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Search results for: POROUS SORBENTS
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Detection of People Swimming in Water Reservoirs with the Use of Multimodal Imaging and Machine Learning
PublicationEvery year in many countries, there are fatal unintentional drownings in different water reservoirs like swimming pools, lakes, seas, or oceans. The existing threats of this type require creating a method that could automatically supervise such places to increase the safety of bathers. This work aimed to create methods and prototype solutions for detecting people bathing in water reservoirs using a multimodal imaging system and...
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Pharmaceutical and forensic drug applications of chiral supercritical fluid chromatography
PublicationTHE SUPERCRITICAL FLUID IS AN EXCELLENT CHOICE AS THE CHROMATOGRAPHIC MOBILE PHASE BECAUSE IT ALLOWS RAPID SEPARATION WITH HIGH EFFICIENCY AND APPLICATIONS INVOLVING ENANTIORESOLUTION ARE COMMON. SUPERCRITICAL FLUID CHROMATOGRAPHY (SFC) IS INCREASINGLY USED FOR ANALYTICAL, SEMI-PREPARATIVE AND PREPARATIVE PURIFICATION OF CHIRAL COMPOUNDS, INCLUDING PRODUCTION OF ENANTIOMERS THAT ARE MAINLY ENCOUNTERED DURING DRUG DEVELOPMENT. SFC...
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Morphology control via dual solvent crystallization for high-mobility functionalized pentacene-blend thin film transistors
PublicationWe present an approach to improving the performance of solution processed organic semiconductor transistors based on a dual solvent system. We here apply this to a blend containing the π-conjugated small molecule 6,13 bis(triisopropylsilylethynyl) pentacene (TIPS-pentacene) and polystyrene, which acts as an inert binder. Using a semiconductor-binder solution of two solvents, where the main solvent is a better solvent of the small...
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Solubilization of keratins and functional properties of their isolates and hydrolysates
PublicationThe keratinous wastes of the textile industry and poultry slaughterhouses may be used as sources of soluble keratins or hydrolysates. This review presents methods for processing raw keratin-based materials into bioproducts with functional and bioactive properties suitable for biomedical, cosmetic, food, and agricultural applications. Soluble keratin can be obtained by thermal treatment in some organic solvents, reduction, or oxidation...
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Metrics for green analytical chemistry
PublicationGreen analytical chemistry, although not being a new concept, does not have a greenness metrics system. Green chemistry metrics are not suitable for analytical procedure assessment because they often refer to the mass of the product. Some efforts have been made to develop suitable metrics for analytical chemistry. Some are simple to use but do not cover all aspects of analytical methods’ environmental impact. Others are more comprehensive...
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Understainding solid-phase microextraction: key factors influencing the extraction process and trends in improving the technique
PublicationAnalytical chemists are faced with the daunting challenges of accurately monitoring the state of the environment and the processes taking place in it and of determining an enormous range of analytes often present in trace and ultratrace amounts in sample matrixes with complex or variable compositions. Further challenges are presented by the need to introduce new methodologies into current analytical practice and equipment to comply...
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Copper-based 2D-coordination polymer as catalyst for allylation of aldehydes
PublicationA copper-tartrate, [Cu2(Tart)2(H2O)2]·4H2O, was synthesized at room temperature in aqueous media using copper chloride and D-tartaric acid. The compound crystallizes in the monoclinic system P21 space group and was characterized by infrared spectroscopy, thermogravimetry, X-ray powder diffraction and the results are in good agreement with the single crystal...
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A method for a comprehensive lipidomic analysis of flaxseed (Linum usitatissimum) with the use of LC–Q-TOF-MS and dispersive micro-solid-phase (μDSPE) extraction
PublicationFlaxseed (FS) is one of the richest sources of α-linolenic acid oil and lignans, and it is suggested that the consumption of flaxseed may contribute to the prevention of certain chronic diseases such as many types of cancer, diabetes, cardiovascular diseases and cerebrovascular stroke. Here, we demonstrate a new method for comprehensive FS lipidome profiling with the use of LC–Q-TOF-MS and dispersive micro-solid-phase extraction....
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Synthesis Methods and Favorable Conditions for Spherical Vaterite Precipitation: A Review
PublicationVaterite is the least thermodynamically stable anhydrous calcium carbonate polymorph. It exists very rare in nature, e.g. in some rock formations or as a component of biominerals produced by some fishes, crustaceans or birds. Synthetic vaterite particles are proposed as carriers of active substances in medicines, additive in cosmetic preparations as well as adsorbents. Also, their utilization as a pump for microfluidic flow is...
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Synthesis and polymerisation techniques of molecularly imprinted polymers
PublicationMolecularly Imprinted Polymers (MIPs) are materials that has been processed using the molecular imprinting technique which permit to obtain well-defined three-dimensional cavities, with affinity to a template molecule, in the polymer matrix. Technology involves three strategies, i.e., covalent, non-covalent and semi-covalent approach, but the most popular is non-covalent approach. The most important components for the synthesis...
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Ultrasound assisted dispersive solid phase microextraction using polystyrene-polyoleic acid graft copolymer for determination of Sb(III) in various bottled beverages by HGAAS
PublicationA new polyoleic acid-polystyrene (PoleS) block/graft copolymer was synthesized and applied as adsorbent for ultrasound assisted dispersive solid phase microextraction (UA-DSPME) of Sb(III) in different bottled beverages and analysis using hydride generation atomic absorption spectrometry (HGAAS). Adsorption capacity of the PoleS was 150 mg g−1. Several sample preparation parameters such as sorbent amount, solvent type, pH, sample...
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Analytical chemistry in technical approaches: immobilization of biosorbent waste containing heavy metals in cemented materials
PublicationAn ecologically safe and economically justified method of stabilization of the used biosorbents was developed. Sorbent contaminated with heavy metals has been successfully solidified/stabilized using a hydraulic binder. The test results indicated that up to 1% of the biosorbent residue used could be added without compromising the compressive strength of the mortar. The compressive strength of the modified mortars did not change...
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Kształtowanie architektoniczne morskich portów jachtowych na przykładzie wybranych miast nadbałtyckich
PublicationPraca w zakresie badawczym analizuje i porównuje podobne krajowe i zagraniczne jachtowe porty morskie z uwzględnieniem trzech etapów: projektowy, w trakcie realizacji i zrealizowane. Wyznacza modele przemian, które mogą stać się pomocnym materiałem przy pracach projektowo - badawczych związanych z projektowaniem i oceną poszczególnych portów jachtowych oraz terenów bezpośrednio lub pośrednio związanych z eksploatacją portu.
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Hybrid nanolayers of star polymers and silver nanoparticles with antibacterial activity
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Ultra thick open tubular traps with an increased inner diameter.
PublicationPrzeanalizowano zagadnienia związane z zastosowaniem otwartych pułapek kapilarnych z grubym nieregularnym filmem polidimetylosiloksanu do wzbogacania lotnych związków organicznych. Przeprowadzone rozważania teoretyczne oraz prace eksperymentalne wykazały, że zwiększenie średnicy wewnętrznej pułapek może znacząco polepszyć ich właściwości. Dla danego natężenia przepływu próbki oraz danego stosunku objętości faz w pułapce, liczba...
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S’attaquer à la suprématie du masculin sur le féminin : le français inclusif dans les publications des universités françaises dans les réseaux sociaux
PublicationThis paper aims to examine the use of inclusive French in the Internet publications of Paris universities on their social media. Three higher education institutions were selected: Paris Dauphine-PSL University, Gustave Eiffel University, and Sorbonne Paris North University. The publications were obtained from Facebook, Instagram, and LinkedIn. Firstly, the groups of people to whom the use of inclusive French referred...
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Constructing a Dataset of Speech Recordingswith Lombard Effect
PublicationThepurpose of therecordings was to create a speech corpus based on the ISLEdataset, extended with video and Lombard speech. Selected from a set of 165sentences, 10, evaluatedas having thehighest possibility to occur in the context ofthe Lombard effect,were repeated in the presence of the so-called babble speech to obtain Lombard speech features. Altogether,15speakers were recorded, and speech parameterswere...
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Electrochemical Evaluation of Sustainable Corrosion Inhibitors via Dynamic Electrochemical Impedance Spectroscopy
PublicationFinding suitable measurement methods for the effective management of electrochemical problems is of paramount importance, particularly for improving efficiency in corrosion protection. The need for accurate measurement techniques specific to nonstationary conditions has long been recognized, and promising approaches have emerged. This chapter introduces dynamic electrochemical impedance spectroscopy as a novel advancement in electrochemistry...
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Chemical reactivity and antimicrobial activity of N-substituted maleimides
PublicationZsyntezowano kilkanaście N-podstawionych maleimidów, zawierających w swojej strukturze podstawniki o różnej wielkości i polarności.Maleimidy o charakterze obojętnym wykazywały silny efekt przeciwgrzybowy; ich aktywność przeciwbakteryjna była zróżnicowana. Niską aktywność przeciwbakteryjną, ale wysoką aktywność cytostatyczną stwierdzono dla maleimidów o charakterze zasadowym. Reaktywność chemiczna i lipofilowość miały wpływ na aktywność...
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System of wireless magnetic sensors for detection and identification of ferromagnetic vehicles
PublicationThe paper presents the results of deformation of the Earth's magnetic field by land vehicles. Basing on the analysis of the shape of the magnetic field deformation, it is possible to detect and identify a vehicle. In order to eliminate the interference of the Earth's magnetic field by the environment, the measurements were performed in a differential configuration. Under a development project a wireless system of magnetic sensors...
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QoS Resource Reservation Mechanisms for Switched Optical Networks
PublicationThe paper regards the problem of resource reservation mechanisms for Quality of Service support in switched optical networks. The authors propose modifications and extensions for resources reservation strategy algorithms with resources pools, link capacity threshold and adaptive advance reservation approach. They examine proposed solutions in Automatically Switched Optical Network with Generalized Multi-Protocol Label Switching...
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Enriching the Context: Methods of Improving the Non-contextual Assessment of Sentence Credibility
PublicationThis paper presents several methods of automatic context enrichment of sentences that need to be evaluated, tagged or fact-checked by human judges. We have created a corpus of medical Web articles. Sentences from this corpus have been fact-checked by medical experts in two modes: contextually (reading the entire article and evaluating sentence by sentence) and without context (evaluating sentences from all articles in random order)....
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Deep eutectic solvent-based shaking-assisted extraction for determination of bioactive compounds from Norway spruce roots
PublicationPolyphenolic compounds play an essential role in plant growth, reproduction, and defense mechanisms against pathogens and environmental stresses. Extracting these compounds is the initial step in assessing phytochemical changes, where the choice of extraction method significantly influences the extracted analytes. However, due to environmental factors, analyzing numerous samples is necessary for statistically significant results,...
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Ionic liquids for nano- and microstructures preparation. Part 2: Application in synthesis
PublicationIonic liquids (ILs) are widely applied to prepare metal nanoparticles and 3D semiconductor microparticles. Generally, they serve as a structuring agent or reaction medium (solvent), however it was also demonstrated that ILs can also play a role of a co-solvent, metal precursor, reducing as well as surface modifying agent. The crucial role and possible types of interactions between ILs and growing particles have been presented in...
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Nowoczesne techniki przygotowania próbki do oznaczania analitów organicznych z zastosowaniem chromatografii gazowej. Część I. Podstawy teoretyczne ekstrakcji. Modern techniques of preparation of samples for determining organic analytes by gas chromatography. Part I. Theoretical principles of extraction.
PublicationPrzedstawiono podstawy teoretyczne technik izolacji i wzbogacania analitów organicznych z próbek gazowych oraz ciekłych. Już pobieżna analiza literatury dotyczącej omawianych zagadnień, pokazuje jak różnorodne i bogate spektrum technik jest stosowane na etapie przygotowania próbki. Z drugiej strony, z punktu widzenia podstaw fizykochemicznych, większość technik opiera się na dwóch zjawiskach: adsorpcji analitów na medium zatrzymującym...
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Studies of the separation performance of silanized silica gel for simulated distillation
PublicationWe present the results of investigations of the chromatographic (sorptive) properties of silanized silica gel as a stationary phase for gas chromatography used for simulated distillation. Commercially available silanized sorbent (particle diameter range 63–200 m, average pore size 60 Å) was sieved to obtain the 80–100 mesh fraction (180–150 m). The obtained results revealed that silanized silica gel allows the complete separation...
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Size Exclusion Coupled to Reversed Phase Liquid Chromatography for the Characterization of Cranberry Products
PublicationA combination of solvent extraction, size exclusion purification, and reversed-phase liquid chromatography with UV absorption and fluorescence detection was here used for the determination of flavan-3-ols and related oligomeric compounds in cranberry products. The method relied on robust, simple, and inexpensive instrumental equipment present in most of routine analytical laboratories. Sample extracts in methanol/water/hydrochloric...
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The role of aluminium in metal–organic frameworks derived carbon doped with cobalt in electrocatalytic oxygen evolution reaction
PublicationWater electrolysis is one of the most crucial processes in the development of new energy sources, where ultra-clean fuel is produced - hydrogen. Oxygen evolution reaction (OER) is the sluggish process of overall water splitting. Therefore, this study presents the design, characterization and electrochemical study of cobalt-based electrocatalysts embedded into porous carbons derived from an Al-metal–organic...
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Effect of hybrid modification by ceramic layer formation in MAO process and laser remelting on the structure of titanium bio-alloy Ti13Nb13Zr
PublicationTo improve the biological properties of titanium alloy Ti13Nb13Zr, hybrid modifications involving micro-arc oxidation (MAO) and Nd: YAG laser remelting were carried out in two combinations. The first consisted of laser modification before the production of the ceramic layer by the micro-arc oxidation process, and the second combination involved Nd: YAG laser modification after the MAO process. The creation of developed surface...
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The use of lightweight aggregate saturated with PCM as a temperature stabilizing material for road surfaces.
PublicationThis paper presents the possibility of adding lightweight building aggregates to increase the stability – mechanical as well as thermal - of constructions and road objects. This stability can be achieved through saturating the porous granules of aggregate with a phase-change material (PCM) that allows the accumulation of solar heat. Intense solar radiation, especially during the summer, can cause the asphalt on road surfaces, bridges...
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The Influence of Calcium Glycerophosphate (GPCa) Modifier on Physicochemical, Mechanical, and Biological Performance of Polyurethanes Applicable as Biomaterials for Bone Tissue Scaffolds Fabrication
PublicationIn this paper we describe the synthesis of poly(ester ether urethane)s (PEEURs) by using selected raw materials to reach a biocompatible polyurethane (PU) for biomedical applications. PEEURs were synthesized by using aliphatic 1,6-hexamethylene diisocyanate (HDI), poly(ethylene glycol) (PEG), α,ω-dihydroxy(ethylene-butylene adipate) (Polios), 1,4-butanediol (BDO) as a chain extender and calcium glycerolphosphate salt (GPCa) as...
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The influence of the Cu2O deposition method on the structure, morphology and photoresponse of the ordered TiO2NTs/Cu2O heterojunction
PublicationThe increased interest in highly ordered titania structures exhibiting tubular shape that could be directly formed onto the stable substrate is related with the intensive research on their modification enabling absorption of light within the wide solar spectrum and its further conversion into electric or chemical energy. Among others, formation of uniform 3D heterojunctions based on the TiO2 nanotubes attracts attention since porous...
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Polyurethane based hybrid ciprofloxacin-releasing wound dressings designed for skin engineering purpose
PublicationPurpose Even in the 21st century, chronic wounds still pose a major challenge due to potentially inappropriate treatment options, so the latest wound dressings are hybrid systems that enable clinical management, such as a hybrid of hydrogels, antibiotics and polymers. These wound dressings are mainly used for chronic and complex wounds, which can easily be infected by bacteria. Materials and methods Six Composite Porous Matrices...
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Conversion of waste biomass into activated carbon and evaluation of environmental consequences using life cycle assessment
PublicationIn this article, activated carbon was produced from Lantana camara and olive trees by H3PO4 chemical activation. The prepared activated carbons were analyzed by characterizations such as scanning electron microscopy, energy-dispersive X-ray spectroscopy, Brunauer–Emmett–Teller, X-ray diffraction, thermogravimetric analysis, and Fourier transform infrared spectroscopy. H3PO4 is used as an activator agent to create an abundant pore...
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Tuning Electrochemical Performance by Microstructural Optimization of the Nanocrystalline Functional Oxygen Electrode Layer for Solid Oxide Cells
PublicationFurther development of solid oxide fuel cell (SOFC) oxygen electrodes can be achieved through improvements in oxygen electrode design by microstructure miniaturisation alongside nanomaterials implementation. In this work, improved electrochemical performance of an La0.6Sr0.4Co0.2Fe0.8O3-d (LSCF) cathode was achieved by the controlled modification of the La0.6Sr0.4CoO3-d (LSC) nanocrystalline interlayer introduced between a porous...
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On time-dependent nonlinear dynamic response of micro-elastic solids
PublicationA new approach to the mechanical response of micro-mechanic problems is presented using the modified couple stress theory. This model captured micro-turns due to micro-particles' rotations which could be essential for microstructural materials and/or at small scales. In a micro media based on the small rotations, sub-particles can also turn except the whole domain rotation. However, this framework is competent for a static medium....
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Study of the Resistance to Influence of Aggressive Liquids on Concrete with Lightweight Aggregate
PublicationThe corrosion of the structure of concrete caused by the aggressive external environment is one of the main problems that can reduce the durability of buildings. The paper analyzes the influence of the type of component on selected properties of lightweight concrete (LWC) exposed to aggressive liquids. When lightweight concrete containing porous aggregates is used, the influence of an aggressive environment may be of particular...
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Model of noise sources in supercapacitors
PublicationThe paper presents detailed model of noise sources in supercapacitors. Noise phenomena observed in supercapacitors may be used as a diagnostic tool for assessment of supercapacitor quality or degradation mechanisms (e.g. corrosion of the electrodes or cloggin g up the pores) during ageing. Therefore, it is important to consider where noise is generated. The equivalent circuit of noise sources existing...
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Analiza mostu kolejowego przez rzekę Martwa Wisła w Gdańsku
PublicationOpracowanie dotyczy konstrukcji nowoprojektowanego mostu kolejowego przez rzekę Martwa Wisła w Gdańsku budowanego w ramach zadania "Projekt poprawy dostępu kolejowego do Portu Gdańsk" (most + dwutorowa linia kolejowa). Celem opracowania jest przeprowadzenie analizy obliczeniowej mostu na podstawie jego charakterystyk dostarczonych przez Zleceniodawcę - Biuro Projektów Budownictwa Komunalnego w Gdańsku w formie projektu architektoniczno-budowlanego....
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Możliwości rozwoju transportu kontenerowego na międzynarodowych drogach wodnych E 70 i E 40
PublicationW artykule przedstawiono charakterystykę przewozów różnego rodzaju ładunków z wykorzystaniem transportu śródlądowego na międzynarodowych drogach wodnych E 70 i E40 na odcinku porty morskie Gdańsk, Gdynia – ujście Wisły – Wisła – rejon Solca Kujawskiego. Zaprezentowano dynamikę rozwoju przeładunków ładunków w portach Gdańsk, Gdynia ze szczególnym uwzględnieniem terminali kontenerowych. Zaproponowano utworzenie portu multimodalnego...
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Evolution of models for sorption of PAHs and PCBs on geosorbents.
PublicationWiedza o tym gdzie są zlokalizowane zanieczyszczenia obecne w osadzie oraz z jaką siłą związane są one z osadem jest niezbędna do oszacowania stopnia i skuteczności procesów remediacjyjnych oraz określenia dostępności, mobilności i toksyczności osadów. Dlatego, aby zrozumieć i poznać procesy zachodzące w tak skomplikowanej matrycy, jaką stanowią osady denne/gleby konstruowane są teoretyczne modele matematyczne opisujące prawdopodobny...
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Merging Proline:Xylitol Eutectic Solvent in Crosslinked Chitosan Pervaporation Membranes for Enhanced Water Permeation in Dehydrating Ethanol
PublicationThe scope of this research aims at merging a new deep eutectic mixture (DES) into a biopolymer-based membrane for a pervaporation application in dehydrating ethanol. Herein, an L-proline:xylitol (at 5:1) eutectic mixture was successfully synthesized and blended with chitosan (CS). A complete characterization of the hybrid membranes, in terms of morphology, solvent uptake, and hydrophilicity, has been conducted. As part of their...
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Ionic liquids in extraction techniques: Determination of pesticides in food and environmental samples
PublicationThe intensive use of pesticides in agricultural practices has promoted the appearance of environmentaland public health problems. Due to that, scientists face challenges with developing simple, fast, sensitive,selective, and low-cost methods dedicated to determining pesticide residues in food and environmentalsamples. Following thefifth principle of Green Analytical Chemistry, chemists are searching for greeneralternatives for...
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Oznaczanie niezmienionych form lotnych związków bromo- i chloroorganicznych w próbkach płynów biologicznych z wykorzystaniem opracowanej metodyki TLHS-DAI-GC-ECD
PublicationRozprawa doktorska dotyczyła opracowania nowej procedury analitycznej opartej na wykorzystaniu analizy fazy nadpowierzchniowej nad cienkim filmem cieczy z samoczynną generacją strumienia ciekłego sorbentu w połączeniu z chromatografem gazowym wyposażonym w detektor wychwytu elektronów (TLHS-DAI-GC-ECD). Skupiono się na :1. wykonaniu badań optymalizacyjnych poprzedzających walidację metodyki TLHS-DAI-GC-ECD (sprawdzenie trwałości...
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Dzielnica reprezentacyjna Gdyni
PublicationKoncepcja Dzielnicy Reprezentacyjnej Gdyni ma historię tak długą jak samo miasto. Już pierwsze plany urnanistyczne z 1926 r. przewidywały jej budowę na południe od portu, jednakże później uległy one zmianie. Szeroko dyskutowany i bardzo interesujący projekt tej dzielnicy powstał w 1938 r., lecz zdołano zaledwie rozpocząć jego realizację przed 1939 r. Projekt ten po wojnie zarzucony odradza się w innym kształcie w czasach współczesnych.
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Construction and investigation of SO2 amperometric sensor with a solid polymer electrolyte membrane
Publicationn this paper a sensor for detection of the sulphur dioxide based on three electrode cell configuration with a liquid electrolyte, a mercury sulphate reference electrode and a solid polymer electrolyte working electrode is presented. Working elec- trode was obtained by using Takenaka-Torikai chemical deposi- tion method by precipitation of Au particles into the pores of the Nafion membrane. Sensors characteristics measurements were...
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Założenia modelu zarządzania kryzysowego bezpieczeństwem w portach morskich
PublicationZłożoność przestrzenna i gospodarcza oraz silne oddziaływanie działalności portowej na procesy społeczno-gospodarcze w regionie, wymaga opracowania specjalnego podejścia do zarządzania bezpieczeństwem na obszarach portowych. W pracy przedstawiono założenia modelu zarządzania kryzysowego bezpieczeństwem w portach morskich uwzględniające zasady międzynarodowego kodeksu ISPS (International Ship and Port Security Code) oraz wymagania...
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The spatial planning of industrial areas in an urbanized area for cargo, in the development of inland waterway transport
PublicationSpatial planning, taking into account the configuration of the surface, i.e. its shape (relief) and the presence and mutual location of objects and points of characteristic water ports, is a derivative of several natural, economic, market, technical, social and political factors. It depends on the destination port, the planned structure of trade in cargo, the forecasted traffic of ships, passageways, the technology of reloading...
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Analysis of Corrugated Coaxial Line with the Use of Body of Revolution and Finite Element Method
PublicationA combination of the body-of-revolution and finite element methods is utilized to the analysis of coaxial lines with corrugated rod and wall. Both periodic and non-periodic structures can be investigated. As the structure is axially symmetrical the two dimensional scalar-vector finite element method can be used, which allows for the investigation of complex geometries and is computationally efficient. A generalized impedance matrix...
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Comparison of different extraction techniques of polychlorinated biphenyls from sediments samples.
PublicationIn this work, problems that may occur during determination of trace levels of polychlorinated biphenyls in sediment samples are described. Main error sources are connected with extraction of analytes prior to final determination. During model studies, polychlorinated biphenyls have been extracted from sedimentreference material (METRANAL 2) with the use of different solvents (dichloromethane, hexsane, and toluene); the process...