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Solvent-Free Synthesis of Phosphonic Graphene Derivative and Its Application in Mercury Ions Adsorption
PublicationFunctionalized graphene was efficiently prepared through ball-milling of graphite in the presence of dry ice. In this way, oxygen functional groups were introduced into material. The material was further chemically functionalized to produce graphene derivative with phosphonic groups. The obtained materials were characterized by spectroscopic and microscopic methods, along with thermogravimetric analysis. The newly developed material...
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Reactions on the surface of the implant under the influence of biofilm
PublicationThe contact of a biomaterial with the biological environment in in vitro and in vivo tests leads to the production of a particular ecosystem in which the active roles perform both, the material surface and the extracellular matrix protein forming a biofilm. Proteins affect cell and bacteria adhesion processes, biological activity of cells and activation of inflammatory response.The knowledge of the reaction mechanisms active on...
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Electrochemical investigations on corosivity of de-icing liquids for railway infrastructure
PublicationThe paper presents the results of electrochemical tests of the de-icing fluid for railway infrastructure. DC and AC electrochemical tests were performed to determine the corrosion rates of structural steel, cast iron and aluminium in the newly produced fluid. The results were compared with the corrosion rates of the same materials in the fluid without corrosion inhibitors. The obtained test results indicate a low corrosion risk...
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Building culture written into the landscape – how to read spatial tradition
PublicationThe article presents a discussion on the experimenting with material leading to practical so-lutions in building structure in the context of the tradition of the place. It sketches out the practical aspects of creation of space while working with different local materials during the intensive workshops within the Structures in Building Culture IP programme. This kind of unique possibility to practice raw materials gives also the...
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Structure and thermoelectric properties of Cs-Bi-Te alloys fabricated by different routes of reduction of oxide reagents
PublicationCesium-bismuth-telluride polycrystalline materials were fabricated using a cost-effective method based on a reduction of oxide reagents, leading to a production of a material with good thermoelectric properties. Several samples with various initial stoichiometry were prepared by melting of oxide powders at 1050 °C, quenching, milling to powders and then reducing in pure hydrogen at 400 °C. Another concept was to obtain the CsBi4Te6...
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Jumping Wave Characteristic during Low Plasticity Burnishing Process
PublicationDuring the low plasticity burnishing process of soft materials such as carbon steel with a hardness of up to 40 HRC (Rockwell grade) a raised structure of the material known as the Jumping Wave forms in front of the tool roll. This phenomenon significantly disturbs the burnishing process, but is very poorly described in the literature. This article presents studies of this phenomenon on the example of burnished 1.0562 steel. The...
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Wpływ geometrii i szorstkości ścian na wielkość naporu materiału sypkiego na dno silosu = Influence of geometry and wall roughness of silo wall on bottom vertical pressure
PublicationW pracy przedstwiono analizę wpływu wysokości i szorstkości ścian silosu cylindrycznego na rozkład naporu na ściany i dno. Badania przeprowadzono dla piasku bezkohezyjnego.
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Palm Oil Fuel Ash-Based Eco-Efficient Concrete: A Critical Review of the Short-Term Properties
PublicationThe huge demand for concrete is predicted to upsurge due to rapid construction developments. Environmental worries regarding the large amounts of carbon dioxide emanations from cement production have resulted in new ideas to develop supplemental cementing materials, aiming to decrease the cement volume required for making concrete. Palm-oil-fuel-ash (POFA) is an industrial byproduct derived from palm oil waste’s incineration in...
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Properties of LiMnBO3 glasses and nanostructured glass-ceramics
PublicationPolycrystalline LiMnBO3 is a promising cathode material for Li-ion batteries. In this work, we investigated the thermal, structural and electrical properties of glassy and nanocrystallized materials having the same chemical composition. The original glass was obtained via a standard melt-quenching method. SEM and 7Li solid-state NMR indicate that it contains a mixture of two distinct glassy phases. The results suggest that the...
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Numerical Modelling of Connections Between Stones in Foundations of Historical Buildings
PublicationThe aim of this paper is to analyse the behaviour of old building foundations composed of stones (the main load-bearing elements) and mortar, based on numerical analysis. Some basic aspects of historical foundations are briefly discussed, with an emphasis on their development, techniques, and material. The behaviour of a foundation subjected to the loads transmitted from the upper parts of the structure is described...
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Extended micropolar approach within the framework of 3M theories and variations thereof
PublicationAs part of his groundbreaking work on generalized continuum mechanics, Eringen proposed what he called 3M theories, namely the concept of micromorphic, microstretch, and micropolar materials modeling. The micromorphic approach provides the most general framework for a continuum with translational and (internal) rotational degrees of freedom (DOF), whilst the rotational DOFs of micromorphic and micropolar continua are subjected...
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Etazene (N,N-diethyl-2-{[(4-ethoxyphenyl)methyl]-1H-benzimidazol-1-yl}-ethan-1-amine (dihydrochloride)): a novel benzimidazole opioid NPS identified in seized material: crystal structure and spectroscopic characterization
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Morphology and the physical and thermal properties of thermoplastic polyurethane reinforced with thermally reduced graphene oxide
PublicationIn this study, thermally reduced graphene oxide (TRG)-containing polyurethane nanocomposites were obtained by the extrusion method. The content of TRG incorporated into polyurethane elastomer systems equaled 0.5, 1.0, 2.0 and 3.0 wt%. The morphology, static and dynamic mechanical properties, and thermal stability of the modified materials were investigated. The application of TRG resulted in a visible increase in material stiffness...
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Numerical modelling of the mesofracture process of sintered 316L steel under tension using microtomography
PublicationThis paper concerns numerical modelling of the deformation process, taking into account the local fracture of porous 316L sinters at the mesoscopic scale using the finite element method. Calculations are performed with the use of geometrical models, to map the realistic shape of the porous mesostructure of the material, obtained by means of computed microtomography. The microtomographic device has limited and insufficient measurement...
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Medical-Grade PCL Based Polyurethane System for FDM 3D Printing—Characterization and Fabrication
PublicationThe widespread use of three-dimensional (3D) printing technologies in medicine has contributed to the increased demand for 3D printing materials. In addition, new printing materials that are appearing in the industry do not provide a detailed material characterization. In this paper, we present the synthesis and characterization of polycaprolactone (PCL) based medical-grade thermoplastic polyurethanes, which are suitable for forming...
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Composites in energy storing prosthetic feet
PublicationComposites reinforced with carbon and glass fibers have become the commonly used material in the production of energy storing prosthetic feet (ESPF/elastic feet prostheses). Their properties ensure a stable and light structure that allows for accumulation, storage and release of energy during walking, thus ensuring an increase in gait efficiency. Depending on the modification of the composite in terms of fiber selection, their...
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Poprawa nośności platform roboczych
PublicationW artykule przedstawiono zagadnienia związanie z zastosowaniem geosyntetyków oraz materiałów wiązanych hydraulicznie (HBM) do stabilizacji platform roboczych pod ciężki sprzęt budowlany.
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Diagnozowanie systemów ochrony katodowej techniką spektroskopii impedancyjnej
PublicationZaprezentowano wyniki badań wykonywanych techniką elektrochemicznej spektroskopii impedancyjnej (EIS) na elementach instalacji ochrony katodowej podziemnego rurociągu stalowego. Przedstawiono widma impedancyjne układów rurociąg-elektrody odniesienia (stacjonarne i przenośne). Wykazano, że przy pomocy EIS można zbadać stan techniczny elektrod odniesienia, co pozwala określić wiarygodność wyników pomiarów potencjału chronionej konstrukcji....
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Application of the Mathar method to identify internal stress variation in steel as a welding process result
PublicationThe paper deals with the method to identify internal stresses in two-dimensional steel members. Steel members were investigated in the delivery stage and after assembly, by means of electric-arc welding. In order to perform the member assessment two methods to identify the stress variation were applied. The first is a non-destructive measurement method employing local external magnetic field and to detecting the induced voltage,...
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Recycling of Waste Rubber by Thermo-Mechanical Treatment in a Twin-Screw Extruder
PublicationRecycling of waste tires is a significant issue considering both environmental and economic aspects. One of the leading recycling routes is the shredding of tires resulting in the generation of ground tire rubber. This material can be easily introduced into various polymer matrices as a filler, reducing the use of conventionally applied petroleum-based materials. In such cases, it is essential to ensure sufficient interfacial compatibility,...
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Biomechanical properties of 3D-printed bone models
PublicationBone lesions resulting from large traumas or cancer resections can be successfully treated by directly using synthetic materials or in combination with tissue engineering methods (hybrid). Synthetic or hybrid materials combined with bone tissue’s natural ability for regeneration and biological adaptation to the directions of loading, allow for full recovery of its biological functions. Increasing interest in new production methods...
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Composite Beams with glass and reinforced or prestressed concrete - early stage of a theorethical and experimental analysis of a shear zone
PublicationThe aim of this article is to present a forgoing preparation for a theoretical and experimental analysis of a shear zone of a composite beams with glass and reinforced or prestressed concrete. Authors present their current knowledge, achievements and predicted challenges in later stages of the research. Properties of component materials are presented in the context of compensating weaknesses of one material with strengths of the...
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Linear Micropolar Elasticity Analysis of Stresses in Bones Under Static Loads
PublicationWe discuss the finite element modeling of porous materials such as bones using the linear micropolar elasticity. In order to solve static boundary-value problems, we developed new finite elements, which capture the micropolar behavior of the material. Developed elements were implemented in the commercial software ABAQUS. The modeling of a femur bone with and without implant under various stages of healing is discussed in details
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A new finite element with variable Young's modulus
PublicationThe Finite Element Method (FEM) is a numerical technique that is well-established in the field of engineering. However, in biological sciences, it is justtaking its first steps. Bone tissue is an example of biological material which isexposed to high loads in its natural environment. Practically every movementof the body results in changing stress levels in the bone. Nature copes with thisvery well but when human intervention is...
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Concentration‐Induced Hetero‐Valent Partial‐Inverse Occupation of Infrared Phosphor
PublicationInfrared luminescent materials have evoked much attention from chemists and material scientists. Although substantial progress is made in materials design, the luminescent mechanism remains ambiguous in the complex structures, presenting major barriers to developing novel infrared luminescent materials. Herein, this study aims to deliberate a complete discussion on infrared phosphors with concentration-induced hetero-valent partial-inverse...
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Measuring radioactive powder samples on the highresolution powder diffraction beamline at the European Synchrotron Radiation Facility
PublicationThis laboratory note describes a new sample preparation technique to enable high-resolution powder diffraction experiments at the European Synchrotron Radiation Facility on radioactive samples. The sample preparation involves setting the active material in resin and several layers of encapsulation suitable for measurement at the beamline. This has allowed low-temperature measurements on very small quantities of samples, providing...
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Fatigue behaviour of SLM maraging steel under variable-amplitude loading
PublicationOne of the most challenging issues for additive manufactured materials is fatigue endurance. Engineering components often operate under complex, variable amplitude loadings, in which existing technological imperfections promote fatigue cracks growth and damage of elements eventually. In this study the effects of different variable-amplitude strain levels on fatigue life, 18Ni300 steel was tested. The work presents various behaviours...
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Materiały do poznania ważek (Odonata) Pojezierza Litewskiego (Polska północno-wschodnia), ze szczególnym uwzględnieniem Suwalskiego Parku Krajobrazowego, zebrane przy okazji XIX Sympozjum Sekcji Odonatologicznej Polskiego Towarzystwa Entomologicznego w 2023 r.
PublicationFrom 6-9 July 2023, the participants of the 19th Symposium of the Odonatological Section of the Polish Entomological Society carried out fieldwork on the dragonflies in and around the Suwałki Landscape Park (SPK) (NE Poland). The symposium was preceded by a field reconnaissance (8-10 June). The results of this fieldwork, which yielded 45 species at 22 sites, are presented and discussed. Three species...
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Nowoczesne rozwiązania stosowane w kontekście ograniczenia strat energetycznych w budynkach oraz poprawy komfortu cieplnego
PublicationW artykule zaprezentowano nowoczesne rozwiązania pozwalające na zmniejszenie energochłonności budynków oraz ograniczenie wpływu warunków atmosferycznych na komfort cieplny. Omówiono metodologię optymalizacji kształtu oraz rodzaju materiałów wykorzystywanych w procesie powstawania budynków użytkowych. Zaprezentowano tu metody oparte o najnowsze zdobycze techniki takie jak materiały budowlane z domieszką PCM (ang. Phase change materials)
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Investigation of functional layers of solid oxide fuel cell anodes for synthetic biogas reforming
PublicationSolid oxide fuel cells (SOFCs) are one of the most promising energy conversion devices due to their high efficiency, low pollution and fuel flexibility. Unfortunately, when hydrocarbons are used as a fuel, for example in the form of a biogas, solid carbon can deposit on the anode surface. This process leads to the degradation of the fuel cell performance. A possible solution to this problem is to apply an additional catalytic material,...
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Insights into Seawater Biodegradation of Sustainable Mater-Bi/Poly(ε-caprolactone)-Based Biocomposites Filled with Diisocyanate-Modified Cellulose Particles
Publication: Due to rapid economic growth, the use of plastics in almost all areas of human life has significantly increased over recent decades, leading to massive pollution. Therefore, works dealing with sustainable and biodegradable polymer materials are vital now. Herein, sustainable MaterBi/poly(ε-caprolactone) (PCL)-based biocomposites, filled with diisocyanate-modified cellulose particles, were prepared and subjected to 12-week seawater...
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Analysis of the Environmental Impact of the Hull Construction of a Small Vessel Based on LCA
PublicationIn recent years, issues related to the impact of human activity on the natural environment have become pressing, and the challenge of global warming necessitates immediate action. To support environmental protection efforts, it has become imperative to adopt a broader perspective when evaluating various products and systems. A valuable tool for such assessments is a life cycle assessment (LCA), which enables a comprehensive analysis...
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Reliability of acicular grindable thermocouples for transient temperature measurements at sliding contacts
PublicationAcicular grindable thermocouples represent an interesting and prospective technique of temperature measurements at sliding contacts. This study aimed at the investigation of their reliability and accuracy as applied to the friction materials of various classes in contact with steel. The tests were conducted on a pin-on-disc tribometer under stationary and transient regimes. The experimental results were validated by comparing the...
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Harmonic Vibrations of Nanosized Magnetoelectric Bodies with Coupled Surface and Interphase Effects: Mathematical Models and Finite Element Approaches
PublicationThe harmonic problems for piezomagnetoelectric nanosized bodies with taking into account the coupled damping and surface effects are considered on the base of the generalized Gurtin-Murdoch model. In the development of previous investigations, the coupled mechanical, electric and magnetic surface effects with surface inertial terms are introduced into the model. For a homogeneous model, the composite material is considered as homogeneous...
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Functionalized polyolefins, synthesis application and industrial relevance
PublicationPolymers play a key role in our modern life full of technical advances and a continuous request for new materials with tailored properties for a low price. Their excellent mechanical properties, good processability, chemical stability and low price make polyolefins the polymers of choice for most commodity and some more specialized applications. As a result, polyolefins account for over 65% of the total world demand of plastic...
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Impact of reclaimed asphalt pavement (RAP) on low-temperature properties of asphalt concrete
PublicationHot mix recycling is a practice which enables reusing materials from old asphalt pavements. Current Polish regulations allow usage of RAP only for binder and base courses, and its amount is limited. Asphalt mixtures with RAP material have to fulfil requirements stated for typical asphalt mixtures. The research presents low-temperature properties of twelve different asphalt concretes with RAP material, determined using three-point...
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Degradable poly(ester-ether) urethanes of improved surface calcium deposition developed as novel biomaterials
PublicationBones, which are considered as hard tissues, work as scaffold for human body. They provide physical support for muscles and protect intestinal organs. Percentage of hard tissues in human body depends on age, weight, and gender. Human skeleton consists of 206 connected bones. Therefore, it is natural that the hard-tissue damage such as fractures, osteoporosis, and congenital lack of bone may appear. The innovative way of bone healing...
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Ongoing Progress on Pervaporation Membranes for Ethanol Separation
PublicationEthanol, a versatile chemical extensively employed in several fields, including fuel production, food and beverage, pharmaceutical and healthcare industries, and chemical manufacturing, continues to witness expanding applications. Consequently, there is an ongoing need for cost-effective and environmentally friendly purification technologies for this organic compound in both diluted (ethanol-water–) and concentrated solutions (water-ethanol–)....
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Cyclic mechanical stress impact on protective properties of organic coatings
PublicationCelem pracy jest zaprezentowanie wyników badań wpływu cyklicznych naprężeń mechanicznych na układy powłoka/metal. Powtarzające się naprężenia mechaniczne zostały zidentyfikowane jako czynnik w znaczącym stopniu przyczyniający się do degradacji powłok. Próbki składające się z powłoki epoksydowej nałożonej na stal St3SAl poddano serii 21000 cykli naprężenie-odpuszczenie. Badania przeprowadzono w zakresie odkształceń elastycznych...
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Three-point bending test of sandwich beams supporting the GFRP footbridge design process - validation
PublicationSome selected aspects concerning material and construction design issues for pedestrian footbridge made of GFRP composite materials are elaborated in this paper. The analysis is focused on validation tests, which are particularly important because of the advanced technology and materials that are used for this innovative bridge. The considered footbridge is a sandwich-type shell structure comprising of PET foam core and outer skins...
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Polyurethanes as a Potential Medical-Grade Filament for Use in Fused Deposition Modeling 3D Printers – a Brief Review
PublicationThe possibility of using 3D printing technology (3DP) in medical field is a kind of revolution in health care. This has contributed to a rapid growth in demand for 3D printers, whose systems and materials are adapted to strict medical requirements. In this paper, we report a brief review of polyurethanes as a potential medical-grade filament for use in Fused Deposition Modeling (FDM) 3D printer technology. The advantages of polyurethanes...
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Measurements of Thermal Conductivity of LWC Cement Composites Using Simplified Laboratory Scale Method
PublicationThe implementation of low-energy construction includes aspects related to technological and material research regarding thermal insulation. New solutions are sought, firstly, to reduce heat losses and, secondly, to improve the environment conditions in isolated rooms. The effective heat resistance of insulating materials is inversely proportional to temperature and humidity. Cement composites filled with lightweight artificial...
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Double ZIF-L structures with exceptional CO2 capacity
PublicationCarbon dioxide emission is an emerging problem nowadays and new methods are designed for its control. In this article, a report on the formation of zeolitic imidazole framework with an apparent double leaf-like morphology DZIF-L is given. The special structure of the materials prevents from aggregation of the particles providing remarkable CO2 capacity. At 0.1 MPa the CO2 uptake was 2.99 ± 0.06 mmol/g. The capacity of synthesized...
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An Attempt to Develop a Model Selection Algorithm of Computer Simulation during the Design Process of Mechanical Response of Any Mechanical Body
PublicationIn the literature, there are algorithms associated with the design of simulations of technological processes, in which the material model has always been defined previously. However, in none of the studies of computer simulation modelling of technological processes known to the authors of this article, is there a detailed description of how the algorithm, or the selection of plastic model used, is subject to this process. This...
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An attempt to develop a model selection algorithm of computer simulation during the design process of mechanical response of any mechanical body
Publicationn the literature, there are algorithms associated with the design of simulations of technological processes, in which the material model has always been defined previously. However, in none of the studies of computer simulation modelling of technological processes known to the authors of this article, is there a detailed description of how the algorithm, or the selection of plastic model used, is subject to this process. This article...
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Multiple Reprocessing of Conductive PLA 3D-Printing Filament: Rheology, Morphology, Thermal and Electrochemical Properties Assessment
PublicationAdditive manufacturing technologies are gaining more and more attention, resulting in the development or modification of 3D printing techniques and dedicated materials. On the other hand, economic and ecological aspects force the industry to develop material recycling strategies. In this work, the multiple reprocessing of a commercially available PLA conductive composite with carbon black filler, dedicated to 3D printing, was investigated....
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Wpływ wybranych parametrów środowiska na przebieg degradacji rur okładzinowych ze stali P110
PublicationMateriały używane na orurowanie odwiertów w poszukiwaniu i wydobyciu ropy i gazu poddawane są niekorzystnym warunkom eksploatacji takich jak: podwyższona temperatura, wysokie ciśnienie, turbulentny przepływ korozyjnych cieczy z zawieszonymi cząstkami stałymi. Jednym z gatunków stali używanych do produkcji rur okładzinowych jest stal P110 (za normą API 5CT) będąca stalą średnio-węglową, niskostopową o wysokiej wytrzymałości. Celem...
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Centrum Nanotechnologii w Gdańsku
PublicationPublikacja jest prezentacją zrealizowanego budynku Centrum Nanotechnologii "B" Politechniki Gdańskiej. Punktem odniesienia dla autorów projektu był zespół historycznych obiektów kampusu Politechniki Gdańskiej, zrealizowanych w stylu neorenesansu niderlandzkiego. Odniesienia do zabudowy historycznej nie są jednak zapożyczeniami ani bezpośrednimi przeniesieniami. Nowo projektowany budynek jest architekturą na wskroś współczesną,...
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Characterization of Highly Filled Glass Fiber/Carbon Fiber Polyurethane Composites with the Addition of Bio-Polyol Obtained through Biomass Liquefaction
PublicationThis work aims to investigate the process of obtaining highly filled glass and carbon fiber composites. Composites were manufactured using previously obtained cellulose derived polyol, polymeric methylene diphenyl diisocyanate (pMDI). As a catalyst, dibutyltin dilaurate 95% and Dabco® 33-LV were used. It was found that the addition of carbon and glass fibers into the polymer matrix causes an increase in the mechanical properties...
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Evaluation of La 2 Ni 0.5 Cu 0.5 O 4+δ and Pr 2 Ni 0.5 Cu 0.5 O 4+δ Ruddlesden-Popper-type layered oxides as cathode materials for solid oxide fuel cells
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