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Search results for: 8-HYDROXYQUINOLINE
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Novel bio-based thermoplastic poly(ether-urethane)s. Correlations between the structure, processing and properties
PublicationThe main purpose of this work was to analyze the effect of the number of unreacted isocyanate groups and the [NCO]/[OH] molar ratio during the chain extension of a prepolymer during the polymerization process on the structure, processing and selected properties of thermoplastic poly(ether-urethane)s. Three series of novel thermoplastic polyurethanes were obtained via a prepolymer route. Three prepolymers were synthesized from diisocyanate...
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Treatment of landfill leachate in a constructed free water surface wetland system over a decade – Identification of disturbance in process behaviour and removal of eutrophying substances and organic material
PublicationAn 8 ha free water surface wetland system in Örebro, Sweden, which has sediment traps followed by 10 ponds for treatment of landfill leachate in the methanogenic stage, was studied from 2003 to 2012. The wetland was irregularly loaded and the leachate characteristics showed high temporal and spatial variability, so Multivariate Statistical Process Control was chosen as the diagnostic tool for detecting anomalies prior to assessing...
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Superconductivity in the intermetallic compound Zr5Al4
PublicationPolycrystalline Zr5Al4 was synthesized using the arc-melting method. Powder X-ray diffraction confirms the previously reported crystal structure of the Ti5Ga4-type P63/mcm with lattice parameters: a = 8.4312(6) A , and c = 5.7752(8) A . Electrical resistivity and low-temperature magnetic susceptibility measurements indicate that Zr5Al4 exhibits superconducting behavior below 2 K. The normalized heat capacity jump at Tc= 1.82 K...
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Algorytm dyskretnej transformacji falkowej zoptymalizowany dla implementacji w mikrokontrolerze
PublicationNajczęściej stosowane algorytmy dyskretnej transformacji falkowej (DWT) wymagają sporych mocy obliczeniowych i dużych ilości pamięci danych, same obliczenia natomiast wykonywane są na liczbach rzeczywistych. Nie można ich zatem bezpośrednio zastosować w mikrontrolerach. Praca przedstawia propozycję optymalizacji algorytmu dyskretnej transformacji falkowej pod kątem implementacji w mikrontrolerze 8-bitowym. Dokonano przyspieszenia...
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Analysis of hydrodynamic pressure fields of motorboats and pontoons in shallow water
PublicationThe article presents the results of calculations of the pressure fields generated by a motorboat at the bottom of a shallow sea. Calculations were made using the boundary elements method (BEM), arranged on the surface of the boat and the bottom of the sea. This method is described in [3], and applied on a free surface linearized boundary condition. Results for four different lengths of motorboats, from 2.85 m to 9.5 m, sea depth...
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Revisiting Toroidal Dipolar Moment in Planar Metamaterial
PublicationThis article revisits the electric, magnetic, and toroidal dipolar moments in the metamaterial structure and presents the flatland design for generating a toroidal dipolar response for the electromagnetic plane wave at normal incidence. Based on the numerical analysis of the surface current, the electric field, the magnetic field, and the quantitative analysis of scattered power supported by the electromagnetic multipole theory,...
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Local hidden–variable models for entangled quantum states
PublicationWhile entanglement and violation of Bell inequalities were initially thought to be equivalent quantum phenomena, we now have different examples of entangled states whose correlations can be described by local hidden-variable models and, therefore, do not violate any of the Bell inequalities. We provide an up-to-date overview of the existing literature regarding local hidden-variable models for entangled quantum states, in both...
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Experimental research of the effect of face milling strategy on the flatness deviations
PublicationIn this paper the dependencies between face milling strategy of EN AW6082-T6 aluminum alloy samples, with difference thicknesses (6, 8, and 12 mm) and two cold rolling directions, and flatness deviations were presented. Three strategies of milling included different proportions of material removed from both sides of the plates. This approach allowed to control the proportions of residual surface stresses on both sides of the specimens,...
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Impact of the Alkyl Side Chains of Cations and Anions on the Activity and Renaturation of Lysozyme: A Systematic Study Performed Using Six Amino‐Acid‐Based Ionic Liquids
PublicationThe impact of the structure of ionic liquid on the activity and renaturation of lysozyme from the hen egg white (HEWL) was investigated. A set of six ionic liquids based on morpholinium cation and N-acylated amino acids as anions were exploited. The matrix used was based on two homologous series: one with N-acetyl-L-valinate [Val] as a common anion and morpholinium cation with a different number of carbon atoms in the n-alkyl chain...
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Optimisation and field assessment of poroelastic wearing course bond quality
PublicationCompared to typical asphalt mixtures, poroelastic mixtures are characterised by high porosity and high flexibility, which are desirable for traffic noise reduction. However, the same properties increase the risk of debonding from the lower layer, which is a significant source of premature damage. The study investigates which of the factors – tack coat agent, type and texture of the lower layer – have the greatest impact on interlayer...
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Inwestycja w wino – ocena sommelierów, rocznik i liczba punktów dystrybucji a wycena
PublicationW opracowaniu wyznaczono za pomocą współczynników korelacji liniowej Pearsona siłę i kierunek oddziaływania pomiędzy: ceną wina a rocznikiem, ceną wina a oceną sommelierów oraz ceną wina a liczbą punktów dystrybucji. Analizie poddano 8 szczepów winnych z rejonu Bordeaux. Najsilniejszy związek odnotowano pomiędzy ceną wina a rocznikiem trunku. W artykule obliczono także wybrane statystyki opisowe dla ceny wina, oceny przyznawanej...
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A new quaternion-based encryption method for DICOM images
PublicationIn this paper, a new quaternion-based lossless encryption technique for digital image and communication on medicine (DICOM) images is proposed. We have scrutinized and slightly modified the concept of the DICOM network to point out the best location for the proposed encryption scheme, which significantly improves speed of DICOM images encryption in comparison with those originally embedded into DICOM advanced encryption standard...
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A Comparative Study on Methods of Distinction Between Near- and Far-Side Defects as Techniques Used Alongside with the Magnetic Flux Leakage Testing
PublicationResults of the finite element analysis show that a far-side defect in a steel plate, with the depth greater by 10% of the plate thickness than a near-side defect, can produce a very similar magnetic flux leakage (MFL) signal. Due to the fact that a measurement of MFL itself can lead to misclassification of a far-side defect as a near-side one, and thus to underestimation of its depth, a comparative study of three complementary...
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A concept for reducing PM 10 emissions for car brakes by 50%
PublicationWith regard to airborne particles with an aerodynamic diameter of less than 10 μm (PM10), in countries in the European Union, the mass of brake emissions equals approximately 8–27% of the total traffic-related emissions. Using a research methodology combining tests at different scale levels with contact mechanics simulations and PM10 chemical characterization, the REBRAKE EU-financed project had the following aims: i) to demonstrate...
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Design, synthesis and biological evaluation of novel N-phosphorylated and O-phosphorylated tacrine derivatives as potential drugs against Alzheimer’s disease
PublicationIn this work, we designed, synthesised and biologically investigated a novel series of 14N- and O-phosphorylated tacrine derivatives as potential anti-Alzheimer’s disease agents. In the reaction of 9-chlorotacrine and corresponding diamines/aminoalkylalcohol we obtained diamino and aminoalkylhydroxy tacrine derivatives. Next, the compounds were acid to give final products 6–13 and 16–21 that were characterised by 1H, 13 C, 31P...
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Wyznaczenie obciążeń na poszycie okrętu wywołanych uderzeniem fal i uderzeniem w lód i ich wpływ na bezpieczeństwo okrętu
PublicationThe main problem is the vessels rather accurate determination of the hydrodynamic loads so-called hydroelasticity outside . This can be done by theoretical analysis , computer simulation or by experiment. This gives the hydrodynamic pressure distribution on the walls of the ship's hull and also on the walls of marine vessels .The most dangerous are the impact of extreme storm waves , the impact of the wharf and the impact zone...
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A New Microwave Ceramic – Polymer Composite with 0-3 Connectivity
PublicationGoal of the present research was to fabricate and study two-phase BiNbO4//PVDF composites with 0-3 connectivity. Such composite consists of there-dimensionally connected polymer matrix loaded with dielectric ceramic particles. In the present case BiNbO4 powder acted as an active phase (dispersed phase) whereas polyvinylidene fluoride (PVDF) acted as a non-active (passive) phase (matrix). BiNbO4//PVDF composites with the volume...
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Fast-response optoelectronic detection of explosives’ residues from the nitroaromatic compounds detonation: field studies approach
PublicationWe are presenting an application of optoelectronic nitrogen dioxide (NO2) analyzer based on cavity enhanced absorption spectroscopy in the detection of traces of explosives after detonation. It has been shown that the analyzer using blue-violet laser is able to detect explosive residues after the detonation of various amounts of nitroaromatic compounds (75g-1kg) with higher efficiency than the HPLC soil sample testing equipment,...
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Energy and valuable organic products recovery from anaerobic processes
PublicationChapter 8 contains: Introduction, Energy balance in wastewater treatment plants and potential energy recovery, Potential valuable products recovery, Anaerobic processes focused on liquid products recovery; Anaerobic digestion (AD) processes focused on gaseous products recovery, Processes enhancing energy and valuable organic products recovery, Conclusions and perspectives. Anaerobic processes offer different pathways for the recovery...
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Wartości wzorcowe wskaźników finansowych przedsiębiorstw giełdowych
PublicationKsiążka składa się z wstępu, sześciu rozdziałów, wniosków końcowych oraz pięciu załączników. Rozdział pierwszy rozpoczyna się przedstawieniem ogólnej klasyfikacji mierników realizacji celu przedsiębiorstwa oraz omówieniem ich podstawowych zalet i mankamentów. W dalszej części tego rozdziału przybliżony został sposób obliczania oraz interpretowania uwzględnionych w części empirycznej wskaźników finansowych. Ponadto w rozdziale...
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Medium-sized cyclic bis(anisylphosphonothioyl)- disulfanes and their corresponding cyclic sulfane-structures and most characteristic reactions
PublicationCyclic 8-, 9-, 10-, and 12-membered bis(anisylphosphonothioyl)disulfanes were synthesized. Next, structurally related 7 to 9-membered cis and trans sulfanes were isolated as a result of sulfur atom extrusion from the parent cyclic disulfanes. The results of the desulfurization of the disulfanes were compared to the results obtained for desulfurization of the respective bis(anisylphosphodithioates). Cyclic disulfanes predominantly...
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Essential oils as potential anti-staphylococcal agents
PublicationAntibiotic therapy of staphylococcal mastitis is characterized by significantly lower cure rates compared to infections caused by other microorganisms. Thus, it is necessary to search for new, alternative, non-antibiotic agents that are effective in the eradication of these bacteria. The aim of our research was to investigate the antimicrobial, especially anti-staphylococcal potential of a large collection (n=36) of essential oils...
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Impact of laser beam welding on mechanical behaviour of 2.25Cr–1Mo (P22) steel
PublicationThe use of welding processes in the manufacturing and repair of structures intended for the energy industry plays a key role in the guarantee of a continuous supply of fossil fuels, which is the basic condition for ensuring energy security. A square butt joint of 10 mm thick plate of 2.25Cr–1Mo (P22) steel was fabricated by autogenous laser beam welding process and then post-weld heat treatment (PWHT) for two sets of process parameters...
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Backscattering properties of southern Baltic herring
PublicationReliable TS(L) relationship is required to improve acoustic algorithms of abundanceestimation of Baltic herring. The relationships, empirically obtained in different parts of theBaltic Sea, produce up to 8 dB – difference in the herring TS. In order to develop an accurateTS(L) relationship, it is important to analyze factors controlling the TS variability. Thepossible impact of the regional difference...
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The Usefulness of Cyclic Diamidines with Different Core-substituents as Antitumor Agents
PublicationA series of related polycationic compds. has been screened for potential antitumor activity by the NCI's in vitro testing (one dose primary anticancer assay and the NCI-60 full panel screening). The GI50 values of triazines 3 and 4 are on av. 1.9 μM and 2.4 μM, resp. Furan 8 deserves mention too (1.9 μM). The biol. test results showed that carbazole 10 possessed cytotoxic activity in the nanomolar range, much better than...
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Eksploatacyjne obciążenia śrub napędowych pogłębiarek różnych typów w podstawowych stanach ich eksploatacji = Operational loads of propellers of different dredgers types in main service states
PublicationArtykuł przedstawia wyniki badań eksploatacyjnych dotyczących jednego z najważniejszych odbiorników energii mechanicznej na pogłębiarkach: śrub napędowych. Badania eksploatacyjne obejmowały pomiary parametrów charakteryzujących obciążenia śrub napędowych pogłębiarek w dwóch podstawowych stanach ich eksploatacji: roboty pogłębiarskie i pływanie swobodne. Przedstawione w pracy wyniki obejmują 10 pogłębiarek (8 pogłębiarek ssących...
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Method using square-pulse excitation for high-impedance spectroscopy of anticorrosion coatings
PublicationArtykuł prezentuje metodę spektroskopii impedancyjnej przeznaczonej do diagnostyki powłok antykorozyjnych na obiektach bezpośrednio w terenie. Aby skrócić czas uzyskania widma impedancji (w zakresie od 1 mHz do 1 MHz) do kilku minut, wykorzystano sygnały harmoniczne do pomiaru widma powyżej 10 Hz a impuls prostokątny w dolnym zakresie częstotliwości. Do wyznaczania widma użyto algorytmów DSP odpowiednich do sygnału pobudzenia....
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Broadband LFM signal source for a module-based diver detection sonar
PublicationPraca przedstawia koncepcję źródła impulsów sondujących sonaru DDS, dla pogrupowanych po stronie nadawczej elementarnych sekcji przetwornika w moduły 8 lub 16 elementowe. Na podstawie oszacowania teoretycznego i pomiarów czwórnikowych określono potrzebną moc wyjściową i topologię tych nadajników. Przedstawione są też uzyskane na drodze pomiarów charakterystyki częstotliwościowe modułów przetwornika, razem z zastosowanym układem...
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Growth, Crystal Structure and Magnetic Characterization of Zn-Stabilized CePtIn4
PublicationThe growth and characterization of CePtIn4, stabilized by 10% Zn substitution for In, is reported. The new material is orthorhombic, space group Cmcm (No. 63), with lattice parameters a = 4.51751(4) Å, b = 16.7570(2) Å, and c = 7.36682(8) Å, and the refined crystal composition has 10% of Zn substituted for In, i.e., the crystals are CePt(In0.9Zn0.1)4. Crystals were grown using a self-flux method: only growths containing Zn yielded...
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Detection and Mitigation of GPS Spoofing Based on Antenna Array Processing
PublicationIn this article authors present an application of spatial processing methods for GPS spoofing detection and mitigation. In the first part of this article, a spoofing detection method, based on phase delay measurements, is proposed. Accuracy and precision of phase delay estimation is assessed for various qualities of received signal. Spoofing detection thresholds are determined. Efficiency of this method is evaluated in terms of...
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Studies on origin of Polish honeys by two-dimensional gas chromatography Ocena pochodzenia surowcowego polskich miodów przy użyciu dwuwymiarowej chromatografii gazowej
PublicationPolish acacia, linden, rapessed and buckwheat-derived honeys and a honydew were analysed for presence of hydrocarbons, alcs., ketones and esters by 2-dimensional gas chromatog. to establish the markers for the honey origin. PrOH was found characteristic for acacia honey, Me(CH2)11OH for linden honey, Me(CH2)6CHOMe for honeydew and Me(CH2)8COOEt for the rapeseed honey. Wykorzystano technikę dwuwymiarowej chromatografii gazowej sprzężonej...
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Determination of SCFAs in water using GC-FID. Selection of the separation system
PublicationIn the present study, an analytical procedure was developed for the determination of short-chain fatty acids (SCFAs) in landfill leachate and municipal wastewater employing injection of aqueous samples to gas chromatograph with flame ionization detector (GC-FID). Chromatographic conditions such as a separation system, injection volume, oven temperature program were investigated and selected. With two columns, one with a polar (polyethylene...
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Studies on applicability of new solid-phase microextraction fibers for the selective extraction and determination of short - chain monocarboksylic acids
PublicationShort-chain monocarobxylic acids, sometimes referred to as volatile fatty acids (VFA), are a group of low molecular weight alkyl monocarboxylic acids that are widely distributed within the environment. These molecules contain any from 2 to 8 carbon atoms and originate from the anaerobic biodegradation of organic matter such as carbohydrates, proteins, and fats. These compounds are commonly found in the effluents from animal farming,...
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Widespread theta synchrony and high-frequency desynchronization underlies enhanced cognition
PublicationThe idea that synchronous neural activity underlies cognition has driven an extensive body of research in human and animal neuroscience. Yet, insufficient data on intracranial electrical connectivity has precluded a direct test of this hypothesis in a whole-brain setting. Through the lens of memory encoding and retrieval processes, we construct whole-brain connectivity maps of fast gamma (30-100 Hz) and slow theta (3-8 Hz) spectral...
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Piezoresponse force microscopy and dielectric spectroscopy study of Ba0.6Sr0.4TiO3 thin films
PublicationResearch on synthesis, characterization and determination of processing – structure – property relationships of commercially important ferroelectric thin films has been performed. The sol-gel-type solution deposition technique was applied to produce good quality thin films of Ba0.6Sr0.4TiO3 (BST60/40) chemical composition on the stainless steel substrates. The thin films were characterized in terms of their microstructure, crystal...
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Comment on "Measurements without probabilities in the final state proposal"
PublicationThe final state proposal [G.T. Horowitz and J.M. Maldacena, J. High Energy Phys.2004(2),8 (2004)] is an attempt to relax the apparent tension betweenstring theory and semiclassicalarguments regarding the unitarity of black hole evaporation. The authors of [R. Bousso and D.Stanford, Phys. Rev. D89, 044038 (2014)] analyze thought experiments where an infalling observerfirst verifies the entanglement between early and late Hawking...
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Do online reviews reveal mobile application usability and user experience? The case of WhatsApp
PublicationThe variety of hardware devices and the diversity of their users imposes new requirements and expectations on designers and developers of mobile applications (apps). While the Internet has enabled new forms of communication platform, online stores provide the ability to review apps. These informal online app reviews have become a viral form of electronic wordof-mouth (eWOM), covering a plethora of issues. In our study, we set ourselves...
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Testing method of analog parts for mixed signal microsystems based on microcontrolles.
PublicationZaproponowano nową metodę detekcji i lokalizacji pojedynczych uszkodzeń parametrycznych, która może znaleźć zastosowanie do samo-testowania sieci analogowych w mikrosystemach mieszanych sygnałowo sterowanych mikrokontrolerami. Metoda ta jest oparta na przekształceniu transformującym próbki odpowiedzi czasowej na pobudzenie impulsem prostokątnym na krzywe identyfikacyjne na płaszczyźnie. Metoda pozwala na detekcję i lokalizację...
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Pojęcie zarządzania, przedsiębiorczości i przewodzenia w teorii kierowania organizacją.
PublicationPoznając współczesne metody i style zarządzania oraz nowe doświadczenia i wyzwania, jakie niesie za sobą konkurencyjność jutra, rodzą się wątpliwości czy poglądy, że odrębnie można rozpatrywać pojęcie zarządzanie i przedsiębiorczość, są słuszne i czy teza ta nie jest błędna, podobnie jak błędne może być odróżnianie pojęcia menedżer od pojęcia lidera czy przedsiębiorcy. Myślę, że różnice między tymi wszystkimi pojęciami obecnie...
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Właściwości glikolizatów oraz zsyntezowanych z nich poliuretanów
PublicationCelem pracy było otrzymanie glikolizatów, jako półproduktów do syntezy poliuretanów. Glikolizaty otrzymywano w reakcji odpadowej miękkiej pianki poliuretanowej (PU) z glikolem butylenowym (GB) przy stosunkach GB : PU wynoszących 2:1, 1:1, 1:2, 1:5, 1:8 i 1:10. W reakcji stosowano katalizatory metaloorganiczne. Otrzymane związki scharakteryzowano poprzez oznaczenie lepkości (wiskozymetrem Brookfield'a), gęstości (piknometrem)...
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Chromatographic lipophilicity determination using large volume injections of the solvents non-miscible with the mobile phase
PublicationA new perspective in the lipophilicity evaluation through RP-HPLC is permitted by analysis of the retentionfactor (k) obtained by injecting large volumes of test samples prepared in solvents immiscible withmobile phase. The experiment is carried out on representative groups of compounds with increasedtoxicity (mycotoxins and alkaloids) and amines with important biological activity (naturally occurringmonoamine compounds and related...
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Electronic nose as a tool for differentiation of volatile organic compounds = Elektroniczny nos jako instrument do rozróżniania lotnych związków organicznych
PublicationW pracy porównano dwie metody analizy zapachów lotnych związków organicznych: klasyczną analizę opartą na percepcji ludzkiego węchu i technikę elektronicznego nosa. W przeprowadzonych badaniach za pomocą klasycznej analizy brało udział 8 ochotników w okresie 2 tygodni. Do instrumentalnej metody analizy zapachu wykorzystano zaprojektowany przez autorów prototypowy 6-cio czujnikowy elektroniczny nos. Przeprowadzone badania z wykorzystaniem...
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Performance and Energy Aware Training of a Deep Neural Network in a Multi-GPU Environment with Power Capping
PublicationIn this paper we demonstrate that it is possible to obtain considerable improvement of performance and energy aware metrics for training of deep neural networks using a modern parallel multi-GPU system, by enforcing selected, non-default power caps on the GPUs. We measure the power and energy consumption of the whole node using a professional, certified hardware power meter. For a high performance workstation with 8 GPUs, we were...
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Evaluation of headspace solid-phase microextraction for the analysis of volatile carbonyl compounds in spirits and alcoholic beverages
PublicationOpracowano metodę oznaczania C1-C6 związków karbonylowych w układzie GC-ECD w roztworach alkoholowych poprzez derywatyzację pentafluorobenzylohydroksy-aminą i mikroekstrakcję w fazie stacjonarnej z fazy nadpowierzchniowej. Zoptymalizowano warunki eksperymantalne: zawartość alkoholu, czas ekspozycji, temperaturę i sposób mieszania próbki. W metodzie tej najpierw przeprowadza się rozcieńczenie spirytusu lub napojów alkoholowych do...
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Coastline change-detection method using remote sensing satellite observation data
PublicationCoastal zones are not only the fundaments for local economics based on trade, shipping and transport services, but also a source of food, energy and resources. Apart from offering diverse opportunities for recreation and tourism, coastal zones provide protection against storms and other meteorological disturbances. Environmental information is also essential because of the direct influence on a country’s maritime zones, which are...
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Ellipsometric investigation of nitrogen doped diamond thin films grown in microwave CH4/H2/N2 plasma enhanced chemical vapor deposition
PublicationThe influence of N2 concentration (1%–8%) in CH4/H2/N2 plasma on structure and optical properties of nitrogen doped diamond (NDD) films was investigated. Thickness, roughness, and optical properties of the NDD films in the VIS–NIR range were investigated on the silicon substrates using spectroscopic ellipsometry. The samples exhibited relatively high refractive index (2.6 6 0.25 at 550 nm) and extinction coefficient (0.05 6 0.02...
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The Effect of Calcination Temperature on Structure and Photocatalytic Properties of WO3/TiO2 Nanocomposites
PublicationSeries ofWO3/TiO2 nanocompositeswere obtained by hydrothermal method followed by calcination in the temperature range from 400∘C to 900∘C. The characteristics of photocatalysts by X-ray diffractometry (XRD), scanning electron microscope (SEM), and diffuse reflectance spectroscopy (DRS) showed that increasing the calcination temperature from 400 to 900∘C resulted in change of photocatalytic activity under UV-Vis light.Moreover,...
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Carbon nitride exfoliation for photocatalysis and photocatalytic ozonation over emerging contaminants abatement
PublicationThe production of graphitic carbon nitride was studied with the addition of a following exfoliation step using ultrasounds, at different times. The treatment produced catalysts with much higher surface areas, from 2.18 m2 g 1 with no treatment to 28.34 m2 g 1 after 36 h of exfoliation. During exfoliation, melem was also produced, and may further enhance the photoluminescence and photocatalytic properties. The photocatalytic reaction...
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Adaptive Sampling for Non-intrusive Reduced Order Models Using Multi-Task Variance
PublicationNon-intrusive reduced order modeling methods (ROMs) have become increasingly popular for science and engineering applications such as predicting the field-based solutions for aerodynamic flows. A large sample size is, however, required to train the models for global accuracy. In this paper, a novel adaptive sampling strategy is introduced for these models that uses field-based uncertainty as a sampling metric. The strategy uses...
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Analysis of efficiency of phosphates sorption by different granulation of selected reactive material
PublicationIn the light of the need to find an effective way to remove phosphorus from wastewater, studies on the suitability of sorption materials in this process should be conducted. The aim of the study was to examine the potential benefits of using selected adsorbents to reduce orthophosphates from the model solution under steady conditions. The study was conducted on a laboratory scale using synthetic wastewater with concentration of...