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Search results for: TRI-LAYER ELECTROLYTE
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Fabrication and properties of electrode material composed of ordered titania nanotubes and pEDOT:PSS
PublicationWe report on the two-stage preparation method of electrode material composed of titania nanotubes and poly(3,4-ethylenedioxythiopene):poly(2-styrenesulphonate) conductive polymer (pEDOT:PSS). Initially, titania nanotube arrays were produced by the anodization process of Ti substrate. Next, the polymer was potentiostatically deposited onto the thermally annealed nanotube arrays from the electrolyte containing monomer and counter...
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Electrical power measurement of LSCNT modified SOFC fueled by biogas mixture at 750 C
Open Research DataThe dataset contains the electrical measurements of IV curves for SOFC with La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s layer working under biogas and H2 feeding stream. The SOFC was reduced at 900C and conditioned for 12 h under H2 prior the measurements. The measurements were performed using Gamry potentiostat/galvanostat
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Characterization of structural, thermal and mechanical properties of bismuth silicate glasses
Publicationhe influence of heating and reduction processes on the structural, thermal and mechanical properties of bismuth-silicate glasses has been investigated. Two compositions of glasses: 40Bi2O3–60SiO2 (Bi0.57Si0.43Ox) and 27Bi2O3–73SiO2 (Bi0.43Si0.57Ox) were fabricated by a typical melt quenching technique. Then the reduction in hydrogen at 380 °C for 20, 42 or 67 h was performed. It was found that a 50 μm-thick layer was formed on...
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Fiber optic low-coherence Fabry-Pérot interferometer with ZnO layers in transmission and reflective mode: comparative study
PublicationA construction of a low-coherence fiber-optic Fabry-Pérot interferometer using a thin ZnO layer as a reflective surfaces was proposed and examined. In the investigated setup, the ZnO layer of thickness 200 nm were deposited on the face of the standard telecommunication single-mode optical fiber (SMF-28). Measurements of interference signal were performed for the interferometer working in the transmission and reflective mode, as...
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New plasmonic platform for enhanced luminescence of Valrubicin
PublicationLuminescence enhanced by new structure of plasmonic platform with aluminum oxide (Al2O3) buffer layer deposited on gold nanostructures is investigated. Regularly distributed gold nanostructures of average dimension of 50 nm formed the active part of plasmonic platforms. They were manufactured on Corning 1737 glass substrate by melting of gold thin film. The nanostructures were coated by dielectric Al2O3 thin film with thickness...
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Nested Space Mapping Technology for Expedite EM-driven Design of Compact RF/microwave Components
PublicationA robust simulation-driven methodology for rapid and reliable design of RF/microwave circuits comprising compact microstrip resonant cells (CMRCs) is presented. We introduce a nested space mapping (NSM) technology, in which the inner space mapping layer is utilized to improve the generalization capabilities of the equivalent circuit model corresponding to a constitutive element of the circuit under consideration. The outer layer...
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Monitoring the curing process of epoxy adhesive using ultrasound and Lamb wave dispersion curves
PublicationMonitoring the stiffness of adhesives is a crucial issue when considering the durability andstrength of adhesive joints. While there are many studies conducted on specimens madeonly from adhesive, the problem of curing of an adhesive film in real joints is moderatelyconsidered. This paper presents the monitoring of stiffening of epoxy adhesive using ultra-sound. Ultrasonic pulse velocity method was firstly applied for monitoring...
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Electrical power measurement of reference SOFC fueled by biogas mixture at 750 C
Open Research DataThe dataset contains the electrical measurements of IV curves for SOFC without La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s layer working under biogas and H2 feeding stream. The SOFC was reduced at 900C and conditioned for 12 h under H2 prior the measurements. The measurements were performed using Gamry potentiostat/galvanostat
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Ultra-thin film of aluminum oxide influence on the plasmon resonance in gold nanostructures
Open Research DataUltra-thin film of aluminum oxide influence on the plasmon resonance in gold nanostructures was measured by UV-VIS spectroscopy. Ultra thin film of Al2O3 was deposited on a gold nanostructures. Thickness of film was 2nm - 8nm. Shift of plasmon resonance was observed, as a result of various dielectric constant of layer.
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Implementation of Hierarchical Control of Drinking Water Supply System
PublicationThe paper presents the outline of the didactical project of a complex computer controlled system realized by the first degree students of the Automatics and Robotics on the Faculty of Electrical and Control Engineering (FoEaCE) in Gdansk University of Technology (GUT). The synthesis, implementation and analysis of a multilayer hierarchical control system for drinking water supply system (DWSS) are main topics of that project. The...
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Incorporating Iris, Fingerprint and Face Biometric for Fraud Prevention in e-Passports Using Fuzzy Vault
PublicationA unified frame work which provides a higher security level to e-passports is proposed. This framework integrates face, iris and fingerprint images. It involves three layers of security: the first layer maps a biometric image to another biometric image which is called biostego image. Three mapping schemes are proposed: the first scheme maps single biometric image to single biostego image, the second scheme maps dual biometric images...
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Insightful studies of AuCu nanostructures deposited on Ti platform: Effect of rapid thermal annealing on photoelectrochemical activity supported by synchrotron radiation studies
PublicationIn this work, we present the influence of annealing atmospheres during rapid thermal annealing (40◦C/s) on nanostructured Ti platforms modified by 10 nm layer of AuCu alloy obtained via magnetron sputtering. The AuCu/Ti platform annealed under hydrogen atmosphere exhibits the best photoelectrochemical activity under visible light, i.e. 27 times higher photocurrent than for pure Ti dimpled platform, and the lowest reflectance with minimum...
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Generalized access control in hierarchical computer network
PublicationThe paper presents the design of the security layer for a distributed system located in the multizone hierarchical computer network. Depending on the zone from which a client’s request comes to the system and the type of the request, it will be either authorized or rejected. There is one common layer for the access to all the business services and interactions between them. Unlike the commonly used RBAC model, this system enforces...
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High temperature corrosion of evaporator tubes with thermal sprayed coatings
PublicationDegradation examinations of outer surface of low-emission steam boiler evaporator tubes are presented in the paper. Metallographic evaluation of scale morphology, its micro sites chemical composition analysis and distribution of elements on cross sections have been performed. Water-wall tubes were exposed in steam boiler for up to two years period. Common tubes made of 16Mo3 steel suffered sulphide and molten salts corrosions....
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Performance improvement of NN based RTLS by customization of NN structure - heuristic approach
PublicationThe purpose of this research is to improve performance of the Hybrid Scene Analysis – Neural Network indoor localization algorithm applied in Real-time Locating System, RTLS. A properly customized structure of Neural Network and training algorithms for specific operating environment will enhance the system’s performance in terms of localization accuracy and precision. Due to nonlinearity and model complexity, a heuristic analysis...
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Evidence for solid state electrochemical degradation within a small molecule OLED
PublicationAcridone derivative have been synthesised and used as OLED (Organic Light Emitting Diode) emitters which were found to be electroactive. Electrochemical investigations showed a side reaction takes place inside an active layer which diminished the overall device efficiency. By using a dopant and host active layer architecture, the formation of the by product was removed. The by-product was identified as a σ-dimer formed inside an...
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Numerical Modeling of Cone Penetration Test in Slightly Overconsolidated Clay with Arbitrary Lagrangian-Eulerian Formulation
PublicationIn this paper the results of the cone penetration test (CPT) modeling with the arbitrary Lagrangian-Eulerian (ALE) formulation provided by Abaqus software package have been presented. The study compares the cone resistance and sleeve friction obtained in numerical analysis with values measured in soundings performed in the uniform layer of clayey soil in the Koszalin area. The clay layer was found to be slightly overconsolidated...
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Detection of petroleum products using optical coherence tomography
PublicationIn this work, we present a novel method developed for the analysis of the properties of thin layers for detecting petroleum products on a water surface using a commercially available optical coherence tomography (OCT) system. The spectral density analysis of the signal from a spectroscopic OCT (S-OCT) enables us to perform the precision calculation of the thin layer thickness and other properties like homogeneity, and dispersion,...
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Changes in conditions of acoustic wave propagation in the Gdansk deep as an effect of climate changes in the Baltic Sea region
PublicationThe article presents the results from a research project investigating acoustic climate changes in the Gdansk Deep based on data extending from 1902 to 2019. This part of the southern Gotland Basin, is rarely discussed in the scientific literature. The speed of sound in the seawater is a function of temperature, salinity, and depth. In such shallow sea as Baltic Sea, the impact of depth is not substantial. The other two factors...
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Intraductal papilloma - Female, 69 - Tissue image [7260729594499541]
Open Research DataThis is the histopathological image of BREAST tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Nanoindentation tests of the hydroxyapatite composite coatings applicated on titanium alloys by the electrophoretic method
Open Research DataCurrently, there are no metal materials that meet all biomechanical and biochemical requirements needed for long life implantable biomaterials. The main purpose of the study was to functionalize the surface of the titanium alloys used in biomaterial implants.
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Formation of gold anostructures detected by SEM microscope
Open Research DataGold nanostructures were prepared on silicon - Si(111) as a substrate. The substrates (1 × 1 cm2 of area) were cleaned with acetylacetone and then rinsed in ethanol. Thin Au films (with thicknesses in a range of 1.7–5.0 nm) were deposited using a table-top dc magnetron sputtering coater (EM SCD 500, Leica) under pure Ar plasma conditions (Argon, Air...
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Scanning electron microscopy (SEM) images of the boron-dopied diamond surfaces
Open Research DataThe dataset contains the scanning electron micrographs (SEM), revealing the surface morphology of diamond electrodes on different substrates. The diamond surface is characterized by an aggregation of crystals that do not form a continuous layer.
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Nanotubular Ti Oxide Layers for Enhancement of Bone-Implant Bonding and Bioactivity
PublicationAbstrakt artykułu pt. ''Nanotubular Ti Oxide Layers for Enhancement of Bone-Implant Bonding and Bioactivity''. The paper describes techniques to improve the bioactivity of titanium and ehnahnce the bone-implant bonding ability by the electrochemical anodization to fabricate titania nanotubular oxide layer.
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Entrepreneurship nests in a polish edge city
PublicationThe last two decades in Poland have been a period of both a dynamic development of the small and medium-sized enterprise sector and a transformation of the city surrounding territories. This development began during the economy transformation after 1989. Population migration and movement of economic entities away from central cities resulted in development of territorial structures within some Polish suburban areas, defined as...
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Shear band evolution phenomena in direct shear test modelled with DEM.
PublicationA direct shear test is widely used in the geotechnical engineering field. It is an easy and quick test to measure the shear properties of soil. This test often replaces more expensive and difficult tri-axial shear test. Despite that the direct shear test is known and used for a long time, it is still not well investigated at the grain scale. This paper deals with the micro behaviour of the cohesionless sand inside the direct shear...
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Analiza strukturalna silanotiolanów : wpływ centrów kwasowych na zmiany w układzie wiązań SI-O-C oraz SI-S grupy sialkoksysilanotiolanowej w ciele stałym / J. Chojnacki.
PublicationW pracy przedstawiono wyniki badań strukturalnych silanotiolanów metali. Wyniki pochodzące z rentgenowskiej analizy strukturalnej zostały zinterpretowane w oparciu o rezultaty obliczeń kwantowo-mechanicznych. Wyznaczono 46 nowych struktur rentgenowskich silanotiolanów i przeanalizowano je łącznie z wynikami badań strukturalnych innych autorów. Zebrano i usystematyzowano wyniki rentgenowskiej analizy strukturalnej dla wszystkich...
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Numerical simulation of laminate composite specimens failure
PublicationThis work presents some numerical results concerning simulation of failure of laminate composite specimens. In the article two tests to determine ultimate strength in an orthotropic layer, are considered: tension (TT1) and compression (TC1) test. The outcome is compared with experimental data provided by [9,10].
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Artificial neural network prophecy of ion exchange process for Cu (II) eradication from acid mine drainage
PublicationThe removal of heavy metal ions from wastewater was found to be significant when the cation exchange procedure was used effectively. The model of the cation exchange process was built using an artificial neural network (ANN). The acid mine drainage waste’s Cu(II) ion was removed using Indion 730 cation exchange resin. Experimental data from 252 cycles were recorded. In a column study, 252 experimental observations validated the...
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Elektrochemiczny czujnik na bazie cieczy jonowej do oznaczania par benzaldehydu
PublicationW pracy przedstawiono prototypowy, laboratoryjny, elektrochemiczny czujnik do oznaczania par benzaldehydu w argonie. Cieczą jonową testowaną jako elektrolit i środowisko reakcji redox była: bis(trifluorometylosulfonylo)imidek 1-butylo,3-metyloimidazolinowy ([BMIM][Tf2N]). W pomiarach użyto komercyjnych elektrod firm: DropSens Co. i BVT Technologies. Walidacji poddano dwa parametry metrologiczne czujnika: granicę wykrywalności i...
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Influence of the ionic strength on the amyloid fibrillogenesis of hen egg white lysozyme
PublicationThe study investigates the role of the electrostatic interactions in the fibrillation of the hen egg white lysozyme (HEWL). In order to achieve this aim the influence of the cations Na+, Mg2+ and Al3+ on the amyloid fibril formation and amorphous aggregation was tested. The amyloids are formed in the solution without added salt but the Thioflavin T fluorescence gives the false-negative result. In these conditions, the HEWL fibrils...
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Enhanced Electrochemical Performance of MnCo1.5Fe0.5O4Spinel for Oxygen Evolution Reaction through Heat Treatment
PublicationMnCo1.5Fe0.5O4 spinel oxide was synthesized using the sol−gel technique, followed by heat treatment at various temperatures (400, 600, 800, and 1000 °C). The prepared materials were examined as anode electrocatalysts for watersplitting systems in alkaline environments. Solid-state characterization methods, such as powder X-ray diffraction and X-ray absorption spectroscopy (XAS), were used to analyze the materials’ crystallographic...
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The effect of morphology and crystalline structure of Mo/MoO3 layers on photocatalytic degradation of water organic pollutants
PublicationMolybdenum oxide layers were formed by anodization of the Mo metallic foil in a water/ethylene glycol-based electrolyte containing fluoride ions. The as-prepared, amorphous samples were annealed in air at different temperatures in a range from 100 �C to 700 �C. The crystal phase and morphology of anodized and annealed MoO3 layers were investigated using X-ray diffraction, Raman spectroscopy, and scanning electron microscopy. The...
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Optical sensor of a person sitting on a chair and dressed in multi-layered clothes vital signs monitoring
PublicationAn optoelectronic device enhancing a smart chair functionality is presented in the paper. Its essential purpose is a detection of a sitting person presence on the chair by means of detecting the vital signs. Additionally, it could be used for determining of clothes layer parameters useful in adjusting a system of a capacitive electrocardiography.
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Multi-instrument analysis of L-band amplitude scintillation observed over the Eastern Arabian Peninsula
PublicationThe study of scintillation-causing ionospheric irregularities is important to mitigate their effects on satellite communications. It is also important due to the spatial and temporal variability of these irregularities, given that their characteristics differ from one region to another. This study investigates the spatial and temporal characteristics of L1 amplitude scintillation-causing ionospheric irregularities over the Eastern...
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Changes in conditions of acoustic wave propagation in the Gdansk deep as an effect of climate changes in the Baltic Sea region
PublicationThe article presents the results from a research project investigating acoustic climate changes in the Gdansk Deepbased on data extending from 1902 to 2019. This part of the southern Gotland Basin, is rarely discussed in thescientific literature.The speed of sound in the seawater is a function of temperature, salinity, and depth. In such shallow sea asBaltic Sea, the impact of depth is not substantial....
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Evaluation of ASON/GMPLS Connection Control Servers Performance
PublicationPerformance aspects have always been very important in telecommunications, especially in control elements. That problem also regards ASON/GMLPS network, which is one of the propositions for Next Generation Network (NGN) transport stratum. In this paper we investigate performance of ASON/GMPLS Connection Control Servers (CCSs) in laboratory testbed, which architecture and operation are also described. In order to evaluate the performance...
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Theoretical Model of Acoustic Wave Propagation in Shallow Water
PublicationThe work is devoted to the propagation of low frequency waves in a shallow sea. As a source of acoustic waves, underwater disturbances generated by ships were adopted. A specific feature of the propagation of acoustic waves in shallow water is the proximity of boundaries of the limiting media characterised by different impedance properties, which affects the acoustic field coming from a source situated in the water layer “ deformed”...
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2-D constitutive equations for orthotropic Cosserat type laminated shells in finite element analysis
PublicationWe propose 2-D Cosserat type orthotropic constitutive equations for laminated shells for the purpose of initial failure estimation in a laminate layer. We use nonlinear 6-parameter shell theory with asymmetric membrane strain measures and Cosserat kinematics as the framework. This theory is specially dedicated to the analysis of irregular shells, inter alia, with orthogonal intersections, since it takes into account the drilling...
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Dissolution of Nb-doped hydroxyapatite prepared via low-temperature mechanochemical method: Spectroscopy studies
PublicationCalcium phosphate glass ceramics with nominal hydroxyapatite stoichiometry doped with niobium were synthesized using simple as well as low-temperature mechanochemical method and then in the form of compressed pellet were submitted to the static dissolution process in distilled water for one month. The results of structural analysis, performed mainly on the base of spectroscopic methods such as: infrared absorption spectroscopy,...
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The effect of multiaxial geocomposite reinforcement on fatigue performance and crack propagation delay in double-layered asphalt beams
PublicationThe presented study investigates the effect of a recently developed multiaxial geocomposite made of polypropylene geogrid and non-woven fabric on the delay of crack propagation, based on four-point bending tests of large asphalt concrete beams – both for reinforced and non-reinforced specimens. Several approaches are described in this study, including analysis of stiffness modulus decrease and analysis of crack propagation using...
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Wide-field magnetometry using nitrogen-vacancy color centers with randomly oriented micro-diamonds
PublicationMagnetometry with nitrogen-vacancy (NV) color centers in diamond has gained significant interest among researchers in recent years. Absolute knowledge of the three-dimensional orientation of the magnetic field is necessary for many applications. Conventional magnetometry measurements are usually performed with NV ensembles in a bulk diamond with a thin NV layer or a scanning probe in the form of a diamond tip, which requires a...
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Tensile failure study of 3D printed PLA using DIC technique and FEM analysis
PublicationThe paper presents the experimental and numerical study of the failure behaviour of Fused Filament Fabricated (FFF) Polylactic Acid (PLA) samples subjected to tensile load. The examined samples are printed in flat orientation with 0◦, 45◦ and 90◦ raster angles. During the experiments the deformation of the specimens is continuously scanned with the 3D Aramis measuring system utilizing the digital imaging correlation technique,...
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Development of Microstructured Carbon Coatings by Substrate-Catalytic CVD
PublicationCarbon nanostructured films were synthesized by chemical vapor deposition (CVD) on H18 stainless steel (AISI 440C) sheets with an H2/CH4/N2 gas mixture at various substrate temperatures. During the synthesis, the iron and chromium oxide layer was formed between the steel and carbonaceous layer. The carbon films exhibited wall-like and spherical morphologies and structures, as characterized by scanning electron microscopy and Raman...
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Scanning electrochemical micrographs of poly(lactic acid) 3D printed electrodes ablated by femtosecond laser
Open Research DataThe dataset contains the scanning electrochemical micrographs of the femtosecond laser (FSL) ablation at the surface of commercially available carbon black-filled poly(lactic acid) 3D printed electrode. The process is used for the increase of the charge transfer of this electrode in electrochemical studies.
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Effective dielectric constant of two phase dielectric systems
PublicationW tym artykule model brick-layer ścianie został rozszerzony na dwufazowe systemy perkolacyjne. Porównano wyniki obliczeń z danymi eksperymentalnymi. Stałe dielektryczne obu faz oraz próg perkolacji pozwala na wyznaczenie efektywnej stałej dielektrycznej systemu dwufazowego.
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Heat tint colours on stainless steel and welded joints
PublicationSurface layer condition of stainless steels and welded joints influences strongly their corrosion resistance. This problem seems to be underestimated. This current study explains the phenomenon of heat tint forming on welds, the methods of its removal, inspection procedures after heat tint removing and post weld finishing
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Wytwarzanie i modyfikacja powierzchni porowatych struktur tytanowych przeznaczonych na implanty
PublicationCelem pracy było wytworzenie stopu Ti-13Nb-13Zr z wykorzystaniem technologii selektywnego topienia laserowego (SLM) oraz jego biofunkcjonalizacja za pomocą utleniania mikrołukowego (MAO), a następnie określenie wpływu parametrów procesowych na właściwości otrzymanych materiałów pod kątem ich zastosowania na implanty. Oceniono wpływ napięcia, natężenia i czasu procesu MAO przeprowadzanego w elektrolicie zawierającym wapń i fosfor...
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Optimalization of TiO2 nanotube geometry using fuzzy reasoning approach
PublicationThe geometry of TiO2 nanotube layer on titanium, obtained by electrochemical anodization, has been determined by using fuzzy reasoning approach. A proposed method showed the possibility of nanotube array architecture optimization by choosing an appropriate anodization condition. A fuzzy logic controller (FLC) was utilized using Matlab Software.
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Badanie właściwości czujników wilgotności na bazie nanocząstek tlenku cynku
PublicationW celu pomiaru wilgotności szeroko stosowane są czujniki elektryczne. Warstwą czynną, zmieniającą swoje właściwości pod wpływem pary wodnej, stanowią najczęściej materiały ceramiczne lub polimerowe. Tlenek cynku jest jednym z materiałów ceramicznych będących dobrym kandydatem do zastosowania go jako warstwy czynną w czujnikach wilgotności. W tej pracy przedstawiono wyniki badań właściwości struktur czujnikowych z warstwą tlenku...