisciplinary research carried out at Podšilo bay in Lopar on the island of Rab (north-eastern Adriatic), on the bases of movable finds and, possibly, geophysical measurements, evidence of ironworking has been detected within a Roman rural site where ceramic building materials production was ascertained before. Preliminary analyses of several samples of slug, iron objects and nearby collected minerals support the...
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9 - Solid oxide fuel and electrolysis cells
PublikacjaIn this chapter, the fundamental reactions, the geometrical designs, the material requirements, and the status of SOFCs and SOECs are presented. In the following seven chapters, the most important components of an SOC are described and the chapter ends with a summary and outlook. The described components are: (i) oxygen-ion conductors (electrolyte), (ii) anode materials for SOFCs (cathode in SOEC mode), (iii) cathode materials...
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An Influence of Factors of Flow Condition, Particle and Material Properties on Slurry Erosion Resistance
PublikacjaThe degradation of materials due to slurry erosion is the serious problem which occurs in the power industries. The paper presents actual knowledge about an influence of individual factors connected with flow conditions, particles and material properties on the slurry erosion resistance. Among the factors connected with operating conditions, an influence of impact angle, and velocity of impact, particle concertation and liquid...
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QUASI-DISTRIBUTED NETWORK OF LOW-COHERENCE FIBER-OPTIC FABRY-PÉROT SENSORS WITH CAVITY LENGTH-BASED ADDRESSING
PublikacjaDistributed measurement often relies on sensor networks. In this paper, we present the construction of low coherent fiber-optic Fabry-Pérot sensors connected into a quasi-distributed network. We discuss the mechanism of spectrum modulation in this type of sensor and the constraints of assembly of such sensors in the network. Particular attention was paid to separate the signals from individual sensors, which can be achieved by...
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Structure and transport properties of donor-doped barium strontium cobaltites
PublikacjaIn this work, Nb-substituted barium strontium cobaltites Ba0.5Sr0.5Co1-xNbxO3-δ (x = 0 – 0.4) have been fabricated and studied. The structural analysis showed that the Nb content influences the lattice constant as well as the distance between the (Co, Nb) and oxygen atoms. The study of morphology of samples showed that the Nb content does not change the porosity, grain size and morphology of the ceramics. The total electrical conductivity...
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Influence of controlled crystallization and SrF2 content on the structure and properties of Eu3+ doped phosphate glasses
PublikacjaNew phosphate glasses and glass-ceramics P2O5–Bi2O3–K2O–Nb2O5-SrF2 doped with Eu were synthesized and studied in this work. The influence of the SrF2 content (0–15 mol%) and the parameters of the heat treatment on their structural and optical properties were investigated. For the above purpose, the structural characterization by FTIR spectroscopy and XRD measurements was carried out, which showed a significant effect of SrF2 on...
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Selection of material for X-ray tomography analysis and DEM simulations: comparison between granular materials of biological and non-biological origins
PublikacjaPhysical properties and X-ray tomography images of five different granular materials: glass bead, glass grit, short grain white rice, sorghum and clay granules (Seramis) are investigated to select the most promising materials for numerical simulations and time-lapse X-ray tomography imaging. The examined materials represent granular materials of non-biological origin (glass bead, glass grit and Seramis) and granular plant materials...
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Study of abrasive slurry dosage in flat surfaces lapping process
PublikacjaPrzedstawiono wyniki badań dozowania pasty i zawiesiny ściernej w procesach docierania powierzchni płaskich. Badano wpływ wielkości dawki ścierniwa na podstawowe parametry chropowatości powierzchni elementów miedzianych i ceramicznych. Docierano miedź betlenową MOOB oraz ceramikę Al2O3 i Al2O3-ZrO2 mikroziarnami węglika krzemu i węglika boru.
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Wear in siding friction tests. Ring-on-ring contact. Sintered alumina ceramics (98%). Paraffin oil lubrication. Specim. sets #20-#21, #22-#23, #24-#25, #26-#27, #28-#29,#30 - #31. Run time: 4-8h.
Dane BadawczeWear in sliding friction tests in ring-on-ring contact. Sintered alumina ceramics (98%) in self-mated contact. Lubrication: paraffin oil. Sliding velocity: 0.2 m/s. Mean contact stress: 10 MPa. Test rig: PT-3 Tribometer.Running time: 4-8h.Specimen sets:Specim. sets (# [upper, rotating] - #[lower, non-rotating]):#20-#21, #22-#23, #24-#25, #26-#27,...
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Wear in siding friction tests. Ring-on-ring contact. Sintered alumina ceramics (98%). Paraffin oil lubrication. Specim. sets #20-#21, #22-#23, #24-#25, #26-#27, #28-#29,#30 - #31. Run time: 0-4h.
Dane BadawczeWear in sliding friction tests in ring-on-ring contact. Sintered alumina ceramics (98%) in self-mated contact. Lubrication: paraffin oil. Sliding velocity: 0.2 m/s. Mean contact stress: 10 MPa. Test rig: PT-3 Tribometer.Running time: 0 - 4h.Specimen sets:Specim. sets (# [upper, rotating] - #[lower, non-rotating]):#20-#21, #22-#23, #24-#25, #26-#27,...
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Geometrically Nonlinear Analysis of Functionally Graded Shells Based on 2-D Cosserat Constitutive Model
PublikacjaIn this paper geometrically nonlinear analysis of functionally graded shells in 6-parameter shell theory is presented. It is assumed that the shell consists of two constituents: ceramic and metal. The mechanical properties are graded through the thickness and are described by power law distribution. Formulation based on 2-D Cosserat constitutive model is used to derive constitutive relation for functionally graded shells. Numerical...
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Investigations on the removal of hydrophobic odorous volatile organic compounds by biotrickling filtration monitored with electronic nose
PublikacjaThe presented paper presents the results of research on the removal of selected hydrophobic volatile organic compounds (VOCs) from their mixture with air by means of a trickled-bed biofiltration. The efficiency of the removal of toluene and α-pinene, as model VOCs, in a three-section biotrickling filter is evaluated using GCFID and additionally monitored with an electronic nose. The results show that the removal of the model mixture...
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Szlifowanie jednostronne ściernicami o spoiwie niklowym z ziarnami z regularnego azotku boru
PublikacjaPrzedstawiono wyniki badań eksperymentalnych szlifowania jednostronnego stali stopowej 40H i ceramiki beztlenkowej SSiC z zastosowaniem ściernic o spoiwie niklowym z ziarnami z regularnego azotku boru B107 i B64. Zaprezentowano uzyskane wartości liniowego ubytku materiałowego oraz parametru Ra chropowatości powierzchni. Scharakteryzowano ogólnie zużycie czynnej powierzchni ściernicy.
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Szlifowanie jednostronne ściernicami o spoiwie niklowym z ziarnami z regularnego azotku boru
PublikacjaPrzedstawiono wyniki badań eksperymentalnych szlifowania jednostronnego stali stopowej 40H i ceramiki beztlenkowej SSiC z zastosowaniem ściernic o spoiwie niklowym z ziarnami z regularnego azotku boru B107 i B64. Zaprezentowano uzyskane wartości liniowego ubytku materiałowego oraz parametru Ra chropowatości powierzchni. Scharakteryzowano ogólnie zużycie czynnej powierzchni ściernicy.
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Wybrane problemy szlifowania powierzchni płaskich z kinematyką docierania
PublikacjaW pracy przedstawiono teoretyczne i doświadczalne podstawy szlifowania powierzchni płaskich z kinematyką docierania. Dokonano kompleksowej analizy zastosowanych układów kinematycznych szlifierek. Przeprowadzono eksperymenty szlifowania jednostronnego ściernicami o spoiwie galwanicznym z ziarnami diamentowymi (D107, D64 i D46) oraz z regularnego azotku boru (B107 i B64). Innowacyjność ściernic polegała na zróżnicowanym utwierdzeniu...
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LDI MAGIC Bezpośrednie naświetlanie laserowe - opracowanie materiałów i procesów dla następnej generacji zintegrowanych etykiet RFID nie zawierających układów scalonych
ProjektyProjekt realizowany w Katedra Inżynierii Mikrofalowej i Antenowej zgodnie z porozumieniem M-ERA.NET3/2021/123/LDI MAGIC/2022 z dnia 2022-12-30
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Zastosowanie narzędzi ze spoiwem galwanicznym w mikroszlifowaniu powierzchni płaskich
PublikacjaW pracy przedstawiono wyniki z badań mikroszlifowania powierzchni płaskich w zmodyfikowanym układzie docierarki jednotarczowej z zastosowaniem narzędzi ze spoiwem galwanicznym. Czynną powierzchnię narzędzia pokryto ziarnami diamentowymi D64 i D107 oraz borazonowymi B64 i B107. Badaniom poddane zostały przedmioty wykonane z ceramiki technicznej o średnicy 34 mm.
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Electrical properties of nanostructures in lead-silicate glasses and nanocomposites doped with iron oxide
Dane BadawczeElectrical properties of iron oxide nanostructures observed in silicate glasses and glass-ceramics were studied. Two different sets of glass samples were prepared. The first group of samples has the composition of (50 − 0.5x)SiO2–(50 − 0.5x)PbO– xFe2O3, where x = 15, 20 and 25 (in mol%). Composition of the second group was 50SiO2–(50−x)PbO–xFe2O3, where...
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Magnetic properties of of lead-silicate glasses and nanocomposites doped with iron oxide
Dane BadawczeMagnetic properties of iron-doped glasses and glass-ceramics were studied. Two different sets of glass samples were prepared. The first group of samples has the composition of (50 − 0.5x)SiO2–(50 − 0.5x)PbO– xFe2O3, where x = 15 and 20 (in mol%). Composition of the second group was 50SiO2–(50−x)PbO–xFe2O3, where x=15, 20 and 25 (in mol%). All sampleswere...
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Cavitation erosion degradation of Belzona® coatings
PublikacjaIn hydrocarbon and maritime industry there is a constant need of materials and coatings withstanding severe conditions. One of adverse phenomena present there is cavitation erosion. The paper presents evaluation of cavitation resistance of three different steel coatings. Belzona 2141 (ACR-Fluid Elastormer), 1321 (Ceramic S-Steal) and 5831 (ST-Barrier) were deployed on P110 steel and subjected to ultrasound cavitation in distilled...
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Zagospodarowanie proszku krzemowego, wytworzonego z odzyskanych w procesie recyklingu uszkodzonych ogniw modułów fotowoltaicznych = Utilization of silicon powder, recovered in the PV cell's production and recycling processes
PublikacjaW artykule przedstawiono wyniki analizy proszku krzemowego różnego pochodzenia i wskazano możliwości technologiczne zagospodarowania proszku krzemowego: jako podstawowego surowca do produkcji nowych ogniw fotowoltaicznych, jako dodatku do stali stopowych, poprawiających ich własności mechaniczne (twardość, wytrzymałość na rozciąganie, udarność) oraz jako materiału do wytwarzania ceramiki, bazującej na proszkach niemetali.
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Niskokoherentny, interferometryczny system do badaniawłaściwości materiałów ceramicznych
PublikacjaPrzedstawiono światłowodowy system dwuwymiarowej wizualizacjiniejednorodnych struktur warstw ceramicznych. Omówiono projekti fizyczną realizację układu wykorzystującego optyczną, niskokoherentną reflektometrię optyczną, która umożliwia nieinwazyjne i bezkontaktowe obrazowanie wewnętrznych struktur różnych materiałówsilnie rozpraszających promieniowanie. Przedstawiono przykładowewyniki pomiarów wewnętrznych warstw ceramiki LSFO....
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Characterization of PLZT Thin Films for Fast Electro-Optical Sampling Circuits
PublikacjaW artykule omówiono technologię wytwarzania cienkich warstw wybranych kompozycji ceramik ołowiowo-lantanowo-cyrkonowo-tytanowych, nazywanych ceramikami PLZT. Przedstawiono wyniki badań jakości warstw za pomocą techniki XRD. wyniki pomiaru grubości warstw, ich względnej przenikalności dielektrycznej i współczynnika załamania. Omówiono kierunki dalszych prac.
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Three electrode configuration measurements of electrolyte-diffusion barrier-cathode interface
PublikacjaMeasurements of a system consisting of cathode/doped ceria diffusion barrier/doped zirconia electrolyte were made using two- and three-electrode configuration. Results obtained on a three-electrode measurement configuration were compared with and reflect the results obtained in two-electrode configuration. Three-electrode measurements allowed separating the impact of the symmetrical interface in the investigated system. They also...
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Physicochemical properties of rock salt-type ordered Sr2MMoO6 (M=Mg, Mn, Fe, Co, Ni) double perovskites
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Coatings for improvement of high temperature corrosion resistance of porous alloys
PublikacjaPorowate stopy metaliczne są potencjalnymi podłożami nośnymi dla tlenkowych ogniw paliwo. Ich stosowanie obniża cenę ogniw paliwowych, co zaowocuje ich szybszą komercjalizacą. Jednak są one podatne na korozję w wysokich temperaturach. Dotychczas brak jest metod, które mogą poprawić rezystancję korozyjną porotawych stopów w wysokich temperaturach porowatych stopy do zastosowań SOFC. W tym artykule zaproponowano sposób na poprawę...
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Influence of free carbon on the Young's modulus and hardness of polymer‐derived silicon oxycarbide glasses
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Processing of polymer‐derived, aerogel‐filled, SiC foams for high‐temperature insulation
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Electric and magnetic properties of Lanthanum Barium Cobaltite
PublikacjaThe cubic Ba0.5La0.5CoO3‐δ was synthesized using solid state reaction. The structural properties were determined by the simultaneous refinement of Synchrotron Powder X‐ray Diffraction and Neutron Powder Diffraction data. Iodometric titration was used to examine the oxygen stoichiometry and average cobalt oxidation state. Low‐temperature magnetic studies show soft ferromagnetic character of fully oxidized material, with θP = 198(3)...
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Evaluation of 316L porous stainless steel for SOFC support
PublikacjaW pracy przedstawiono wyniki badań stali typu 316L związanych z zastosowaniem w tlenowych ogniwach paliwowych.
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La 0.6 Sr 0.4 Co 0.2 Fe 0.8 O 3-δ oxygen electrodes for solid oxide cells prepared by polymer precursor and nitrates solution infiltration into gadolinium doped ceria backbone
PublikacjaInfiltration is a method, which can be applied for the electrode preparation. In this paper oxygen electrode is prepared solely by the infiltration of La0.6Sr0.4Co0.2Fe0.8O3‐δ (LSCF) into Ce0.8Gd0.2O2-δ (CGO) backbone. The use a polymer precursor as an infiltrating medium, instead of an aqueous nitrate salts solution is presented. It is shown that the polymer forms the single-phase perovskite at 600 °C, contrary to the nitrates...
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Characteristics of La0.8Sr0.2Ga0.8Mg0.2O3-delta -supported micro-tubular solid oxide fuel cells with bi-layer and tri-layer electrolytes
PublikacjaIn this study, La0.8Sr0.2Ga0.8Mg0.2O3−δ (LSGM)-supported micro tubular solid oxide fuel cells (T-SOFCs) with two different configurations, one containing an LSGM–Ce0.6La0.4O2−δ (LDC) bi-layer electrolyte (Cell A) and one containing an LDC–LSGM–LDC tri-layer electrolyte (Cell B), were fabricated using extrusion and dip-coating. After optimizing the paste formulation for extrusion, the flexural strength of the dense and uniform LSGM...
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Low temperature deposition of dense MnCo 2 O 4 protective coatings for steel interconnects of solid oxide cells
PublikacjaIn this work manganese cobalt spinel (MnCo2O4) coatings were deposited on steel substrates by spray pyrolysis at 390 °C. This is at much lower temperatures than previously reported (typically in excess of 900 °C). It was possible to produce coatings with well controlled thickness (2-5-10 μm). The as-deposited coatings were evaluated for their microstructural changes and electrical conductivity up to 800 °C. Results confirm the...
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Fabrication of wormhole-like YSZ and Ni-YSZ by the novel soft-hard template CTAB/NaCl-assisted route. Suppressing Ni coalescence in SOFC
PublikacjaA novel one-pot synthesis route leading to the formation of a wormhole-like structure was developed for the successful fabrication of porous YSZ and Ni-YSZ systems. This method involved co-precipitation in the presence of the micelle-forming agents CTAB/Pluronic P123 and crystallising NaCl. The obtained skeletons were mechanically stable and presented almost 50% uniform, open porosity without using any additional pore-formers....
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Processing of Ce0.8Gd0.2O2-δ barrier layers for solid oxide cells: The effect of preparation method and thickness on the interdiffusion and electrochemical performance
PublikacjaCe0.8Gd0.2O1.9 (CGO) barrier layers are required to mitigate the chemical reactions between Sr-containing oxygen electrode materials and Zr-based oxygen ion conductors in high-temperature solid oxide cells. Barrier layers produced by different methods were studied in this work. As a reference, a cell with no barrier layer was measured. The application of the powder-processed barrier layers, considerably increases the performance....
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Antimony substituted lanthanum orthoniobate proton conductor – structure and electronic properties.
PublikacjaX‐ray and neutron diffraction have been utilized to analyze the crystalline and electronic structure of lanthanum orthoniobate substituted by antimony. Using X‐ray absorption spectroscopy and photoelectron spectroscopy, changes in the electronic structure of the material upon substitution have been analyzed. The structural transition temperature between fergusonite and scheelite phases for 30 mol% antimony substitution was found...
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Preparation and characterisation of iron substituted Mn1.7Cu1.3-xFexO4 spinel oxides (x = 0, 0.1, 0.3, 0.5)
PublikacjaSpinel oxides with the general formula Mn1.7Cu1.3-xFexO4 (x= 0, 0.1, 0.3, 0.5) were prepared and evaluated in this work for their properties at high temperatures. The effect of partially substituting Cu by Fe has not been studied so far for this group of materials and is thus evaluated in this work. Mn1.7Cu1.3-xFexO4 powders were synthesised by a soft chemistry process and studied in terms of crystallographic phase analysis, electrical...
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Electrophoretic co-deposition of Mn1.5Co1.5O4, Fe2O3 and CuO: Unravelling the effect of simultaneous addition of Cu and Fe on the microstructural, thermo-mechanical and corrosion properties of in-situ modified spinel coatings for solid oxide cell interconnects
PublikacjaA systematic microstructural, thermo-mechanical and electrical characterization of simultaneous Fe–Cu doped Mn–Co spinel coatings processed by electrophoretic co-deposition on Crofer 22 APU is here reported and discussed. An innovative approach for the simultaneous electrophoretic deposition of three spinel precursors is designed, conceived and optimised, with the aim of outlining time- and energy-saving spinel modification routes....
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Electrophoretic co-deposition of Fe2O3 and Mn1,5Co1,5O4: Processing and oxidation performance of Fe-doped Mn-Co coatings for solid oxide cell interconnects
PublikacjaThe “in-situ” Fe-doping of the manganese cobalt spinel was achieved by electrophoretic co-deposition of Mn1,5Co1,5O4 and Fe2O3 powders followed by a two-step reactive sintering treatment. The effects on the coating properties of two different Fe-doping levels (5 and 10 wt.% respectively) and two different temperatures of the reducing treatment (900 and 1000 °C) are discussed. Samples with Fe-doped coatings demonstrated a lower...
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Comparison of Cu1.3Mn1.7O4 spinels doped with Ni or Fe and synthesized via wet chemistry and solid-state reaction methods, designed as potential coating materials for metallic interconnects
PublikacjaThe influence of the method applied to synthesize Cu-Mn-O spinel was evaluated. The methods selected for the investigation were EDTA gel processes and solid-state reaction synthesis. From the obtained powders, sinters were prepared and assessed in terms of their properties as potential coating materials. Additionally, the influence of Ni and Fe dopants was evaluated. The results show that the EDTA gel processes method seems to...
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Enhanced acceptor concentration, proton conductivity, and hydration in multicomponent rare‐earth ortho‐niobates
PublikacjaThe structural properties of (La0.2Nd0.2Sm0.2Gd0.2Eu0.2)1−xCaxNbO4−δ (x = 0–0.05) series have been studied by X-ray powder diffraction at room temperature. The thermal properties were investigated using thermogravimetry, from which the concentration of proton defects was determined. Additionally, dilatometry studies were carried out, from which the thermal expansion coefficients and the phase transition temperature between low-...
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Elucidating photoluminescent properties of Eu‐doped Ca–Al–Si–O(–N) glasses and the local structures of Eu ions
PublikacjaEuropium (Eu) ion–doped luminescent materials have attracted considerable attention for their numerous optical applications. Eu-doped Ca–Al–Si–O(–N) glasses were synthesized from a mixture of oxynitride glasses and Eu2O3 powder using a standard melt-quenching technique in a radiofrequency furnace. The source Eu trivalent ions primarily changed to Eu2+ during melting, and the ratio of Eu2+ ions increased with an increase in Eu content...
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Wojciech Sadowski prof. dr hab. inż.
OsobyWojciech Sadowski (ur. 2.02.1954 r. w Ostaszewie), naukowiec, polski inżynier, profesor Politechniki Gdańskiej, specjalista z fizyki ciała stałego, nanotechnologii, optoelektroniki. Studia wyższe ukończył w 1979 r. w Leningradzkim Instytucie Elektrotechnicznym w Leningradzie w specjalności dielektryki i półprzewodniki, uzyskując tytuł zawodowy magistra inżyniera elektronika. Od 1979 r. pracuje na Politechnice Gdańskiej, pełniąc...
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Hebb–Wagner polarization method for determining the oxygen ion conductivity in barium cerate-zirconate
PublikacjaIn this work, the partial conductivity of oxygen ions in BaCe0.6Zr0.2Y0.2O3 was studied at different temperatures and water partial pressures. For this purpose, a modified DC Hebb–Wagner polarization method with an electrode blocking for protons and electrons was used. A new type of measuring cell as well as a suitable calculation model were proposed for the determination of partial oxygen ionic conductivity in materials with three...
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Wear in siding friction tests. Ring-on-ring contact. Sintered alumina ceramics (98%). Paraffin oil lubrication. Specim. sets #20-#21, #22-#23, #24-#25, #26-#27, #28-#29,#30 - #31. Run time: 0-4h. High frequency burst recording.
Dane BadawczeWear in sliding friction tests in ring-on-ring contact. Sintered alumina ceramics (98%) in self-mated contact. Lubrication: paraffin oil. Sliding velocity: 0.2 m/s. Mean contact stress: 10 MPa. Test rig: PT-3 Tribometer. High frequency burst recording.Running time: 0 - 4h.Specimen sets:Specim. sets (# [upper, rotating] - #[lower, non-rotating]):#20-#21,...
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A review: Fabrication of porous polyurethane scaffolds
PublikacjaThe aim of tissue engineering is the fabrication of three-dimensional scaffolds that can be used for the reconstruction and regeneration of damaged or deformed tissues and organs. A wide variety of techniques have been developed to create either fibrous or porous scaffolds from polymers, metals, composite materials and ceramics. However, the most promising materials are biodegradable polymers due to their comprehensive mechanical...
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Educational and cognitive aspects of adaptation of nonuse spaces in monumental sacral objects.
PublikacjaThe area of attics and towers in historic churches in Europe are yet quite inaccessible places for visitors, shrouded in the atmosphere of mysticism, hiding many secrets. Introduction of the new public function into the non-used zones of the monumental sacral objects has many aspects including educational and cognitive ones which are discussed in the following article. The article indicates items that can be found in the zone above...
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Impact of strontium non-stoichiometry of SrxTi0.3Fe0.7O3-δ on structural, electrical, and electrochemical properties for potential oxygen electrode of intermediate temperature solid oxide cells
PublikacjaThis work presents the results of a comprehensive study on the impact of the A-site non-stoichiometry of SrxTi0.3Fe0.7O3-δ (x = 0.90, 0.95, 1.00, 1.05) ceramics on their physicochemical properties. The materials were fabricated by the conventional solid-state reaction method and their structure was determined by X-ray diffractometry, X-ray photoelectron spectroscopy and electron microscopy. Their sintering and thermal expansion...
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Effect of MAO coatings on cavitation erosion and tribological properties of 5056 and 7075 aluminum alloys
PublikacjaTwo ceramic coatings have been applied on 5056 and 7075 aluminum alloy by microarc oxidation (MAO) technology. The mass losses, surface morphologies and the phase constituents of the MAO coatings before and after cavitation tests were examined by means of digital scales, scanning electron microscopy (SEM) and X-ray diffraction (XRD), respectively. In order to assess the impact of the mechanical properties of the surface layer on...
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Roofing Materials as Pollution Emiters - Concentration Changes During Runoff
PublikacjaThe influence of roofing material on concentration of pollutants in roof runoff waters and changes of pollution concentration in time were investigated. In field studies four roofing material types were taken into consideration - ceramic tile, bituminous membrane, asbestos tile and zinc sheeting. Samples were collected since November 2007 to March 2008, anions, cations, metals, PAHs, pesticides and PCB were determined. The existence...
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Electromagnetic forced vibrations of composite nanoplates using nonlocal strain gradient theory
PublikacjaThis article is intended to analyze forced vibrations of a piezoelectric-piezomagnetic ceramic nanoplate by a new refined shear deformation plate theory in conjunction with higher-order nonlocal strain gradient theory. As both stress nonlocality and strain gradient size-dependent effects are taken into account using the higher-order nonlocal strain gradient theory, the governing equations of the composite nanoplate are formulated....
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Experimental study on earthquake-induced pounding between structural elements made of different building materials
PublikacjaCelem artykułu jest pokazanie wyników dwóch eksperymentów dotyczących zderzeń pomiędzy elementami wykonanymi z różnych materiałów budowlanych, takich jak: stal, beton, drewno i ceramika. Pierwszy z nich polegał na zrzucaniu kul na płaską powierzchnię, drugi dotyczył zderzeń modeli konstrukcji poddanych wymuszeniom sejsmicznym na stole wstrząsowym. Wyniki testów pokazują, iż wpływ materiału elementów kolidujących ze sobą na zachowanie...
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Hydrożele
PublikacjaOd wieków ludziom towarzyszyły trzy główne rodzaje materiałów: szkło, ceramika i metale. Wraz z rozwojem cywilizacji poszukuje się coraz to nowszych substancji, które wykazują cenne właściwości i pozwalają na szerokie zastosowanie. Jednym z takich przykładów są hydrożele, które często nazywane są superabsorbentami. Jak sama nazwa wskazuje są to żele zawierające wodę. Podstawowym elementem ich budowy jest polimer, czyli wielkocząsteczkowa...