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Determination of flavanols by liquid chromatography with fluorescence detection. Application to the characterization of cranberry-based pharmaceuticals through profiling and fingerprinting approaches
PublikacjaIn this work, a new method based on reversed-phase high-performance liquid chromatography (HPLC) with fluorescence detection (FLD) was established for the determination of catechins and related oligomeric proanthocyanidins (PACs) in cranberry-based pharmaceuticals. Compounds were recovered by liquid extraction using methanol/water/hydrochloric acid (60:39:1, v:v:v) as the extraction solvent. The chromatographic separation was carried...
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The role of centrifugal partition chromatography in the removal of β-asarone from Acorus calamus essential oil
PublikacjaΒ-asarone is a phenylpropane derivative present in the rhizomes of Acorus calamus, that was proved to exhibit toxic effects in humans. Because of its presence the whole plant that is commonly used in traditional medicine for its sedative, anti-inflammatory, neuroprotective and other properties has limited application nowadays. In the study, qualitative and quantitative analysis of a collection of nine essential oil (EO) samples...
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The New LM-PCR/Shifter Method for the Genotyping of Microorganism
PublikacjaTechniques relies on the ligation of appropriates adapters (LM-PCR) as AFLP, PCR MP and ADSRRS are successfully used for epidemiological studies for prokaryotic and eukaryotic microorganisms. In this study we propose a new method, called the LM-PCR/Shifter, based on the use of a Class IIS restriction enzyme giving restriction fragments with different 4 base 5' overhangs (Shifter) and the ligation of appropriate oligonucleotide...
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Study on the Positioning Accuracy of the GNSS/INS System Supported by the RTK Receiver for Railway Measurements
PublikacjaCurrently, the primary method for determining the object coordinates is positioning using Global Navigation Satellite Systems (GNSS) supported by Inertial Navigation Systems (INS). The main goal of this solution is to ensure high positioning availability, particularly when access to satellite signals is limited (in tunnels, areas with densely concentrated buildings and in forest areas). The aim of this article is to determine whether...
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LC–MS/MS analysis, antioxidant and anticholinergic properties of galanga (Alpinia officinarum Hance) rhizomes
PublikacjaGalanga (Alpinia officinarum Hance) is a pungent and aromatic rhizome, which is a member of the ginger family (Zingiberaceae). The rhizomes of this plant have been used as a traditional medicine in far east countries for relieving stomach ache, invigorating the circulatory system, treating colds, and reducing swelling. The aim of this study was to investigate antioxidant and anticholinergic properties of galanga. For this purpose,...
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Derecho Evolving from a Mesocyclone—A Study of 11 August 2017 Severe Weather Outbreak in Poland: Event Analysis and High-Resolution Simulation
PublikacjaThis study documents atmospheric conditions, development, and evolution of a severe weather outbreak that occurred on 11 August 2017 in Poland. The emphasis is on analyzing system morphology and highlighting the importance of a mesovortex in producing the most significant wind damages. A derecho-producing mesoscale convective system (MCS) had a remarkable intensity and was one of the most impactful convective storms in the history...
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Distribution and bioavailability of mercury in the surface sediments of the Baltic Sea
PublikacjaThe study aimed to determine the level of mercury (Hg) and its labile and stable forms in the surface sediments of the Baltic Sea. The work considers the impact of current and historical sources of Hg on sediment pollution, together with the influence of different environmental parameters, including water inflows from the North Sea. Surface sediments (top 5 cm) were collected in 2016–2017 at 91 stations located in different...
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Porównanie przemian termooksydatywnych zachodzących w wybranych olejach oliwkowych, oleinie palmowej i oleju rzepakowym podczas modelowego smażenia kawałków ziemniaków w głębokim tłuszczu
PublikacjaBadano przemiany zachodzące w tłuszczu podczas procesu "głębokiego smażenia" kawałków ziemniaków. Jako medium smażalnicze stosowano oleje: oliwkowe (pomace, sansa) oleinę palmową oraz rzepakowy. Określano zachodzące w nich zmiany takich wyróżników jak liczba kwasowa, liczba nadtlenkowa, anizydynowa, współczynnik ekstynkcji przy 232nm oraz zawartości frakcji polarnej, sumy dimerów i polimerów, współczynnik załamania światła oraz...
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The dynamics of the total outputs of Japanese information and communication technology sectors: A further study
PublikacjaThe purpose of this study is to continue the previous studies which discussed the impacts of the changes of final demands on the total outputs of the Information and Communication Technology (ICT) sectors of the specific country. More specifically, this study aims to conduct a deeper analysis regarding these impacts. This study focuses on the case of Japan. This study employs a demand-pull Input-Output (IO) quantity model, one...
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An air-assisted dispersive liquid phase microextraction method based on a hydrophobic magnetic deep eutectic solvent for the extraction and preconcentration of melamine from milk and milk-based products
PublikacjaIn the current research, a fast and sustainable air-assisted hydrophobic magnetic deep eutectic solvent-based dispersive liquid phase microextraction followed by UV–Vis spectrophotometry measurements was optimized for the extraction and determination of melamine in milk and milk-based products. The central composite design was applied for the optimization of factors affecting the recovery of melamine. Quantitative extraction of...
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Optimization of parallel implementation of UNRES package for coarse‐grained simulations to treat large proteins
PublikacjaWe report major algorithmic improvements of the UNRES package for physics-based coarse-grained simulations of proteins. These include (i) introduction of interaction lists to optimize computations, (ii) transforming the inertia matrix to a pentadiagonal form to reduce computing and memory requirements, (iii) removing explicit angles and dihedral angles from energy expressions and recoding the most time-consuming energy/force terms...
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Improving the Accuracy in Sentiment Classification in the Light of Modelling the Latent Semantic Relations
PublikacjaThe research presents the methodology of improving the accuracy in sentiment classification in the light of modelling the latent semantic relations (LSR). The objective of this methodology is to find ways of eliminating the limitations of the discriminant and probabilistic methods for LSR revealing and customizing the sentiment classification process (SCP) to the more accurate recognition of text tonality. This objective was achieved...
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A CMOS Pixel With Embedded ADC, Digital CDS and Gain Correction Capability for Massively Parallel Imaging Array
PublikacjaIn the paper, a CMOS pixel has been proposed for imaging arrays with massively parallel image acquisition and simultaneous compensation of dark signal nonuniformity (DSNU) as well as photoresponse nonuniformity (PRNU). In our solution the pixel contains all necessary functional blocks: a photosensor and an analog-to-digital converter (ADC) with built-in correlated double sampling (CDS) integrated together. It is implemented in...
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Molecular basis of lipopolysaccharide heterogeneity in Escherichia coli: envelope stress-responsive regulators control the incorporation of glycoforms with a third 3-deoxy-α-D-manno-oct-2-ulosonic acid and rhamnose.
PublikacjaMass spectrometric analyses of lipopolysaccharide (LPS) from isogenic Escherichia coli strains with nonpolar mutations in the waa locus or overexpression of their cognate genes revealed that waaZ and waaS are the structural genes required for the incorporation of the third 3-deoxy-α-D-manno-oct-2-ulosonic acid (Kdo) linked to Kdo disaccharide and rhamnose, respectively. The incorporation of rhamnose requires prior sequential incorporation...
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Chemical denudation and the role of sulfide oxidation at Werenskioldbreen, Svalbard
PublikacjaThis study aims to determine the rate of chemical denudation and the relationships between dominant geochemical reactions operating in the proglacial and subglacial environments of the polythermal glacier Werenskioldbreen (SW Svalbard) during an entire ablation season. Water sampling for major ion chemistry was performed at a proglacial hydrometric station and from subglacial outflows from May to September 2011. These data were...
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The Influence of Loop Heat Pipe Evaporator Porous Structure Parameters and Charge on Its Effectiveness for Ethanol and Water as Working Fluids
PublikacjaAbstract: This paper presents the results of experiments carried out on a specially designed experimental rig designed for the study of capillary pressure generated in the Loop Heat Pipe (LHP) evaporator. The commercially available porous structure made of sintered stainless steel constitutes the wick. Three different geometries of the porous wicks were tested, featuring the pore radius of 1, 3 and 7 um. Ethanol and water as two...
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Stable and degradable microgels linked with cystine for storing and environmentally triggered release of drugs
PublikacjaEnvironmentally sensitive, degradable microgels based on poly(N-isopropylacrylamide) (pNIPA) crosslinked with the diacryloyl derivative of cystine (BISS) were synthesized by applying surfactant-free emulsion polymerization. pNIPA contributed the sensitivity to temperature to the microgels and the cross-linker made them degradable and sensitive to pH. The morphology of the microgels was investigated by using scanning and transmission...
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analizator do spektroskopii wysokoimpedancyjnej z wykorzystaniem cps
PublikacjaW artykule przedstawiono opracowany i wdrożony do produkcji seryjnej analizator do spektroskopii wysokoimpedancyjnej. Dzięki zastosowaniu obwodu wejściowego w postaci sondy pomiarowej (2 i 3 zaciskowej) analizator umożliwia pomiary w zakresie 100 ohm < |Zx| < 100 Gohm. Do wyznaczania składowych ortogonalnych sygnałów pomiarowych wykorzystano technikę cyfrowego przetwarzania sygnałów. Pozwoliła ona na pomiary w szerokim zakresie...
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Badania właściwości eksploatacyjnych betonu asfaltowego o nieciągłym uziarnieniu i mastyksu grysoweo SMA do cienkich warstw ścieralnych
PublikacjaArtykuł przedstawia wyniki badań właściwości mieszanek mineralno-asfaltowych przeznaczonych do cienkich warstw ścieralnych. Wykonano badania odporności mieszanek na: starzenie, działanie wody i mrozu, deformacje trwałe oraz na spękania niskotemperaturowe. Przebadano 2 rodzaje mieszanek: beton o nieciągłym uziarnieniu i mastyks grysowy SMA. Zastosowano 4 rodzaje asfaltów: 1 zwykły, niemodyfikowany i 3 modyfikowane. Stwierdzono,...
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Three-Dimensional Fractography for Conventional and Additive Manufactured Steels After Bending-Torsion Fatigue
PublikacjaIn this study, fracture surface topography parameters were measured to investigate the effects of multiaxial loading. In order to assess the metrological aspects of fracture for notched specimens made of high-strength steels processed by both conventional and additively manufacturing (AM) techniques, an optical surface profilometer was used. Three bending moment to torsion moment ratios (B/T) were studied, i.e. 2, 1 and 2/3. The...
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Badania eksperymentalne prostownika osiemnastopulsowego o mocy 150 kVA z opcjonalnym szeregowym energetycznym filtrem aktywnym
PublikacjaW artykule przedstawiono system sterowania oraz wybrane wyniki badań eksperymentalnych przekształtnika AC / DC składającego się z osiemnastopulsowego diodowego prostownika na bazie dławików sprzężonych i szeregowego energetycznego filtra aktywnego. Przebadano i porównano trzy konfiguracje przekształtnika o mocy 150kVA: (1) osiemnastopulsowy prostownik bez dodatkowych elementów, (2) prostownik z dodatkowym dławikiem sieciowym oraz...
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An efficient algorithm for finding ideal schedules
PublikacjaPodejmujemy problem szeregowania zadań jednostkowych z zadanymi czasamy przybycia i zależnościami kolejnościowymi. Uszeregowanie jest idealne jeśli jednocześnie minimalizuje maksymalny oraz średni czas zakończenia zadania. Podajemy przyklad pokazujący, że uszeregowania idealne nie istnieją dla relacji zależności zadań będącej drzewem, gdy dopuścimy możliwość wystąpienia przerwań. Z drugiej strony podajemy algorytm o złożoności...
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Scenarios in regional planning – theory and practice in Poland
PublikacjaAbstract. It is important to recognise future conditions in planning because it primes future actions. Scenarios are useful prognostic tools, especially when the social and institutional behaviour plays a crucial role. The aims of the paper are: (1) to indicate the roles and the place of scenarios in the strategic plan building process; (2) to analyse and evaluate the application of scenarios in regional planning in Poland; (3)...
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Second-order Stark effect and polarizability of a relativistic two-dimensional hydrogenlike atom in the ground state
PublikacjaThe second-order Stark effect for a planar Dirac one-electron atom in the ground state is analyzed within the framework of the Rayleigh-Schrödinger perturbation theory, with the use of the Sturmian series expansion of the generalized Dirac-Coulomb Green's function. A closed-form analytical expression for the static dipole polarizability of that system is found. The formula involves the generalized hypergeometric function ${}_{3}F_{2}$...
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The effect of package type on selected parameters of nutritional quality of the chilled stored red sauerkraut
PublikacjaThe key elements responsible for the quality of food are the technologies used toprocess raw materials and preserve obtained products. The aim of this paper wasto investigate the effect of package type (bags made from low density polyethylene[PE-LD] and the metallized polyethylene terephthalate [PET met/PE foil]) onselected quality parameters of the chilled stored red sauerkraut. Vegetables wereanalyzed before packaging and after...
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Influence of Analyte Flow Rate on Signal and Response Time of the Amperometric Gas Sensor with Nafion Membrane
PublikacjaW publikacji przedstawiono rezultaty badań nad wpływem zmian objętościowego natężenia przepływu gazu na sygnał i czas odpowiedzi prototypowego czujnika ditlenku siarki z membraną nafionową. Porównywano właściwości czujników różniących się materiałem elektrody pracującej oraz składem roztworu elektrolitu wewnętrznego. Zastosowano elektrody pracujące wykonane z napylonych próżniowo na powierzchnię membrany nafionowej złota i platyny....
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Diagnostyka techniczna węzła zawieszenia ślizgacza odbieraka prądu - badania laborarotyjne
PublikacjaWęzeł zawieszenia ( odsprężynowania ) ślizgacza odbieraka prądu odgrywa istotną rolę w dynamicznym przebiegu odbioru prądu, zwłaszcza przy dużych prędkościach jazdy. Proponowana metoda diagnozowania jego sprawności polega na pobudzeniu drgań układu sieć jezdna, ślizgacza i konstrukcja nożycowa odbieraka. Drgania te mają różny charakter przy różnej sztywności węzła zawieszenia ślizgacza. Analiza spektralna tych drgań może być sygnałem...
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Effective residue-to-binary converter with the Chinese Remainder Theorem
PublikacjaKonwersja liczb z systemu resztowego do systemu binarnego jest podstawową operacją we wszystkich układach cyfrowego przetwarzania sygnałów, które wykorzystują system resztowy. W niniejszej pracy zaproponowano nową metodę konwersji opartą o chińskie twierdzenie o resztach dla modułów 5- i 6-bitowych. Specyficzną cechą nowej metody jest sposób obliczania tzw. współczynnika nadmiaru w formule chińskiego twierdzenia o resztach, co...
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The Influence of Selected Parameters of Numerical Modelling on Strains and Stresses at Weld Toe Notch
PublikacjaLatest development in the field of welding technology and prefabrication enabled massive production of thin-walled sandwich structures. Multi-layered sandwich structures are fabricated with the use of high-power CO2 lasers, friction welding, arc welding, hybrid welding, or other technique designed for the special purpose. Steel or aluminium alloy plates with thickness between 1 and 5 mm are connected by internal stiffeners. Strength...
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Signals features extraction in radioisotope liquid-gas flow measurements using wavelet analysis
PublikacjaKnowledge of the structure of a flow is significant for the proper conduct of a number of industrial processes. In this case, a description of a two-phase flow regimes is possible by use of the time-series analysis in time, frequency and state-space domain. In this article the Discrete Wavelet Transform (DWT) is applied for analysis of signals obtained for water-air flow using gamma ray absorption. The presented method was illustrated...
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Bioconversion of waste materials to hydrogen via dark fermentation using Enterobacter aerogenes
PublikacjaHydrogen can be obtained via dark fermentation with the use of anaerobic Enterobacter aerogenes. The efficiency of hydrogen production by fermentation techniques is strongly dependent on the con-ditions used i.e. the pH range, temperature, composition of fermentation broths, oxygen content, or even the presence of substances with potentially inhibitory effects on the microbiological culture [1-4]. The paper describes the study...
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DBpedia and YAGO Based System for Answering Questions in Natural Language
PublikacjaIn this paper we propose a method for answering class 1 and class 2 questions (out of 5 classes defined by Moldovan for TREC conference) based on DBpedia and YAGO. Our method is based on generating dependency trees for the query. In the dependency tree we look for paths leading from the root to the named entity of interest. These paths (referenced further as fibers) are candidates for representation of actual user intention. The...
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NLP Questions Answering Using DBpedia and YAGO
PublikacjaIn this paper, we present results of employing DBpedia and YAGO as lexical databases for answering questions formulated in the natural language. The proposed solution has been evaluated for answering class 1 and class 2 questions (out of 5 classes defined by Moldovan for TREC conference). Our method uses dependency trees generated from the user query. The trees are browsed for paths leading from the root of the tree to the question...
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The unstable thermoelectric effect in non-stoichiometric Cu2Se during the non-equilibrium phase transition
PublikacjaThe superionic α ↔ β phase transition in Cu1.96Se thermoelectric material is investigated by means of thermal analysis (DSC) and measurements of Seebeck coefficient and electrical conductivity. Results of the DSC measurements with 1–10 K/min heating and cooling rates show that the material is close to the equilibrium phase composition during the transformation. However, the kinetic limitation of the process exists, which is indicated...
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Hybrid cross-linked chitosan/protonated-proline:glucose DES membranes with superior pervaporation performance for ethanol dehydration
PublikacjaThis work explores a protonated L-proline:glucose (molar ratio 5:1) deep eutectic solvent (DES) in fabricating biopolymer membranes utilizing chitosan (CS). Initially, the miscibility of CS and DES to prepare homogeneous dense blend membranes has been investigated. Different techniques, such as scanning electron microscopy, contact angle (CA), atomic force microscopy (AFM), Fourier transformed infrared spectroscopy (FTIR) and swelling...
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Predicting the impact of traffic–induced vibrations on buildings using artificial neural networks
PublikacjaTraffic–induced vibrations may constitute a considerable load to a building, cause cracking of plaster, cracks in load–bearing elements or even a global structural collapse of the whole structure [1-4]. Vibrations measurements of real structures are costly and laborious, not justified in all cases. The aim of the paper is to create an original algorithm, to predict the negative dynamic impact on the examined residential building...
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Synthesis, physicochemical and theoretical studies on new rhodium and ruthenium dimers. Relationship between structure and cytotoxic activity
PublikacjaTwo dimeric compounds of the general formulae (Et3NH)2[Rh2(μ2-L)4Cl2] (1) (where L = thiophene-2-carboxylate) and [((η6-p-cymene)Ru)2(μ-Cl)3]PF6 (2) have been synthesized using a new method. The unique anionic complex 1 (space group P bca) has octahedral coordination in which the equatorial positions are occupied by the oxygen atoms of four thiophene-2-carboxylates in a paddle wheel fashion. In complex 2 (space group ), each Ru(II)...
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Determination of MDPBP in postmortem blood samples by gas chromatography coupled with mass spectrometry
PublikacjaMDPBP (1-(3,4-methylenedioxyphenyl)-2-(1-pyrrolidinyl)-1-butanone) is a new psychoactive substance sold on the black market. It has been a controlled drug of abuse in Poland and China since 2015 as some toxic and fatal cases connected with use of synthetic cathinone derivatives were observed. The fatal case outlined here concerns a 19 year-old man, who was found dead with an envelope containing white powder lying nearby the cadaver....
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A new strategy for PET depolymerization: Application of bimetallic MOF-74 as a selective catalyst
PublikacjaLarge-volume production of poly(ethylene terephthalate) (PET), especially in the form of bottles and food packaging containers, causes problems with polymer waste management. Waste PET could be recycled thermally, mechanically or chemically and the last method allows to obtain individual monomers, but most often it is carried out in the presence of homogeneous catalysts, that are difficult to separate and reuse. In view of this,...
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Chromium (III) removal by perennial emerging macrophytes in floating treatment wetlands
PublikacjaFloating treatment wetlands (FTWs) are a sustainable solution to treat polluted water, but their role in chromium (Cr(III)) removal under neutral pH conditions remains poorly understood. This study evaluated the potential of FTWs planted with two perennial emergent macrophytes, Phragmites australis and Iris pseudacorus, to remove Cr(III) and nutrients (N and PO4-P) from water containing 7.5 mg/L TN, 1.8 mg/L PO4-P, and Cr(III)...
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Optical and electrical properties of ultrathin transparent nanocrystalline boron-doped diamond electrodes
PublikacjaThe optical properties of ultrathin (less than 100 nm) boron-doped nanocrystalline diamond (B-NCD) film were investigated in a wavelength range of 200 ÷ 20000 nm. The B-NCD refractive index showed values close to that of monocrystalline diamond (n = 2.45) in a broad wavelength range (450 ÷ 4000 nm). A transmittance up to 70% and the average film thickness of 70 nm were achieved. A special cone-shaped shim was used in the deposition...
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Antibiotic resistance and prevalence of class 1 and 2 integrons in Escherichia coli isolated from two wastewater treatment plants, and their receiving waters (Gulf of Gdansk, Baltic Sea, Poland)
PublikacjaIn this study, antimicrobial-resistance patterns were analyzed in Escherichia coli isolates from raw (RW) and treated wastewater (TW) of two wastewater treatment plants (WWTPs), their marine outfalls (MOut), and mouth of the Vistula River (VR). Susceptibility of E. coli was tested against different classes of antibiotics. Isolates resistant to at least one antimicrobial agent were PCR tested for the presence of integrons. Ampicillin-resistant...
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Low temperature broad band dielectric spectroscopy of multiferroic Bi6Fe2Ti3O18 ceramics
PublikacjaIn the present research the tool of broadband dielectric spectroscopy was utilized to characterize dielectric behavior of Bi6Fe2Ti3O18 (BFTO) Aurivillius-type multiferroic ceramics. Dielectric response of BFTO ceramics was studied in the frequency domain (Δν=0.1Hz – 10MHz) within the temperature range ΔT=-100°C – 200°C. The Kramers-Kronig data validation test was employed to validate the impedance data measurements and it was found...
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Digits Recognition with Quadrant Photodiode and Convolutional Neural Network
PublikacjaIn this paper we have investigated the capabilities of a quadrant photodiode based gesture sensor in the recognition of digits drawn in the air. The sensor consisting of 4 active elements, 4 LEDs and a pinhole was considered as input interface for both discrete and continuous gestures. Index finger and a round pointer were used as navigating mediums for the sensor. Experiments performed with 5 volunteers...
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S-scheme heterojunction Bi2O3-ZnO/Bentonite clay composite with enhanced photocatalytic performance
PublikacjaThe industrial waste water is always a bottleneck problem in the modern civilization of the present era. In a quest to develop effective methods for the elimination of lethal pollutants from the waste water and water remediation, this work is focused on the development of a rapid and proficient approach for preparing supported binary metal oxide catalyst for photocatalytic advance oxidation process used in waste water treatment...
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Unusual behavior of secondary amine group as a leaving group
PublikacjaIn our recent project we focused on reactivity of2,2-dimethyl-4,6-dioxane-1,3-dione carbamoilo- and thiocarbamoylo- derivatives as a ketenesource. Meldrum`s acid derivatives after thermal decomposition gives substituted keteneswith stoichiometric yield, that can be trapped with various spectrum of nucleophiles likealcohols, thiols, amine, imines etc. In case of5-[3-(dimethylamino)-sulfanyl-propyliden]-2,2-dimethyl-1,3-dioxane-4,6-dione...
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Method of earth fault loop impedance measurement without nuisance tripping of RCDs in 3-phase low-voltage circuits
PublikacjaVerification of electrical safety in low-voltage power systems includes the measurement of earth fault loop impedance. This measurement is performed to verify the effectiveness of protection against indirect contact. The widespread classic methods and meters use a relatively high value of the measuring current (5–20) A, so that they are a source of nuisance tripping of residual current devices (RCDs). The meters dedicated to circuits...
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Nickel-nanodiamond coatings electrodeposited from tartrate electrolyte at ambient temperature
PublikacjaIn this study, nanocrystalline Ni and Ni-diamond coatings were obtained by electrodeposition from tartrate electrolyte at ambient temperature aiming at improving corrosion and wear properties of the material. The created surfaces were investigated with regard to microhardness, adhesion, wear- and corrosion-resistance. The various methods such as atomic force microscopy, scanning electron microscopy, electrochemical impedance spectroscopy...
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Photocatalytical degradation of toluene and cyclohexane using LED illumination
PublikacjaA sol-gel process followed by hydrothermal reaction was used to prepare coupled WO3-TiO2 photocatalysts with varying amounts of WO3 in respect to TiO2 (3 mol% and 5 mol% respectively). Additionally, photocatalysts have been subjected to different calcination temperatures of 400ºC and 800ºC, which allowed us to compare how these affect photodegradation efficiency. Photocatalysts were characterized under a scanning electron microscope,...
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Effect of TiO2 Concentration on Microstructure and Properties of Composite Cu–Sn–TiO2 Coatings Obtained by Electrodeposition
PublikacjaIn this work, Cu–Sn–TiO2 composite coatings were electrochemically obtained from a sulfate bath containing 0–10 g/L of TiO2 nanoparticles. The effect of TiO2 particles on kinetics of cathodic electrodeposition has been studied by linear sweep voltammetry and chronopotentiometry. As compared to the Cu–Sn alloy, the Cu–Sn–TiO2 composite coatings show rougher surfaces with TiO2 agglomerates embedded in the metal matrix. The highest...