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Electrochemically directed biofunctionalization of a lossy-mode resonance optical fiber sensor
PublicationIn this work, we present a direct electrochemical biofunctionalization of an indium-tin-oxide-coated lossy-mode resonance optical fiber sensor. The functionalization using a biotin derivative was performed by cyclic voltammetry in a 10 mM biotin hydrazide solution. All stages of the experiment were simultaneously verified with optical and electrochemical techniques. Performed measurements indicate the presence of a poly-biotin...
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Hybrid Technique for the EM Scattering Analysis with the Use of Ring Domain Decomposition
PublicationA hybrid technique combining finite-element and mode-matching methods for the analysis of scattering problems in open space is presented here. The main idea is based on impedance matrix descriptions of the boundary surrounding the discrete computational domain and combine it with external field described analytically. The discrete analysis, which is the most time- and memory-consuming, is limited here only to the close proximity...
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3D PCB package for GaN inverter leg with low EMC feature
PublicationThis paper presents the adaptation of a 3D integration concept previously used with vertical devices to lateral GaN devices. This 3D integration allows to reduce loop inductance, to ensure more symmetrical design with especially limited Common Mode emission, thanks to a low middle point stray capacitance. This reduction has been achieved by both working on the power layout and including a specific shield between the devices and...
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A case study of robust sliding mode control applied to inverted pendulum on a cart
PublicationA control problem of an inverted pendulum on a cart has been addressed in this paper. In particular, a synthesis of alternative sliding mode control for stabilisation of an inverted pendulum at an upper equilibrium point has been investigated. Hence, the feasibility of implementing the developed control system, taking into account primarily the friction of the cart against the gantry and the limited length of the gantry, in a real...
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On stress singularity near the tip of a crack with surface stresses
PublicationIn the framework of the simplified linear Gurtin–Murdoch surface elasticity we discuss a singularity of stresses and displacements in the vicinity of a mode III crack. We show that inhomogeneity in surface elastic properties may significantly affect the solution and to change the order of singularity. We also demonstrate that implicitly or explicitly assumed symmetry of the problem may also lead to changes in solutions. Considering...
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Recent advances in hydrogen production from biomass waste with a focus on pyrolysis and gasification
PublicationThis paper presents the results research on the optimal fuel compositions and the control parameters of the spark ignition engine fueled with syngas-biogas-hydrogen for the purpose of setting up a flexible electronic control unit for the engine working in a solar-biomass hybrid renewable energy system. In syngas-biogas-hydrogen mixture, the optimal content of hydrogen and biogas is 20% and 30%, respectively. Exceeding these thresholds,...
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Comprehensive methodology for Staphylococcus aureus lipidomics by liquid chromatography and quadrupole time-of-flight mass spectrometry
PublicationStaphylococcus aureus is a common pathogen known to cause relatively minor infections as well as severe disorders in humans. Although there is fair amount of published data concerning various aspects of its biology, epidemiology, genetics, etc., there is still a scarce amount of data presenting reliable and thorough investigations regarding high-throughput analysis of total S. aureus lipid content. Therefore, the aim of this study...
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Soft-mode enhanced type-I superconductivity in LiPd2Ge
PublicationThe synthesis, crystal structure, and physical properties (magnetization, resistivity, heat capacity) in combination with theoretical calculations of the electronic structure and phonon properties are reported for intermetallic compounds LiPd2X (X = Si, Ge, and Sn). LeBail refinement of powder x-ray diffraction data confirms that all compounds belong to the Heusler family (space group Fm-3m, No. 225). The lattice parameter increases...
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Towards a multi-basin SWAT model for the migration of nutrients and pesticides to Puck Bay (Southern Baltic Sea)
PublicationBackground This paper analyzes the impact of changes in fertilization on crop yields and the runoff of nutrients from a small agricultural catchment (176 km2) to a shallow bay, using the SWAT model. Puck Bay is part of the Gulf of Gdansk and belongs to the Baltic Sea. The whole area of Puck Bay (364 km2) is protected (Natura 2000) yet despite this it suffers from eutrophication problems due to the relatively minimal depth and...
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Flexible syngas-biogas-hydrogen fueling spark-ignition engine behaviors with optimized fuel compositions and control parameters
PublicationThis paper presents the results research on the optimal fuel compositions and the control parameters of the spark ignition engine fueled with syngas-biogas-hydrogen for the purpose of setting up a flexible electronic control unit for the engine working in a solar-biomass hybrid renewable energy system. In syngas-biogas-hydrogen mixture, the optimal content of hydrogen and biogas is 20% and 30%, respectively. Exceeding these thresholds,...
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Approximate solution for Euler equations of stratified water via numerical solution of coupled KdV system
PublicationWe consider Euler equations with stratified background state that is valid for internal water waves. The solution of the initial-boundary problem for Boussinesq approximation in the waveguide mode is presented in terms of the stream function. The orthogonal eigenfunctions describe a vertical shape of the internal wave modes and satisfy a Sturm-Liouville problem. The horizontal profile is defined by a coupled KdV system which is...
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A Novel [4+2] Cycloaddition Reaction Involving Lawesson’s Reagent. Structure and Specific Fragmentations of a New Cyclic 1,2-Thiaphosphinane-4-one
PublicationA crude morpholine enamine of acetone treated with Lawesson’s reagent unexpectedly yielded a six-membered thiaphosphinane-4-one. This compound is the first example of a new class of heterocycles. It has been proven that it is formed from 4-methyl-2-morpholino-1,3-pentadiene which is usually present in crude morpholine enamine batches. A mechanism of this regioselective reaction was postulated and a characteristic chair-like conformation...
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Destructive impact of PWM inverters on traction AC motors
PublicationThe electric traction drives with an AC motor fed by a frequency converter are used more and more often nowadays. The most significant side effects, of a converter's output voltage forming PWM method for AC motor windings, are steep voltage changes, which can initiate several destructive phenomena. The paper presents the adverse influence of a converter common mode voltage on the motor windings's increased voltage exposure and...
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Destructive Consequences of PWM Inverter Feeding for Traction AC Motors
PublicationThe electric traction drives with an AC motor fed by a frequency converter are used more and more often nowadays. The most significant side effects, of a converter's output voltage forming PWM method for AC motor windings, are steep voltage changes, which can initiate several destructive phenomena. The paper presents the adverse influence of a converter common mode voltage on the motor windings' increased voltage exposure and the...
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Influence of statistical errors on damage detection based on structuralflexibility and mode shape curvature
PublicationDamage detection procedures based on measured natural frequencies and building structure mode shapes are discussed in this paper. Modal curvature and structural flexibility approaches are tested. Attention is paid to the modal identification errors that influence damage detection. This problem is studied using a computer simulation of a simple supported beam. For practical cases, the peak picking methodand its statistical errors...
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A measurement system for nonlinear surface spectroscopy with an atomic force microscope during corrosion process monitoring
PublicationIn addition to traditional imaging the surface, atomic force microscopy (AFM) enables wide variety of additional measurements. One of them is higher harmonic imaging. In tapping mode the nonlinear contact between tip and specimen results in higher frequency vibrations. More information available from the higher harmonics analysis proves to be helpful for more detailed imaging. Such visualization is espe-cially useful for heterogeneous...
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Implementation of the digital receiver in multibeam long-range sonar
PublicationThe article presents the implementation of a digital receiver in multibeam long - range sonar. Developed by the authors of the article, the implementation was part of sonar modernisation on large Polish Navy ships. The article explains the structure of the receiver, its design details and requirements affecting the architecture. The technical solutions regarding the equipment and signal processing algorithms for determining receiving...
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Standing Waves and Acoustic Heating (or Cooling) in Resonators Filled with Chemically Reacting Gas
PublicationStanding waves and acoustic heating in a one-dimensional resonator filled with chemically reacting gas, is the subject of investigation. The chemical reaction of A ! B type, which takes place in a gas, may be reversible or not. Governing equations for the sound and entropy mode which is generated in the field of sound are derived by use of a special mathematical method. Under some conditions, sound waves propagating in opposite...
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Assessment of copper surface coverage with corrosion inhibitor using AFM-based local electrical measurements
PublicationThe paper presents a new method of assessment of metal surface coverage with corrosion inhibitor and thus of inhibitor protective performance. It is based on the atomic force microscopy measurement performed in a contact mode. Apart from topography images the proposed approach allows acquisition of local DC maps and local electrical impedance spectra via application of DC bias voltage or AC perturbation signal between the conductive...
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Chosen Analysis Results Of The Prototype Multicell Piezoelectric Motor
PublicationThis paper presents the design, modeling and tests of the prototype multicell piezoelectric motor (MPM). A new concept of the electromechanical structure of the considered prototype is based on three rotating-mode actuators. The electromechanical structure of each actuator has been considered as an independent one - referred to as a “single cell” (single actuator). Combined three resonant actuators generate three traveling waves...
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Niekorzystny wpływ przekształtnikowego zasilania PWM na silniki asynchroniczne trakcyjne
PublicationThe electric traction drives with an AC motor fed by a frequency converter are used more and more often nowadays. The most significant side effects, of a converter's output voltage forming PWM method for AC motor windings, are steep voltage changes, which can initiate several destructive phenomena. The paper presents the adverse influence of a converter common mode voltage on the motor windings' increased voltage exposure and the...
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Impedance monitoring of corrosion degradation of plasma electrolytic oxidation coatings (PEO) on magnesium alloy
PublicationImpedance technique based on continuous multisinusoidal current perturbation was used to explain degradation process of plasma electrolytic oxidation coatings (PEO) on magnesium alloy. An obtained impedance spectrum was fitted by electrical equivalent circuit to describe properties of conversion layer on magnesium alloy. Additionally, galvanostatic mode maintained during experiment, with DC current equal to zero, allowed to achieve...
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Jahn-Teller and related conical intersections in the benzene radical cation and the monofluoro derivate
PublicationThe multi-state multi-mode vibronic interactions in the benzene radical cation and its monofluoro derivative have been investigated theoretically, based on high-level electronic structure calculations for the system parameters and a quantum treatment of the nuclear motion. The available experimental data are well reproduced. The interplay of different vibronic coupling mechanisms is pointed out leading to multiple nonadiabatic...
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New concept and analysis of the multicell piezoelectric motor
PublicationThis work presents the design, modeling and tests of the prototype multicell piezoelectric motor (MPM). A new concept of the electromechanical structure of the considered prototype is based on three rotating-mode actuators. The electromechanical structure of each actuator has been considered as an independent one - referred to as a ”single cell” (single actuator). Combined three resonant actuators generate three traveling waves...
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Surface quality control of a thin SiN layer by optical measurements
PublicationFiber optic interferometers have a wide range of applications, including biological and chemical measurements. Nevertheless, in the case of a reflective interferometer setup, standard silver mirrors cannot be used in every measurement, due to their chemical activity. This work investigates the surface quality of a thin optical layer of silicon nitride (SiN), which can serve as an alternative material for silver mirrors. We present...
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Distance learning trends: introducing new solutions to data analysis courses
PublicationNowadays data analysis of any kind becomes a piece of art. The same happens with the teaching processes of statistics, econometrics and other related courses. This is not only because we are facing (and are forced to) teach online or in a hybrid mode. Students expect to see not only the theoretical part of the study and solve some practical examples together with the instructor. They are waiting to see a variety of tools, tutorials,...
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Local basis function estimators for identification of nonstationary systems
PublicationThe problem of identification of a nonstationary stochastic system is considered and solved using local basis function approximation of system parameter trajectories. Unlike the classical basis function approach, which yields parameter estimates in the entire analysis interval, the proposed new identification procedure is operated in a sliding window mode and provides a sequence of point (rather than interval) estimates. It is...
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The influence of combination of binding agents on fatigue properties of deep cold in-place recycled mixtures in Indirect Tensile Fatigue Test (ITFT)
PublicationThe publication presents fatigue properties of cold recycled mixtures for eight combinations of binding agents (cement and bituminous emulsion). Cold recycled mixtures were evaluated in Indirect Tensile Fatigue Test (ITFT) at the temperature of 20 C in controlled stress mode. As a function of horizontal stress, fatigue life is strongly influenced by combination of the binding agents. When fatigue life is analyzed as a function...
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approximation of photonic crystal fibres with large air holes by the step index fibre model
PublicationAn equivalent step index fibre with a silica core and air cladding is used to model photonic crystal fibres with large air holes. We model this fibre for linear polarisation (we focus on the lowest few transverse modes of the electromagnetic field). The equivalent step index radius is obtained by equating the lowest two eigenvalues of the model to those calculated numerically for the photonic crystal fibres. The step index parameters...
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An optimal sliding mode control based on immune-wavelet algorithm for underwater robotic manipulator
PublicationIn this paper, a robust optimal Sliding Mode Controller (SMC) based on new algorithm of Artificial Immune System (AIS) is proposed for trajectory tracking of underwater manipulators. A new AIS algorithm is used to derive optimal values of surface parameters and boundary layer thickness in SMC with considering minimum torques and error. Surface parameters and boundary layer thickness are considered as antibody in AIS and Morlet...
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Zmodyfikowana metoda prognozowania rezultatów nadzorowania drgań narzędzie--przedmiot obrabiany. W: Projektowanie mechatroniczne. Zagadnienia wybrane. Praca zbiorowa pod red. T. Uhla. Kraków: Kated. Robotyki i Dynam. Masz.AGH**2003 s. 125-134, 3 rys. 1 tab. bibliogr. 6 poz.
PublicationW pracy przedstawiono zmodyfikowaną metodę prognozowania rezultatów nadzoro-wania drgań narzędzie-przedmiot obrabiany za pomocą sterowanej programowo prędkości obrotowej wrzeciona. Istotą modyfikacji jest uwzględnienie w mode-lu złożoności geometrycznej narzędzia oraz efektu rozproszenia energii pro-cesu skrawania. Podano opis dynamiki skrawania niestacjonarnego modelu obli-czeniowego, oraz sposobu nadzorowania. Zamieszczono...
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Design and modeling of the piezoelectric motor based on three resonance actuators
PublicationThis paper describes a piezoelectric motor which combines advantages from two existing piezoelectric motors topologies. The research work presents the design, simulations and measurements of the piezoelectric motor with three rotation-mode actuators. The aim of the project was to obtain the high speed piezoelectric motor. Other advantages of this conception are blocking torque, short response times, the ability to work in a hostile...
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Acoustic Heating Produced in the Thermoviscous Flow of a Shear-Thinning Fluid
PublicationThis study is devoted to the instantaneous acoustic heating of a shear-thinningfluid. Apparent viscosity of a shear-thinning fluid depends on the shear rate. Thatfeature distinguishes it from a viscous Newtonian fluid. The special linear combi-nation of conservation equations in the differential form makes it possible to derivedynamic equations governing both the sound and non-wave entropy mode inducedin the field of sound. These...
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Determination of Failure Causes of a Steam Turbine Casing
PublicationThe paper presents results of research and failure analysis undertaken to determine failure causes of a steam turbine casing. After 130,000 hours of service the crack in a outer shell of the turbine casing was found. The inner shell of the casing was made of cast steel grade G21CrMoV5-7, and the outer shell of grade G20CrMo4-5. Following research were performed in order to determine causes of the casing failure: chemical analysis;...
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Common methods for the chiral determination of amphetamine and related compounds I. Gas, liquid and thin-layer chromatography
PublicationThis article reviews the most common, useful methods for the chiral determination of amphetamine (AM) and AM-deriveddesigner drugs in different of matrix, including blood, hair, urine, medicaments or standard solutions, taking into considerationarticles published in the past 15 years. We consider chromatographic methods (e.g., gas, liquid, high-performance liquid, and thinlayer). We describe several types of chiral derivatization...
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Quasi-resonant DC-link voltage inverter with enhanced zero-voltage switching control
PublicationA new topology modification of the parallel quasi-resonant circuit for a dc-link voltage inverter enables regulation of the zero voltage dc-link subperiods and the dc-link voltage gradient settings. The proposed circuit is based on four MOSFET switches with free-wheeling diodes for controlled quasi-resonant recharging between L-C tank in order to assure inverter zero voltage switching (ZVS) conditions. Design optimization of the...
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Fiber optic microsphere with a ZnO thin film for potential application in a refractive index sensor – theoretical study
PublicationOptical fiber sensors of refractive index play an important role in analysis of biological and chemical samples. This work presents a theoretical investigation of spectral response of a fiber optic microsphere with a zinc oxide (ZnO) thin film deposited on the surface and evaluates the prospect of using such a structure for refractive index sensing. A microsphere is fabricated by an optical fiber tapering method on the base of...
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Shielded coupled strip and slot guides with a thin omega pseudochiral medium layer
PublicationA method of moments combined with mode matching technique is applied to analyze the shielded coupled strip and slot line structures containing a thin plate of Omega pseudochiral medium. The boundary problems are simplified by introducing for omega medium the approximate continuity conditions. Such mathematical model allows to examine the field displacement effect appearing in the considered guide resulting from the coupling between...
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Hybrid Method Analysis of Unshielded Guiding Structures
PublicationA combination of mode matching, finite element methods and generalized impedance matrix is presented in a context of propagation problems for open guiding structures. The computational domain is divided into two regions: the first one is a circular cylinder containing whole guiding structure and the second one surrounds this artificial cylinder. The impedance matrix is calculated with the use of finite element method in the first...
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The Reactivity of the Imine Bond within Polynuclear Nickel(II) Complexes
PublicationThree novel Ni complexes with the Schiff base ligand 2-methoxy-6-(E-2-pyridyliminomethyl)-phenol (L1) are described. In comparison with the similar 2-(pyridine-2-ylimino-methyl)phenol (pymp), the mode of coordination of L1 is altered due to the presence of methoxy substituent introducing the sterical hindrance. During the synthesis of the complexes, partial hydrolysis of the ligand was observed. Since such immediate hydrolysis...
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Comparison of hydrophilic interaction and reversed phase liquid chromatography coupled with tandem mass spectrometry for the determination of eight artificial sweeteners and common steviol glycosides in popular beverages
PublicationHydrophilic interaction liquid chromatography (HILIC) coupled with tandem mass spectrometry (MS/MS) was used to separate artificial and natural sweeteners approved for use in European Union (EU). Among three tested HILIC columns (BlueOrchid PAL-HILIC, Ascentis Express Si and Acclaim™ Trinity™ P2) the last one was selected for the development of HILIC method due to the best results obtained with it. Early eluting and coeluting compounds...
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Application of dynamic headspace and gas chromatography coupled to mass spectrometry (DHS-GC-MS) for the determination of oxygenated volatile organic compounds in refinery effluents
PublicationThe paper presents a new procedure for the determination of oxygenated volatile organic compounds (O-VOCs) in postoxidative effluents from the production of petroleum asphalt using dynamic headspace coupled to gas chromatography-mass spectrometry in the selected ion monitoring (SIM) mode (DHSGC-MS). Among the GC capillary columns tested, a polar SLB-IL111 column with the ionic liquid stationary phase was found to be superior due...
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A spline-based FE approach to modelling of high frequency dynamics of 1-D structures
PublicationIn this paper a computational methodology leading to the development of a new class of FEs, based on the application of continuous and smooth approximation polynomials, being splines, has been presented. Application of the splines as appropriately defined piecewise elemental shape functions led the authors to the formulation of a new approach for FEM, named as spFEM, where contrary to the well-known NURBS approach, the boundaries...
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Modeling protein structures with the coarse-grained UNRES force field in the CASP14 experiment
PublicationThe UNited RESidue (UNRES) force field was tested in the 14th Community Wide Experiment on the Critical Assessment of Techniques for Protein Structure Prediction (CASP14), in which larger oligomeric and multimeric targets were present compared to previous editions. Three prediction modes were tested (i) ab initio (the UNRES group), (ii) contact-assisted (the UNRES- contact group), and (iii) template-assisted (the UNRES-template...
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Microfluidically Frequency-Reconfigurable Compact Self-Quadruplexing Tunable Antenna with High Isolation Based on Substrate Integrated Waveguide
PublicationThis communication presents a novel concept of microfluidically frequency-reconfigurable self-quadruplexing tunable antenna for quad-band applications. At the initial design stage, a substrate-integrated square cavity is divided into four unequal quarter-mode cavity resonators by inserting an X-shaped slot on the top surface of the cavity. Applying four 50-ohm microstrip feed-lines to these four quarter-mode cavity resonators enables...
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Electrical and mechanical characterization of two-phase alloys by means of scanning probe microscopy in dynamic impedance spectroscopy mode
PublicationDynamic impedance spectroscopy, evaluated for measuring non-stationary systems, was used in combination with scanning probe microscope. Using this approach, localized impedance measurements in the AFM contact mode could be carried out. Additionally, impedance–force curves were made at each phase of investigated materials to illustrate the relation between impedance and the force applied to a probe. Therefore, correlation of electrical...
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Implementation of DEIS for reliable fault monitoring and detection in PEMFC single cells and stacks
PublicationDynamic Electrochemical Impedance Spectroscopy (DEIS) was presented as novel method for diagnostic and monitoring of PEMFC stack and single cells operation. Impedance characteristics were obtained simultaneously with current - voltage characteristics for stack and each individual cell. Impedance measurements were performed in galvanodynamic mode. It allowed to compare performance of each cell and identification of faulty cell operation...
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Electromagnetic plane wave scattering from a cylindrical object with an arbitrary cross section using a hybrid technique
PublicationA hybrid technique combining finite-element and mode-matching methods for the analysis of scattering problems in open and closed areas is presented. The main idea of the analysis is based on the utilization of the finite-element method to calculate the post impedance matrix and combine it with external excitation. The discrete analysis, which is the most time- and memory-consuming, is limited here only to the close proximity of...
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The Concept of a Methodology for Selecting the Optimal Parameters of Heat Received from a Nuclear Power Plant Operating in a Partial Cogeneration Mode
PublicationThe paper presents the concept of the objective function which is to allow the selection of optimal parameters of the district heating system using a nuclear power plant operating in partial cogeneration mode. The concept is based on research carried out a number of years ago. The size of annual expenses was proposed as the objective function, which allows to compare the operation of a nuclear power plant in partial cogeneration...
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Crystal growth and properties of a binary intermetallic ZrBi2 compound
PublicationSingle crystals of ZrBi2 were grown by a self-flux method. The material adopts TiAs2 structure type with lattice parameters: a = 10.233(4) Å, b = 15.581(2) Å, c = 3.994(5) Å. Crystals of ZrBi2 were studied by means of magnetic susceptiblity, specific heat and resistivity measurements. The compound reveals a metallic-like behavior (RRR = 30). The Sommerfeld coefficient equals γ = 1.59(16) mJ mol-1 K-2 and Debye temperature ΘD =...