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Search results for: 81.15.GH
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Value co‐creation (VCC) and value co‐destruction (VCD) via open government data (OGD): Empirical case of Tanzania
PublicationHaving emphasized upon the potential benefits of Open Government Data (OGD) initiatives via value derivation and innovation pursuits of the stakeholders, it falls in place to complement this line of OGD research in the specific case of Tanzania, a developing country, to support the inferences. Specifically, it is important to understand the manner in which OGD VCC-one of the hinges of OGD initiatives- and OGD VCD-a possible fall...
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A COMPREHENSIVE REVIEW OF LIFE CYCLE ASSESSMENT AND ENERGY EFFICIENCY IN 3D PRINTING FOR CONSTRUCTION: CURRENT STATE, BENEFITS, LIMITATIONS, AND FUTURE OUTLOOK
PublicationThe agenda of Industry 4.0 strongly affects design and construction at all its phases, and three-Dimensional Printing (3DP) is an essential part of it. The emerging technology has the potential to become a more valid and accepted form of construction. This research is based on a literature review regarding the relationships between the concepts of Life Cycle Assessment (LCA) and energy efficiency for 3DP in construction research...
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Doświadczenia z eksploatacji oczyszczalni hydrofiowych.
PublicationW pracy przedstawiono doświadczenia z eksploatacji dotychczas monitorowanych obiektów hydrofitowych w Polsce. Na podstawie uzyskanych wyników monitoringu obiektów przyzagrodowych i lokalnych wykazano, że jednostopniowe obiekty hydrofitowe zapewniały skuteczne usuwanie substancji organicznej wyrażonej w BZT5 i ChZTCr oraz zawiesiny ogólnej. Średnia efektywność usuwania BZT5 wynosiła 76,4% w zakresie obciążeń od 15 do 115 kg/ha·d....
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Effect of porosity on physical properties of lightweight cement composite with foamed glass aggregate
PublicationThis paper reports on a study of physical properties of lightweight cement composite. We investigate the possibility of replacing traditional aggregate with Granulated Ash Aggregate (GAA) and above all with Granulated Expanded Glass Aggregate (GEGA). For this purpose, 15 specimens of different percentage share of each aggregate in total aggregate volume were tested: 0%, 25%, 50%, 75% or 100% of foam glass aggregate (GEGA) partially...
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Biopolyols obtained via microwave-assisted liquefaction of lignin: structure, rheological, physical and thermal properties
PublicationThe present study examined the application of polyols obtained via microwave-assisted liquefaction of lignin in the production of rigid polyurethane foam. Lignin was liquefed in crude glycerol and 1,4-butanediol at diferent temperatures (130–170 °C), without a catalyst and using various biomass concentrations (15 and 30 wt%). The physicochemical properties, process yield, and FTIR-based identifcation of the obtained polyols were...
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Load-carrying capacity of axially loaded concrete-filled steel tubular columns made of thin tubes
PublicationAn experimental investigation was conducted on 30 CFST columns. An influence of the following factors on load-carrying capacity of the investigated columns was analyzed: the column slenderness (l1 = 42, l2 = 27 and l3 = 15), the tube thickness (the reinforcement ratio was equal to 4% or 6%), the way of applying the load to CFST columns (through the concrete core or through the entire cross-section), the bond strength between a...
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Effective degradation of sulfide ions and organic sulfides in cavitation-based Advanced Oxidation Processes (AOPs)
PublicationThe paper presents the results of investigations on the effectiveness and reaction rate constants of the oxidation of sulfide ions and organic sulfides in real industrial effluents from the production of bitumens (2000 mg S2- L-1) using hydrodynamic and acoustic cavitation. The content of the effluents was analysed in terms carbon disulfide, dimethyl sulfide, and di-tert-butyl disulfide concentration. A possibility of complete...
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Quality Evaluation of Voice Transmission Using BPL Communication System in MV Mine Cable Network
PublicationThis article presents results of a quality evaluation study, considering voice transmission in a 6 kV medium voltage cable network using the BPL (Broadband over Power Line) communication system. The tests are carried out under real mining conditions for the selected power cable without voltage, earthed at both sides. Such a method of monitoring work conditions is of great importance, especially during a disaster. Power cables are...
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Technologia unieszkodliwiania osadów ściekowych przy zastosowaniu metody hydrofitowej
PublicationMetoda hydrofitowa odwadniania i stabilizacji osadów ściekowych polega na wielowarstwowych zalewów osadami o niskim stężeniu suchej masy 0,5-1%. Najczęściej w tym celu wykorzystuje się specjalnie zbudowane obiekty naziemne lub podziemne zasiedlone trzcina pospolitą. Pomimo naturalnego charakteru procesu w porównaniu z urządzeniami mechanicznymi skuteczność odwadniania osadów w obiektach trzcinowych jest bardzo wysoka. Materiał...
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Tereny polarne - interesującym obszarem do badań. - Część 1 Analityka próbek pochodzących od organizmów żywych
PublicationŚrodowisko Arktyki stanowi unikalny w skali globalnej ekosystem, charakteryzujący się niezwykłą wrażliwością na zmiany związane z postępującą antropopresją. Ze względu na warunki środowiskowe oraz położenie geograficzne, obszar Archipelagu Svalbard uznawany jest za rezerwuar zanieczyszczeń pochodzenia antropogenicznego. W pracy zestawiono i omówiono informacje dotyczące zanieczyszczeń zdeponowanych w próbkach pochodzących od organizmów...
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Evaluation of structural change during fast transformation process of cross-linked NR into liquid NR by light pyrolysis
PublicationThe presence of cross-linked networks in rubber creates a tremendous problem for recycling and reusing of waste rubber. Fast transformation of cross-linked natural rubber (NR) into liquid natural rubber was carried out by light pyrolysis in temperature range from 240 to 300 °C in variable time (in range: 1–30 min). The transformation efficiency was evaluated by measuring the sol fraction and the cross-link density of the gel fraction....
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Electrodes consisting of PEDOT modified by Prussian Blue analogues deposited onto titania nanotubes – Their highly improved capacitance
PublicationIn this work we present the outstanding energy storage of prepared inorganic-organic heterojunction where hydrogenated ordered titania nanotubes (H-TiO2NT) were modified by the hybrid made of poly(3,4-ethylenedioxythiophene) (pEDOT) and iron hexacyanoferrate centres (Fehcf, Prussian Blue). The material TiO2NT/pEDOT:Fechf was obtained electrochemically by means of: anodization, hydrogenation and finally, electropolymerization of...
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Innovative Turbine Intake Air Cooling Systems and Their Rational Designing
PublicationThe improved methodology of the engine intake air cooling system designing based on the annual effect due to cooling was developed. It involves determining the optimal value of cooling capacity, providing the minimum system sizes at maximum rate of annual effect increment, and its rational value, providing a close to maximum annual effect without system oversizing at the second maximum rate of annual effect increment within the...
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Electrochemical determination of nitroaromatic explosives at boron-doped diamond/graphene nanowall electrodes: 2,4,6-trinitrotoluene and 2,4,6-trinitroanisole in liquid effluents
PublicationThe study is devoted to the electrochemical detection of trace explosives on boron-doped diamond/graphene nanowall electrodes (B:DGNW). The electrodes were fabricated in a one-step growth process using chemical vapour deposition without any additional modifications. The electrochemical investigations were focused on the determination of the important nitroaromatic explosive compounds, 2,4,6-trinitrotoluene (TNT) and 2,4,6-trinitroanisole...
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Liquefaction of alder wood as the source of renewable and sustainable polyols for preparation of polyurethane resins
PublicationLiquefaction of wood-based biomass gives different polyol properties depending on the reagents used. In this article, alder wood sawdust was liquefied with glycerol and poly(ethylene glycol) solvents. Liquefaction reactions were carried out at temperatures of 120, 150 and 170 °C. The obtained bio-polyols were analyzed in order to establish the process efficiency, hydroxyl number, acid value, viscosity and structural characteristics...
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Hybrid‐mode single‐slope ADC with improved linearity and reduced conversion time for CMOS image sensors
PublicationIn the paper, a single‐slope analog‐to‐digital converter (ADC) for integrated CMOS image sensor applications with an improved technique of conversion has been proposed. The proposed hybrid‐mode ADC automatically uses one of the following conversion techniques: time based (i.e. PWM) or voltage based (i.e. single‐slope). During the ADC operation, the clock frequency and reference voltage are modified in order to reduce the conversion...
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The Impact of Spatiotemporal Changes in Land Development (1984–2019) on the Increase in the Runoff Coefficient in Erbil, Kurdistan Region of Iraq
PublicationNowadays, geospatial techniques are a popular approach for estimating urban flash floods by considering spatiotemporal changes in urban development. In this study, we investigated the impact of Land Use/Land Cover (LULC) changes on the hydrological response of the Erbil basin in the Kurdistan Region of Iraq (KRI). In the studied area, the LULC changes were calculated for 1984, 1994, 2004, 2014 and 2019 using the Digital Elevation...
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Dynamics of Antimicrobial Peptide Encapsulation in Carbon Nanotubes: The Role of Hydroxylation
PublicationIntroduction: Carbon nanotubes (CNTs) have been widely employed as biomolecule carriers, but there is a need for further functionalization to broaden their therapeutic application in aqueous environments. A few reports have unraveled biomolecule–CNT interactions as a measure of response of the nanocarrier to drug-encapsulation dynamics. Methods: Herein, the dynamics of encapsulation of the antimicrobial peptide HA-FD-13 (accession...
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Analyzing the Impact of Simulated Multispectral Images on Water Classification Accuracy by Means of Spectral Characteristics
PublicationRemote sensing is widely applied in examining the parameters of the state and quality of water. Spectral characteristics of water are strictly connected with the dispersion of electromagnetic radiation by suspended matter and the absorp-tion of radiation by water and chlorophyll a and b.Multispectral sensor ALI has bands within the ranges of electromagnetic radia-tion: blue and infrared, absent in sensors such as Landsat, SPOT,...
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Experimental and numerical investigation on shell and coil storage unit with biodegradable PCM for modular thermal battery applications
PublicationThermal energy storage (TES) in automotive applications is currently growing in importance. TES can visibly reduce primary energy consumptions, decrease CO2 emission, and improve thermal comfort in electric as well as hybrid vehicles. However, to meet the new ambitious target (15% reduction of CO2 emissions in the new cars until 2025) it is required to use plug-in electric vehicles. For this reason, this paper focuses on the optimization...
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The correlation between nutritional and health potential and antioxidant properties of raw edible oils from cultivated and wild plants
PublicationThe nutritional properties and health potential of oils from 15 various cultivated and wild plants were investigated on the basis of the fatty acids profiles, total carotenoids and tocopherols content, antioxidant properties and health potential indexes such as atherogenicity index (AI). The oil contents of the plants varied between 0.9 g/100 g for lychee seeds and 29.7 g/100 g for borage seeds. The tocopherol content in oils ranged...
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Review of cigars and cigar-type products as potential sources of consumer exposure to heavy metals
PublicationThe popularity of cigars, growing since 1993, has not gone hand in hand with the increased interest of researchers in these products. Although the literature widely describes the harmfulness of tobacco and the content of toxic substances in tobacco products, the topic is often treated selectively as relating primarily to cigarettes and rarely extends to other products of the broadly defined tobacco industry. However, there is no...
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Impact and stretching standardized tests as useful tools for assessment of viscoelastic behavior for highly rubberized asphalt binder
PublicationAsphalt binder is generally identified as a brittle material at low service temperature or under high-speed load, and the brittleness becomes serious after weathering aging. Improving the toughness of asphalt binder through adding high-content of crumb tire rubber is an efficient method to solve this problem. Devulcanized rubber modified asphalt binder (DRMA) with different contents (15–40%) of devulcanized rubber (DR) were prepared...
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Properties of New Composite Materials Based on Hydroxyapatite Ceramic and Cross-Linked Gelatin for Biomedical Applications
PublicationThe main aim of the research was to develop a new biocompatible and injectable composite with the potential for application as a bone-to-implant bonding material or as a bone substitute. A composite based on hydroxyapatite, gelatin, and two various types of commercially available transglutaminase (TgBDF/TgSNF), as a cross-linking agent, was proposed. To evaluate the impacts of composite content and processing parameters on various...
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Gender as a moderator between Present-Hedonistic time perspective and depressive symptoms or stress during COVID-19 lock-down
PublicationAlthough numerous studies have addressed the impact of the COVID-19 lock-downs on psychological distress, scarce data is available relating to the role of Present-Hedonistic (PH) time perspective and gender differences in the development of depressive symptoms and stress during the period of strict social distancing. We hypothesized that gender would moderate the relationship between PH and depressiveness or stress levels, such...
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Prediction of pile shaft capacity in tension based on some direct CPT methods – Vistula Marshland test site
PublicationThis paper presents different CPT methodologies for the prediction of the pile shaft resistance in tension on the example of three reference screw piles of the Jazowa test site in Poland. The shaft capacity was estimated based on the cone resistance, sleeve friction and CPT excess pore water pressure. Three piles with a diameter of 0.4 m and the length...
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Antimicrobial resistance of fecal indicators in disinfected wastewater
PublicationThe main objective of the study was to assess the potential of three systems (UV irradiation, ozonation, and micro/ultrafiltration) operated in a pilot scale in removal of antimicrobial-resistant fecal bacteria from secondary effluent of the local wastewater treatment plant (700,000 population equivalent). The effectiveness of the processes was analysed using the removal ratio of fecal indicators (Escherichia coli and Enterococcus...
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The speciation of selected heavy metals in sewage sludge stabilized in reed basins
PublicationThe aim of the work was to determine influence of time on organic matter content, nutrients concentrations as well as speciation of selected heavy metals (Cd, Pb, Ni, Cr, Cu and Zn) in sewage sludge stabilized in reed basins during 7-15 years. The analyzed sewage sludge was collected from reed basins from four municipal WWTPs located in Denmark serving from 9 000 to 40 000 pe in Vallo, Rudkøbing, Nakskov and Helsinge. Sewage...
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Badania rozproszenia elektronów na cząsteczkach tlenu w szerokim zakresie kątów rozproszenia
PublicationCelem pracy były badania wzbudzenia cząsteczki tlenu od poziomów oscylacyjnych v=1 do v=5 stanu podstawowego X3 Sigma g- oraz stanu oscylacyjnego v=0 stanu wzbudzonego a1 delta g przeprowadzone dla energii elektronów padających równej 10eV oraz w szerokim zakresie kątów rozproszenia od 15 do 180 stopni. Aby wyznaczyć różniczkowe przekroje czynne dla tych stanów wzbudzonych, zmierzono różniczkowe przekroje czynne na rozproszenie...
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Influence of Giant Reed (Arundo Donax L.) Culms Processing Procedure on Physicochemical, Rheological, and Thermomechanical Properties of Polyethylene Composites
PublicationGiant reed (Arundo donax L.) is a plant species with a high growth rate and low requirements, which makes it particularly interesting for the production of different bioproducts, including natural fibers. This work assesses the use of fibers obtained from reed culms as reinforcement for a high-density polyethylene (HDPE) matrix. Two different lignocellulosic materials were used: i) shredded culms and ii) fibers obtained by culms...
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A multiparameter simulation-driven analysis of ship turning trajectory concerning a required number of irregular wave realizations
PublicationIn times of progressive automation of the marine industry, accurate modeling of ship maneuvers is of utmost importance to all parties involved in maritime transportation. Despite the existence of modern collisionavoidance algorithms using 6DOF motion models to predict ship trajectories in waves, the impact of stochastic realization of irregular waves is usually neglected and remains under-investigated. Therefore, herein, this phenomenon...
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Government in the metaverse: Requirements and suitability for providing digital public services
PublicationDigital government comprises all means to enable governments to interact with their constituents digitally. The metaverse provides a virtual reality environment where various activities can be carried out without physically visiting the places of interest, including the public authorities. Yet, how governments can use the metaverse is unknown. This paper aims to extend the understanding of the metaverse architecture requirements...
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Assessment of hearing in coma patients employing auditory brainstem response, electroencephalography, and eye-gaze-tracking
PublicationThe results of the study conducted by Tagliaferri et al. in 12 European countries indicate that the ratio of registered brain injury cases in Europe amounts to 150-300 per 100 000 people, with the European mean value of 235 cases per 100 000 people. The project presented in the paper assumes development of a combined metric of patients’ state remaining in coma by intelligent fusion of GCS (subjective Glasgow Coma Scale or its derivatives)...
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Evaluation of the glycerolysis process and valorisation of recovered polyol in polyurethane synthesis
PublicationIn this study, the glycerolysis of polyurethane (PU) foam and the applicability of obtained glycerolysate (GLY) for cast PUs were investigated. It was found that crude glycerine with purity grade of 84% might be successfully used for the glycerolysis. The optimal conditions were determined as follows: reaction time of 60 min at 220 °C using dibutyltin dilaurate catalyst (0.5%). Moreover, the purification of GLY by means of liquid-liquid...
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The Morphology, Structure, Mechanical Properties and Biocompatibility of Nanotubular Titania Coatings before and after Autoclaving Process
PublicationThe autoclaving process is one of the sterilization procedures of implantable devices. Therefore, it is important to assess the impact of hot steam at high pressure on the morphology, structure, and properties of implants modified by nanocomposite coatings. In our works, we focused on studies on amorphous titania nanotubes produced by titanium alloy (Ti6Al4V) electrochemical oxidation in the potential range 5–60 V. Half of the...
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Sonocatalytic degradation of tetracycline antibiotic using zinc oxide nanostructures loaded on nano-cellulose from waste straw as nanosonocatalyst
PublicationThe aim of the present investigation was the combination of ZnO nanostructures with nano-cellulose (NC) for the efficient degradation of tetracycline (TC) antibiotic under ultrasonic irradiation. The removal efficiency of 12.8% was obtained by the sole use of ultrasound (US), while the removal efficiency increased up to 70% by the US/ZnO treatment process. Due to the integration of ZnO nanostructures with NC, the removal efficiency...
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Ordered TiO2 nanotubes with improved photoactivity through self-organizing anodization with the addition of an ionic liquid: effects of the preparation conditions
PublicationModifying the geometric and surface parameters of oriented TiO2 nanotubes (NTs) is beneficial to the utilization of solar energy for chemical reactions, and this performance may be further improved. Thus, the effects of adding an ionic liquid (IL), 1-butylpiridinium chloride [BPy][Cl], and the effects of the water content and preparation conditions on the surface morphological, physicochemical, photocatalytic and photoelectrochemical...
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Przestrzenne aspekty produkcji i sprzedaży trolejbusów Solaris Trollino
PublicationKomunikacja trolejbusowa nie jest popularną formą transportu miejskiego w Polsce, ale polski producent taboru dla komunikacji - Solaris Bus & Coach - jest wiodącym producentem trolejbusów niskopodłogowych w Europie. W artykule przedstawiono ideę budowy trolejbusów, rozwój konstrukcji oraz postęp w produkcji i sprzedaży trolejbusów w latach 2001-2014. W analizowanym okresie polska firma wprowadziła na rynek nowy produkt – trolejbus...
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Bio polyetherurethane composites with high content of natural ingredients: hydroxylated soybean oil based polyol, bio glycol and microcrystalline cellulose
PublicationIn our study, we focused on obtaining bio-polyurethane composites using bio-components such as bio glycol, modified natural oil-based polyol, and microcrystalline cellulose (MCC). The pre-polymer method was used to prepare the bio polyurethane matrix. Prepolymer was synthesized using 4,4’-diphenylmethane diisocyanate (MDI) and a polyol mixture containing 50 wt.% of commercial polyether and 50 wt.% of hydroxylated soybean oil (H3)....
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The comparison of SrTi0.98Nb0.02O3–δ-CeO2 and SrTi0.98Nb0.02O3–δ-YSZ composites for use in SOFC anodes
PublicationComposites of Nb-doped strontium titanate mixed with yttria-stabilized zirconia or cerium oxide in 50:50, 70:30 and 85:15 weight ratios were evaluated as possible anode/electrolyte interface materials for solid oxide fuel cells in terms of chemical compatibility, electrical conductivity and mechanical properties. It has been shown that composite samples prepared by typical powder-mixing methods remain single-phase up to 1400°C....
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Homogeneity study of candidate reference material (contaminated soil) based on determination of selected metals, PCBs and PAHs
PublicationReference materials (RMs) are an indispensable part of QA/QC system and have played a critical role in the continual expansion of analytical capabilities of the analytical laboratories. The homogeneity study of the candidate for reference material is essential for the quality of reference material (certified reference material) used in quality assurance activities. The homogeneity study of candidate for reference materials of contaminated...
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Change in Heavy Metals Concentrations in Sediments Deposited in Retention Tanks in a Stream after a Flood
PublicationOur paper presents the results of heavy metal (HM) (Zn, Cu, Pb, Cd) content in bottom sediments from retention tanks along Oliwa Stream in Gdańsk, Poland, before a flood (BF) and after a flood (AF) 14-15 July 2016. The flood had a huge impact on the quality of bottom sediments and their displacement. The concentrations of HM differed significantly for research series conducted 3 months BF and 8 months AF. The concentration of Cu...
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Sludge Treatment Reed Beds (STRBs) as a Eco-solution of Sludge Utilization for Local Wastewater Treatment Plants
PublicationSewage sludge is a by-product of wastewater treatment processes. In Poland, the amout of sewage sludge has been still growing in recent years, due to inhencement of pollutants removal in wastewater treatment plants (WWTPs). One of the systems used to transform sewage sludge into fertilizer is a technology called Sludge Treatment Reed Beds (STRBs). Reed systems are periodically irrigated with sewage sludge with a low dry matter...
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Curing epoxy resin with anhydride in the presence of halloysite nanotubes: the contradictory effects of filler concentration
PublicationEpoxy resins can be cured with a wide variety of curing agents such as amines and anhydrides, but anhydride curing would be more favorable for research purpose because of epoxy-anhydride curing taking place slowly at room temperature. Incorporation of natural nanosized minerals into epoxy is of environmental importance. Halloysite nanotubes (HNTs) display chemical properties similar to those of silica and alumina, and hydroxyl...
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Low energy elastic scattering of electrons from hexafluoropropene (C3F6)
PublicationWe present cross sections from a joint experimental and theoretical study on elastic electron scattering from hexafluoropropene (C3F6) in the gas phase. The experimental results, using low energy electron spectroscopy, were obtained at incident electron energies of 0.5, 1, 1.5, 2, 3, 4, 5, 6, 10, 12, 15 and 20 eV, for scattering angles ranging from 10°to 130°. The theoretical method used in the computation of the integral, momentum...
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Analysing the impact of traffic incidents on express road traffic flow using FREEVAL
PublicationTraffic incidents occurring on motorways or express roads cause disruptions and deteriorate traffic conditions. The impact will differ depending on the type of incident, its duration and space blocked on the roadway and can be measured with e.g. average speed reduction, extension of travel time, time lost or overall costs of traffic disruptions. The aim of the paper is to analyse this impact, based on data from the Tri-City Ring...
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Wpływ mikrosfer – frakcji popiołu odpadów paleniskowych - na strukturę i właściwości fizyczno-mechaniczne betonu
PublicationGospodarka odpadowa od wielu lat budzi duże zainteresowanie. Mając na uwadze potrzebę dalszego rozszerzania bazy materiałów pochodzenia mineralnego w budownictwie, zwrócono uwagę na drobną frakcję ziarnową odpadów paleniskowych - mikrosfery. Przedstawione wyniki badań w monografii udzielają odpowiedzi czy zastosowanie mikrosfer popiołowych, jako substancji aktywnej w środowisku zaczynu cementowego, może w znaczący sposób modyfikować...
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Ground Tire Rubber Modified by Elastomers via Low-Temperature Extrusion Process: Physico-Mechanical Properties and Volatile Organic Emission Assessment
PublicationIn this paper, low-temperature extrusion of ground tire rubber was performed as a proecological waste tires recycling method. During this process, ground tire rubber was modified with constant content of dicumyl peroxide and a variable amount of elastomer (in the range: 2.5–15 phr). During the studies, three types of elastomers were used: styrene-butadiene rubber, styreneethylene/butylene-styrene grafted with maleic anhydride and...
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Towards evaluation of the Second Generation Intact Stability Criteria - examination of a fishing vessel vulnerability to surf-riding, based on historical capsizing
PublicationThe Second Generation Intact Stability Criteria (SGISC) are the latest achievements in the field of intact ship stability assessment. The criteria are the result of massive international cooperative efforts and extensive research that lasted more than 15 years. Even though they are based on a solid scientific foundation, the trial period has commenced to collect user experience and further validation. One of possible approaches...
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Thermal and Mechanical Behavior of Elastomers Incorporated with Thermoregulating Microcapsules
PublicationPolyurethane (PU) is one of the principal polymers in the global plastic market thanks to its versatility and continuous improvement. In this work, PU elastomeric materials having thermoregulating properties through the incorporation of microcapsules (mSD-(LDPE·EVA-RT27)) from low-density polyethylene and vinyl acetate containing paraffin®RT27 as PCM were produced. Elastomers were synthesized while varying the molar ratio [NCO]/[OH]...