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Search results for: SPM
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Rapid method for the determination of organochlorine pesticides and PCBs in fish muscle samples by microwave-assisted extraction and analysis of extracts by GC-ECD
PublicationA procedure for the multiresidue determination of organochlorine pesticides and polychlorinated biphenyls in fish muscle samples has been developed. The method is based on the microwave-assisted extraction (MAE) of food samples from an acetonitrile-water (95 + 5, v/v) mixture followed by SPE cleanup of the extracts and analysis by GC with an electron capture detector. MAE operational parameters, such as the extraction solvent,...
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The efficiency of scientific activities and technology transfer in higher education in Poland
PublicationThe objective of the article is to measure and evaluate the efficiency of scientific activity and technology transfer to the economy by public higher education institutions (HEIs) in Poland and to formulate recommendations for state policy to increase the effectiveness of the technology transfer process by them. The study measured scientific activity and technology transfer separately in two groups of higher education institutions...
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Effect of kenaf fibre modification on morphology and mechanical properties of thermoplastic polyurethane materials
PublicationThe presented study examined the morphology and mechanical properties of biocomposites obtained from kenaf natural fibre and thermoplastic polyurethane. Kenaf was modified using various methods, namely: acetylation, blocked isocyanate, maleic anhydride and permanganate treatment. Those methods and ways of carrying out of surface modifications were not studied before on kenaf/thermoplastic polyurethane composites. Different fibre...
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Tuning the extraction properties of ionogel-coated Solid-phase microextraction fibers based on the solvation properties of the ionic liquids
PublicationA silica-based network was used to immobilize ionic liquid-based ionogels and applied as a fiber coating forsolid-phase microextraction (SPME). The ionogels were prepared by a sol–gel process, using two ionic liquids,triethylsulfonium bis(trifluoromethylsulfonyl)imide ([Set3][TFSI]) and 1-butyl-1-methylpiperidinium bis(tri-fluoromethylsulfonyl)imide ([C4C1Pip][TFSI]), as well as their equimolar mixture. Methyltrimethoxysilane wasused...
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Autogenous Fiber Laser Welding of 316L Austenitic and 2304 Lean Duplex Stainless Steels
PublicationThis study presents results of experimental tests on quality of dissimilar welded joints between 316L austenitic and 2304 lean duplex stainless steels, welded without ceramic backing. Fiber laser welded butt joints at a thickness of 8 mm were subjected to non‐destructive testing (visual and penetrant), destructive testing (static tensile test, bending test, and microhardness measurements) and structure observations (macro‐ and...
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Electrochemical oxidation of PFOA and PFOS in landfill leachates at low and highly boron-doped diamond electrodes
PublicationPolyfluorinated alkyl substances (PFASs) may reach landfill leachates (LLs) due to improper waste management. In this study perfluorooctanoate (PFOA) and perfluorooctane sulphonate (PFOS) were used as representatives of PFASs in the decomposition on boron-doped diamond electrodes (BDDs) with high (10k ppm) and low (0.5k ppm) boron doping concentrations. The result shows that although better COD removal efficacies are obtained on...
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Conductive printable electrodes tuned by boron-doped nanodiamond foil additives for nitroexplosive detection
PublicationAn efficient additive manufacturing-based composite material fabrication for electrochemical applications is reported. The composite is composed of commercially available graphene-doped polylactide acid (G-PLA) 3D printouts and surface- functionalized with nanocrystalline boron-doped diamond foil (NDF) additives. The NDFs were synthesized on a tantalum substrate and transferred to the 3D-printout surface at 200 °C. No other electrode...
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Investigation of the Efficiency of a Dual-Fuel Gas Turbine Combustion Chamber with a Plasma‒Chemical Element
PublicationThe study is devoted to the possibility of increasing the efficiency of the working process in dual-fuel combustion chambers of gas turbine engines for FPSO vessels. For the first time, it is proposed to use the advantages of plasma‒chemical intensification of the combustion of hydrocarbon fuels in the dual-fuel combustion chambers, which can simultaneously operate on gaseous and liquid fuels. A design scheme of a combustion chamber...
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Fabrication of the cross-linked PVA/TiO2/C nanocomposite membrane for alkaline direct methanol fuel cells
PublicationA crosslinked Poly(vinyl alcohol) based composite membrane was developed through a phase inversion process for use in alkaline direct methanol fuel cells (ADMFCs). The titanium dioxide (TiO2) and carbon nanoparticles (NPs) have been incorporated into the PVA polymer matrix to improve the mechanical and thermal properties. The membrane samples were further modified with maleic acid, a carboxylic acid acting as the cross-linker,...
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Theoretical and experimental analysis of guided wave propagation in plate-like structures with sinusoidal thickness variations
PublicationGuided waves have attracted significant attention for non-destructive testing (NDT) and structural health monitoring (SHM) due to their ability to travel relatively long distances without significant energy loss combined with their sensitivity to even small defects. Therefore, they are commonly used in damage detection and localization applications. The main idea of incorporating guided waves in NDT and SHM is based on processing...
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Solar light driven degradation of textile dye contaminants for wastewater treatment – studies of novel polycationic selenide photocatalyst and process optimization by response surface methodology desirability factor
PublicationThe unplanned anthropogenic activities and raced industrial revolution detrimentally causes serious threat to terrestrial and aquatic life. A high discharge of wastewater from industries using dyes affects living organisms and the environment. This paper presents studies on polycationic selenides (PCS) synthesized by hydrothermal methods for photocatalytic degradation of dyes. The synthesized PCS were confirmed by various characterization...
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The Impact of the Antigenic Composition of Chimeric Proteins on Their Immunoprotective Activity against Chronic Toxoplasmosis in Mice
PublicationToxoplasmosis may pose a serious threat for individuals with weakened or undeveloped immune systems. However, to date, there is no specific immunoprophylaxis for humans. Thus, the aim of this study was to evaluate the immunogenicity of three trivalent—SAG2-GRA1-ROP1L (SGR), SAG1L-MIC1-MAG1 (SMM), and GRA1-GRA2-GRA6 (GGG)—and two tetravalent—SAG2-GRA1-ROP1-GRA2 (SGRG) and SAG1-MIC1-MAG1-GRA2 (SMMG)—chimeric T. gondii proteins, as...
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A facile approach to fabricate load-bearing porous polymer scaffolds for bone tissue engineering
PublicationBiodegradable porous scaffolds with oriented interconnected pores and high mechanical are load-bearing biomaterials for bone tissue engineering. Herein, we report a simple, non-toxic, and cost-effective method to fabricate high-strength porous biodegradable scaffolds, composed of a polymer matrix of polycaprolactone (PCL) and water-soluble poly (ethylene oxide) (PEO) as a sacrificial material by integrating annealing treatment,...
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GTR/Thermoplastics Blends: How Do Interfacial Interactions Govern Processing and Physico-Mechanical Properties?
PublicationIn this work, GTR/thermoplastics blends (in ratio 50/50 and 75/25 wt.%) were prepared by melt-compounding in an internal mixer. During research, trans-polyoctenamer rubber (TOR), ethylene-vinyl acetate copolymer (EVA), ethylene-octene copolymer (EOC), and linear low-density polyethylene (LLDPE), were used in their thermoplastic phase. Microstructure and processing-performance property interrelationships of the studied materials...
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Ionic liquids-based microextraction techniques
PublicationIn recent years, the development of highly efficient analytical techniques is of great importance, however, the direct analysis of complex sample matrix is still impossible in many cases. Therefore, the step of sample preparation is commonly involved in an analytical procedure. Over the years, it has been realized that the major source of inaccuracy and imprecision on general analysis results from the operations associated to sample...
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A multi-analytical approach to the characterization of natural organic dyestuffs and inorganic substrates present in the 19th-century artistic oil paints manufactured by a French art materials supplier Richard Aines
PublicationThis paper presents a comprehensive analysis of artistic paints produced in the 19th century by a French art materials supplier Richard Ain`es. Improved mild extraction with hydrofluoric acid enabled the observation of intact organic dyes. Reversed-phase liquid chromatography with diode-array and mass spectrometry detection was utilised for the identification of 35 dyes present in yellow and red paint samples, and in selected plant...
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Multi-Technique Investigation of Grave Robes from 17th and 18th Century Crypts Using Combined Spectroscopic, Spectrometric Techniques, and New-Generation Sequencing
PublicationThe textile fragments of the funeral clothes found in the 17th and 18th century crypts were subjected to spectroscopic, spectrometric, and microbial investigation. The next-generation sequencing enabled DNA identification of microorganisms at the genus and in five cases to the species level. The soft hydrofluoric acid extraction method was optimized to isolate different classes of dyes from samples that had direct contact with...
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BEZCZUJNIKOWE STEROWANIE WOLNOOBROTOWYM SILNIKIEM PMSM Z KOMPENSACJĄ MOMENTU ZACZEPOWEGO
PublicationW pracy przedstawiono propozycję rozwiązania problemu bezczujnikowego sterowania wolnoobrotową maszyną synchroniczną z magnesami trwałymi PMSM. Przedstawiono silnik PMSM, który zastosowano w stanowisku badawczym. Omówiono problem występowania tętnień momentu napędowego wynikający głównie ze znacznego momentu zaczepowego. Pokazano rozwiązanie kompensujące tętnienia momentu napędowego w silniku PMSM. Przygotowano procedurę startową...
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Selectivity of amperometric gas sensors in multicomponent gas mixtures
PublicationIn recent years smog and poor air quality became a growing environmental problem. There is a need to continuously monitor the quality of air. The lack of selectivity is one of the most important problems limiting the use of gas sensors for this purpose. In this study, a selectivity of the six amperometric gas sensors is being investigated. Calibration of sensors has been performed in order to find a correlation between concentration...
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Electrical and structural properties of Nb-doped SrTiO3
PublicationNiobium-doped strontium titanate synthesized via conventional solid-state reaction has been studied. Influence of niobium content on the lattice parameters and electrical conductivity has been reported. Various reduction conditions have been investigated. For samples reduced in hydrogen at 1400°C, a transition from thermally activated to metallic behavior has been observed. Maximum electrical conductivity (ca. 55 Scm−1 at 650°C)...
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BADANIA KOMPOZYTOWEGO MOSTU DLA PIESZYCH
PublicationThe paper presents in situ load testing of the innovative footbridge of FOBRIDGE grant mounted at Gdansk University of Technology. The span of composite sandwich structure (GFRP skins, PET core) and the scope of static and dynamic tests are presented. The selected, representative results of in situ measurements and data obtained from the SHM monitoring system are discussed. Besides the standard testing procedures on the full scale...
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Impedance Studies of Phosphate-iron Glasses Containing Niobium and Titanium
PublicationThe ac and dc conductivity in phosphate-iron-niobate glasses with addition of titanium oxide was investigated as a function of temperature and frequency with the use of impedance spectroscopy. The topography and microstructure of glasses were investigated by the means of X-ray diffraction (XRD), scanning electron microscopy (SEM), and confocal microscopy methods. The obtained results show that all samples are amorphous but they...
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Polarization interferometer using a Liquid Crystalline Polymer waveplate for wavelength measurement
PublicationA two-beam polarization interferometer for measuring wavelength changes of a tunable semiconductor laser was designed, built and tested. This interferometer uses a λ/8 waveplate made from Liquid Crystalline Polymer in order to generate two output signals in quadrature. The λ/8 waveplate can be manufactured either on a beamsplitter face or on the mirror surface, reducing the cost and complexity of the optomechnical assembly. Experiment...
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Wykorzystanie wymiennych kart pamięci Flash w mikroprocesorowych rejestratorach danych pomiarowych
PublicationW artykule przedstawiono możliwość wykorzystania kart pamięci Flash w mikroprocesorowych urządzeniach rejestracji danych pomiarowych. Dokonano przeglądu najpopularniejszych kart oraz omówiono ich właści-wości. Na przykładzie kart MMC i SD opisano sposób odczytu i zapisu danych przy wykorzystaniu interfejsu SPI. Rozważono różne struktury zapisu danych. W oparciu o wykonany prototyp rejestratora oszacowano zapotrzebowanie na zasoby...
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Kant i kantyzmy : o okresach i sposobach obecnosci Kanta w filozofii
PublicationArtykuł omawia pięć etapów obecności Kanta w filozofii:1) wczesny kantyzm, gdzie obraz filozofi Kanta nie był jeszcze zamkniety.2)idealizm niemiecki, gdzie Kant staje się sam ogniwem jako rozwój.3) etap neokamntyzmu, redukują Kanta do teorii poznania i filozogii krytycznej.4) etap ontologicznej i metafizycznej interpretacji Kanta.5) etap współczesny: rewidujący wiele fałszywych opini o historycznym Kancie i okreslany przez wielkość...
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Funcionality assessment of Citrus Hysteria peel as a protective barrier using gas chromatography
PublicationThe aim of this study was to analyse the volatile fractions of fruit peel and pulp using two-dimensional gas chromatography technique coupled with mass spectrometry. The isolation of the compounds was achieved by microextraction to the stationary phase from the headspace of the sample (HS-SPME). Mass spectrometry with time-of-flight analyser (TOF-MS) was used to identify the chemical compounds. There are no reports in the literature...
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Phase Separation and Electrical Properties of Manganese Borosilicate Glasses
PublicationThe structure and electrical properties of manganese borosilicate glasses of a composition of xMnO-(0.8-x)SiO2-(0.2)B2O3 (x=0.4, 0.5 and 0.6 in mol) were investigated by impedance spectroscopy, SEM, XRD and confocal microscopy methods. The influence of composition on the glass structure and electrical properties was discussed. A separation of two amorphous phases was observed and it was concluded that one phase is SiO2-rich and...
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PRZEDELĄD HAŁAŚLIWOŚCI NAWIERZCHNI DROGOWYCH W POLSCE I W INNYCH KRAJACH UNII EUROPEJSKIEJ
PublicationW pracy przedstawiono szczegółowo dwiemetody badania hałaśliwości nawierzchni drogowych (SPB i CPX) i zaprezentowano wyniki pomiarów przeprowadzonych metodą CPX na nawierzchniach drogowych na przestrzeni ostatnich 14 lat. Pomiary przeprowadzono na 154 odcinkach zlokalizowanych na terenie Polski oraz na 419 odcinkach na terenie innych państw europejskich. Dokonano oceny hałaśliwości warstw scieralnych występujących w naszym kraju...
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Simultaneous detrmination of selected phenoxyacid herbicides and chlorophenols in surface and seawater by HPLC coupled to DAD.
PublicationDo badań wykorzystano metodę ekstrakcji do fazy stałej (SPE) w celu wzbogacenia analitów. Ekstrakty analizowano techniką wysokosprawnej chromatografii cieczowej (HPLC) z detekcją DAD. Opracowana metoda umożliwia oznaczenie 14 związków z grupy kwasów fenoksyoctowych i chlorofenoli w czasie 22 min. Odzysk analitów wynosił powyżej 60% dla fenoksykwasów i powyżej 70% w przypadku chlorofenoli. Granica oznaczalności dla oznaczania...
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Propozycja zagospodarowania osadów ściekowych z Gdańskiej Oczyszczalni Ścieków ''Wschód'.
PublicationPrzedstawiono możliwości zagospodarowania osadów ściekowych z oczyszczalni ''Wschód'' w Gdańsku. Po analizie dopuszczalnych rozwiązań: składowania, nawożenia gleb i rekultywacjiobszarów poprzemysłowych - najbardziej przyszłościowe wydaje się współpalanie suchych osadów z węglem w miejskiej elektrociepłowni. Oczyszczalnia produkuje ok. 22 t s.m. osadów dziennie. Do suszenia może być wykorzystana para odpadowa Rafinerii Gdańskiej,...
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Reduction of vibration level by the spindle speed optimisation during ball end milling of flexible details
PublicationPraca dotyczy nadzorowania drgań podczas skrawania przedmiotów podatnych frezem kulistym. Przedsatwiono wspomaganą komputerowo procedurę nadzorowania z optymalizacją prędkości obrotowej narzędzia. Przy modelowaniu wykorzystano niestacjonarny model obliczeniowy. Rezultatem modelowania jest układ hybrydowy, w którym oddzielono podukłady: modalny, łączący i strukturalny. Metoda wymaga identyfikacji częstości własnych co może być wykonane...
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Fermentacja metanowa kapusty białej oraz osadu nadmiernego
PublicationW pracy przedstawiono wyniki badań fermentacji metanowej biomasy kapusty białej i osadu nadmiernego pobranego z oczyszczalni ścieków Saur Neptun Gdańsk S.A. Proces fermentacji prowadzono w warunkach mokrych, w sposób quaziciągły, w temperaturze 37°C. Zaobserwowano, że poddając fermentacji beztlenowej wsad zawierający kapustę białą oraz osad nadmierny można uzyskać biogaz o średnim składzie 50% metanu i 50% ditlenku węgla. Podczas...
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Software tool for modelling of mechatronic systems with elastic continua
PublicationThe paper presents a systematic computational package for modelling and analysis of complex systems composed of multiple lumped and distributed parameter subsystems. The constructed computer program enables the frequency domain analysis of a class of linear systems and to obtain reduced order model in the form of bond graph. Obtained modal bond graph can be directly exported into 20-Sim package to further processing including nonlinear...
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Microstructure and Dielectric Properties of Barium-vanadate Glasses
PublicationThe ac and dc conductivity in barium-vanadate glasses was investigated as a function of temperature and frequency with the use of impedance spectroscopy. The topography and microstructure of glasses were investigated by the means of X-ray diffraction (XRD) and scanning electron microscopy (SEM) methods. The XRD results show that all samples are amorphous but microscopy investigation reveals that glasses with greater amount of V2O5...
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Sequential induction of mitotic catastrophe followed by apoptosis in human leukemia MOLT4 cells by imidazoacridinone C-1311
PublicationWykazano, że pochodna imidazoakrydonu C-1311 indukuje zahamowanie progresji komórek MOLT4 w fazie G2M cyklu życiowego. Podwyższona ekspresja fosfoepitopu MPM-2 przy jednoczesnym zaniku ufosforylowanej formy Tyr15-cdc2 wskazywała, iż komórki początkowo zablokowane w fazie G2 przechodziły do mitozy. Jednocześnie na skutek nieprawidłowego przebiegu mitozy komórki ulegały katastrofie mitotycznej. Analiza biochenicznych markerów apoptozy...
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Solid phase microextraction combined with chromatography - a powerful tool for determination of warfare agents and related compounds
PublicationOpisano zastosowanie mikroekstrakcji do fazy stacjonarnej do izolacji wzbogacania środków bojowych i produktów ich degradacji w powietrzu, wodzie i glebie oraz próbkach bilogicznych. Na etapie oznaczeń końcowych stosuje się najczęściej chromatografię gazową. Anality można pobierać przez bezpośrednie zanurzenie włókna w próbce ciekłej i gazowej oraz w fazie nadpowierzchniowej. Stosując SPME-GC można osiągnąć niskie granice oznaczalności...
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The project IDENT: Multimodal biometric system for bank client identity verification
PublicationBiometric identity verification methods are implemented inside a real banking environment comprising: dynamic handwritten signature verification, face recognition, bank cli-ent voice recognition and hand vein distribution verification. A secure communication system based on an intra-bank client-server architecture was designed for this purpose. Hitherto achieved progress within the project is reported in this paper with a focus...
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The influence of rubber recyclate morphology on the properties of rubber-asphalt composite
PublicationIn the paper wastes, mostly in the form of used tires, were analyzed. One of the methods of waste tires application use them as a modifier of asphalt. However, the properties of rubber-asphalt composites depend on the morphology of waste tiregranulate and kind of tire recycled (car/truck). In this chapter, the influence of grinding methods of waste tire on the prop¬erties of rubber-asphalt composites were studied. SEM analysis...
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Dynamics of Ice Jam Formation and Release
PublicationThe numerical model DynaRICE and its application to ice jam formation and release is presented. The model is a two-dimensional coupled flow and ice dynamic model. The ice dynamic component, which includes both the internal ice resistance and boundary friction on ice motion, uses a Lagrangian SPH method. The hydrodynamic component of the model uses a streamline upwind finite element method, which is capable of simulating trans-critical...
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Electrochemical oxidation of sulphamerazine at boron-doped diamond electrodes: Influence of boron concentration
PublicationThe boron-doped diamond (BDD) electrodes with different boron concentrations have been tested as electrode material for sulphamerazine (SRM) oxidation in water solution. An investigation of the electrode morphology and molecular structure was carried out using high resolution scanning electron microscopy (SEM) and Raman spectroscopy. Electrochemical results showed clearly that the kinetics and efficiency of SRM oxidation were dependent...
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Application of Headspace Solid-phase Microextraction with Poly(1-vinyl-3- Hexylimidazolium Chloride) Polymeric Ionic Liquid Coating using GC - MS to Determine Volatile Fatty Acids in Dairy Wastewater
PublicationVolatile fatty acids were determined in this study using headspace solid-phase microextraction (HS-SPME) with a poly(1-vinyl-3-hexylimidazolium chloride) polymeric ionic liquid coated fiber followed by gas chromatography - mass spectrometry. Experimental parameters such as extraction time and temperature, sample volume as well as desorption time and temperature were optimized. Detection limits of the method were in the range of...
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Stress analysis of suspended rail vehicle bogie
PublicationNiniejsza publikacja została poświęcona analizie wytrzymałościowej wybranych elementów wózka – osi zestawu kołowego i ramy. Obliczenia osi wykonano w oparciu o metodę analityczną przy rozpatrzeniu różnych materiałów jej wykonania. Do sprawdzenia wytrzymałości ramy wykorzystano metodę elementów skończonych, a obciążenie wyznaczono zgodnie z wytycznymi normy PN-EN 13749. Sam wózek jest częścią podwieszanego elektrycznego zespołu...
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Subiektywny pomiar jakości programów radiowych strumieniowanych w sieci metodą crowdsourcingu
PublicationObecnie słuchacze mają dostęp do swoich ulubionych programów i audycji radiowych za pośrednictwem naziemnego standardu analogowego FM (Frequency Modulation) oraz cyfrowego DAB+ (Digital Audio Broadcasting plus). Należy podkreślić, że ten sam materiał nadawany jest jednocześnie w kilku technikach (tzw. simulcast), a znaczna większość rozgłośni udostępnia swoje programy także online. Niniejsza praca przedstawia wyniki badań dotyczących...
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Pre-oxidation of porous ferritic Fe22Cr alloys for lifespan extension at high-temperature
PublicationPre-oxidation of porous ferritic Fe22Cr alloys was extensively studied in this paper. Weight gain measurements and SEM analysis revealed that pre-oxidation performed at 900◦C for 40 min increased the lifespan of the alloy. A Cr evaporation study did not disclose any significant influence of the pre-oxidation process on the Cr content in the alloy. For a more detailed assessment, TEM imaging and X-ray tomography measurements of...
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Fabrication, structural and electrical properties of Sr(V,Nb)O 3-δ perovskite materials
PublicationThe SrV1-xNbxO3-δ materials with different niobium content in perovskite B-sublattice were prepared by a solid-state reaction process. The microstructure and phase compositions of obtained samples were analyzed by the X-ray diffraction technique (XRD) and scanning electron microscopy (SEM). The electrical conductivity of samples was measured by a DC 4-wire method in range of 100–600 °C in different gas conditions. The oxidation...
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Modeling DAC Application Execution Time
PublicationAn application written in the Divide And Conquer paradigm is more difficult to model than SPMD application because of complex algorithm, causing use of many coefficients in a computational complexity function. Processors are divided into various layers, each layer contains different number of processors. Data packets processed in different layers and transferred between layers have different length. Moreover first layer processors use...
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Dynamic Response of the Suspended on a Single Cable Footbridge
PublicationThe article presents numerical simulations, dynamic in situ load tests and a structural health monitoring (SHM) system installed in a suspended on a single cable footbridge. Numerical simulations performed prior to construction indicated the possibility of structural dynamics problems, finally confirmed in the course of dynamic test loading. In the dynamic load course the bridge deck developed vibrations displaying accelerations...
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Sterowanie przekształtnikiem sieciowym z funkcją filtru aktywnego bez pomiaru napięcia sieci.
PublicationW artykule przedstawiono strukturę oraz wyniki badań symulacyjnych układu sterowania trójfazowym, tranzystorowym przekształtnikiem sieciowym pośredniego przemiennika częstotliwości. Układ zapewnia kompensację odkształceń prądów zasilających powodowanych przez równolegle przyłączone do sieci odbiory nieliniowe. Dzięki zastosowaniu zmodyfikowanego regulatora prądu z predykcją SEM układ pracuje bez pomiaru napięcia sieci. Zapewniona...
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Implementacja zmodyfikowanej metody biliniowej 2D w elektronicznym systemie wbudowanym
PublicationPrzedstawiono implementację zmodyfikowanej metody biliniowej 2D diagnostyki sieci analogowych we wbudowanych mikrosystemach mieszanych sygnałowo sterowanych mikrokontrolerami. Metoda cechuje się prostym algorytmem diagnostycznym, który z powodzeniem można zaimplementować w 8-bitowych, powszechnie stosowanych mikrokontrolerach z interfejsem SPI, oraz nie wymaga nadmiernej rozbudowy mikrosystemu o część testującą (BIST). Zaletą metody...
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Simultaneous Determination of Indolic Compounds in Plant Extracts by Solid-Phase Extraction and High-Performance Liquid Chromatography with UV and Fluorescence Detection
PublicationA high-performance liquid chromatographic method with UV and fluorescence detection (HPLC-DAD-FLD) was developed for simultaneous determination of indolic compounds in plant material. Indole-3-carbinol (I3C), indole-3-acetic acid (I3AA), indole-3-acetonitrile (I3ACN), and 3,3′-diindolylmethane (DIM) were used as representative compounds that cover a wide spectrum of indole structures occurring in nature. For concentration and purification...