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Thermostability and photophysical properties of mixed-ligand carboxylate/benzimidazole Zn(II)-coordination polymers
PublicationThe reaction between Zn(NO3)2*6H2O or Zn(CH3COO)2*2H2O and isophthalic acid (1,3-H2bdc) in the presence of benzimidazole (Hbzim) in dimethylformamide (DMF)/ethanol (EtOH)/H2O solvent mixture at room temperature yielded two structurally different coordination polymers: [Zn2(1,3-bdc)2(Hbzim)2] (1) and [Zn2(1,3-bdc)(bzim)2] (2). (1) is a 2D-layered framework with a molecule of benzimidazole coordinated to the Zn center, whereas (2)...
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Małgorzata Szczerska prof. dr hab. inż.
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Pressure in charge. Neglected parameter in hydrothermal synthesis turns out to be crucial for electrochemical properties of ammonium vanadates
PublicationAmmonium vanadates are of great interest as they exhibit unusual electrical and sensory properties.(NH4)2V6O16and (NH4)2V10O25$8H2O with various morphology were obtained in the hydrothermalsynthesis under controlled temperature and pressure. It was shown, that the pure (NH4)2V10O25$8H2Owas obtained under 50 bar of initial pressure, whereas lower pressure lead to the mixture of twocompounds. The influence of the pressure was studied...
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Physical and sealing properties of BaO–Al2O3–SiO2–CaO–V2O5 glasses for solid oxide fuel cell applications
PublicationIn this study, the properties of BaO–Al2O3–SiO2 (SAB) glasses incorporated with CaO and V2O5 as the network modifier and additive, respectively, are evaluated. The electrical resistivities of the glasses decrease upon the addition of CaO but increase upon increasing their V2O5 content because the V5+ species lower the ionic mobility of the glasses. The addition of V2O5 improves the wettability of the glasses on the Crofer 22 APU...
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Mechanical Properties and Wear Susceptibility Determined by Nanoindentation Technique of Ti13Nb13Zr Titanium Alloy after “Direct Laser Writing”
PublicationLaser treatment has often been applied to rebuild the surface layer of titanium and its alloys destined for long-term implants. Such treatment has always been associated with forming melted and re-solidified thin surface layers. The process parameters of such laser treatment can be different, including the patterning of a surface by so-called direct writing. In this research, pulse laser treatment was performed on the Ti13Nb13Zr...
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Obtaining and Characterization of the PLA/Chitosan Foams with Antimicrobial Properties Achieved by the Emulsification Combined with the Dissolution of Chitosan by CO2 Saturation
PublicationA new method of obtaining functional foam material has been proposed. The materials were created by mixing the poly lactic acid (PLA) solution in chloroform, chitosan (CS) dissolved in water saturated with CO2 and polyethylene glycol (PEG), and freeze-dried for removal of the solvents. The composite foams were characterized for their structural (SEM, FT-IR, density, porosity), thermal (DSC), functional (hardness, elasticity, swelling...
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The correlation between nutritional and health potential and antioxidant properties of raw edible oils from cultivated and wild plants
PublicationThe nutritional properties and health potential of oils from 15 various cultivated and wild plants were investigated on the basis of the fatty acids profiles, total carotenoids and tocopherols content, antioxidant properties and health potential indexes such as atherogenicity index (AI). The oil contents of the plants varied between 0.9 g/100 g for lychee seeds and 29.7 g/100 g for borage seeds. The tocopherol content in oils ranged...
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Obtaining and Characterization of the PLA/Chitosan Foams with Antimicrobial Properties Achieved by the Emulsification Combined with the Dissolution of Chitosan by CO2 Saturation
PublicationA new method of obtaining functional foam material has been proposed. The materials were created by mixing the poly lactic acid (PLA) solution in chloroform, chitosan (CS) dissolved in water saturated with CO2 and polyethylene glycol (PEG), and freeze-dried for removal of the solvents. The composite foams were characterized for their structural (SEM, FT-IR, density, porosity), thermal (DSC), functional (hardness, elasticity, swelling...
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The comparison of antioxidant properties and nutrigenomic redox-related activities of vitamin C, C-vitamers, and other common ascorbic acid derivatives
PublicationThe term ‘vitamin C’ describes a group of compounds with antiscorbutic activity of L-ascorbic acid (AA). Despite AA’s omnipresence in plant-derived foods, its derivatives have also been successfully implemented in the food industry as antioxidants, including the D-isomers, which lack vitamin C activity. This study aimed to determine the relationship between redox-related activities for five derivatives of AA using electrochemical,...
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The electrical properties mesurements of SOFC with Ce0.9Cu0.1O2-s functional layer
Open Research DataThe dataset includes the electrical properties mesurements of SOFC with Ce0.9Cu0.1O2-s layer. Samples were produced using aqueous soft chemistry methods (microemulsion method) and applied in form of a layer onto the anode of the commercial SOFC. The SOFC was working under biogas feeding at 750oC. The layers were sintered at 1100oC.
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The electrical properties mesurements of SOFC with Ce0.9Co0.1O2-s functional layer
Open Research DataThe dataset includes the electrical properties mesurements of SOFC with Ce0.9Co0.1O2-s layer. Samples were produced using aqueous soft chemistry methods (microemulsion method) and applied in form of a layer onto the anode of the commercial SOFC. The SOFC was working under biogas feeding at 750oC. The layers were sintered at 1100oC.
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The electrical properties mesurements of SOFC with Ce0.8Co0.1Cu0.1O2-s functional layer
Open Research DataThe dataset includes the electrical properties mesurements of SOFC with Ce0.8Co0.1Cu0.1O2-s layer. Samples were produced using aqueous soft chemistry methods (microemulsion method) and applied in form of a layer onto the anode of the commercial SOFC. The SOFC was working under biogas feeding at 750oC. The layers were sintered at 1100oC.
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The electrical properties mesurements of SOFC with Ce0.8Co0.15Cu0.05O2-s functional layer
Open Research DataThe dataset includes the electrical properties mesurements of SOFC with Ce0.8Co0.15Cu0.05O2-s layer. Samples were produced using aqueous soft chemistry methods (microemulsion method) and applied in form of a layer onto the anode of the commercial SOFC. The SOFC was working under biogas feeding at 750oC. The layers were sintered at 1100oC.
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Identification and properties of the psychrophilic bacterium Desulfolatea psychrophila single-stranded DNA binding proteins
PublicationTo study the biochemical properties of SSB from Desulfolatea psychrophila (DpsSSB), we have cloned the ssb genes obtained by PCR and have developed Escherichia coli overexpression systems. The gene consists of an open reading frame of 426 nucleotides encoding SSB protein of 142 amino acids with a calculated molecular mass of 15.6 kDa and it is the smallest known bacterial SSB protein indentified to date. The amino-acid sequence...
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Crystal structures of aminotransferases Aro8 and Aro9 from Candida albicans and structural insights into their properties
PublicationAminotransferases catalyze reversibly the transamination reaction by a ping-pong bi-bi mechanism with pyridoxal 5′-phosphate (PLP) as a cofactor. Various aminotransferases acting on a range of substrates have been reported. Aromatic transaminases are able to catalyze the transamination reaction with both aromatic and acidic substrates. Two aminotransferases from C. albicans, Aro8p and Aro9p, have been identified recently, exhibiting...
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Eu3+ doped tellurite glass ceramics containing SrF2 nanocrystals: Preparation, structure and luminescence properties
PublicationEu3+ doped tellurite glass ceramics containing SrF2 nanocrystals were prepared using melt quenching technique and subsequent heat treatment of glass in 370 °C for different time periods. Thermal properties of glass matrix have been determined based on DSC measurements. XRD and XPS results confirmed formation of SrF2 nanocrystals in glass matrices after annealing at 370 °C. FTIR studies revealed absorption bands in the range of...
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Effect of slightly crosslinked butyl rubber and compatibilizer additives on properties of recycled polyethylene-ground tire rubber blends
PublicationSlightly crosslinked butyl rubber, (PhMe2CO)(2) and maleic anhydride were added as compatibilizer to the recycled polyethylene-ground tire rubber blends. Recycled postprodn. and postconsumer (shredded bottle caps) polyethylene wastes were used. The thermoplastic compns. were studied for statistic and dynamic mech. properties and morphol. The addn. of butyl rubber resulted in a decrease of the tensile strength and hardness of the...
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Emission and properties of airborne wear particles from train brake friction materials based on novolac phenolic resins and butadiene rubbers
PublicationThe emission of airborne particulate matter from a train brake depends on the formulation of its friction material. This study investigates the emission and properties of wear particles from train brake friction materials based on straight or resorcinol-modified novolac phenolic resin and nitrile or styrene butadiene rubber used as binding ingredients. The wear particles are generated by a pin-on-disc tribomachine inside an aerodynamic...
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Mechanical, durability, depolluting and electrical properties of multifunctional mortars prepared with commercial or waste carbon-based fillers
PublicationCarbon-based fillers from industrial wastes and commercial ones were compared to improve the properties of lime-based mixes. As commercial fillers, graphene nanoplatelets and activated carbon were used, whereas as industrial wastes a char obtained by the gasification of biomasses and a used foundry sand were chosen. Carbon-based wastes were found to be a good cost-effective alternative to commercial carbon based fillers to increase...
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The In-House Method of Manufacturing a Low-Cost Heat Pipe with Specified Thermophysical Properties and Geometry
PublicationVarious types of heat pipes are available to purchase off the shelf, from various manufacturers, but most of them have strictly defined geometry and technical parameters. However, when there is a need to use a heat pipe (HP) with an unusual size and shape or working conditions other than the standard ones, it becomes very costly to order them from manufacturers, especially in small quantities, and only a few producers are willing...
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Experimental study on the effect of selected sterilization methods on mechanical properties of polylactide FFF specimens
PublicationPurpose: Biodegradable polymers are widely used in personalized medical devices or scaffolds for tissue engineering. The manufacturing process should be finished with sterilization procedure. However, it is not clear how the different sterilization methods have an impact on the mechanical strength of the three-dimensional (3D)-printed parts, such as bone models or personalized mechanical devices. This paper aims to present the...
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Determination of flow properties of a pneumatic hose from changes in air pressure in a tank being emptied or filled by a differently configured pneumatic line
Open Research DataThe aim of the study was to determine the flow properties of various pneumatic hoses. The experiments were to measure the pressure changes in a being filled or emptied tank for a differently configured pneumatic line, including pneumatic hoses of different length and diameter. Three test configurations were used: (1) pressure source -> pneumatic...
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Structure and properties comparison of poly(ether-urethane)s based on nonpetrochemical and petrochemical polyols obtained by solvent free two-step method
PublicationThe application of thermoplastic polyurethanes (TPU) is becoming more and more extensive, and the decreasing of used petrochemical monomers and reduction of energy for the polymerization and processing processes is getting increasingly important. In this paper, we confirmed the positive influence of high bio-based monomers contents (by replacing petrochemical polyol and glycol by bio-based counterparts) on processing and properties...
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The Chemical and Biological Properties of Nanohydroxyapatite Coatings with Antibacterial Nanometals, Obtained in the Electrophoretic Process on the Ti13Zr13Nb Alloy
PublicationThe risk of an early inflammation after implantation surgery of titanium implants has caused the development of different antimicrobial measures. The present research is aimed at characterizing the effects of nanosilver and nanocopper dispersed in the nanohydroxyapatite coatings, deposited on the Ti13Zr13Nb alloy, and on the chemical and biological properties of the coatings.The one-stage deposition process was performed by the...
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Effect of TiO2 Concentration on Microstructure and Properties of Composite Cu–Sn–TiO2 Coatings Obtained by Electrodeposition
PublicationIn this work, Cu–Sn–TiO2 composite coatings were electrochemically obtained from a sulfate bath containing 0–10 g/L of TiO2 nanoparticles. The effect of TiO2 particles on kinetics of cathodic electrodeposition has been studied by linear sweep voltammetry and chronopotentiometry. As compared to the Cu–Sn alloy, the Cu–Sn–TiO2 composite coatings show rougher surfaces with TiO2 agglomerates embedded in the metal matrix. The highest...
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Thermal, electrical, and magnetic properties of Fe2O3–PbO–SiO2 glass prepared by traditional melt-quenching and twin roller fast-cooling methods
PublicationIn this study, Fe–Pb–Si oxide glasses containing between 12.5 and 17.5 mol% Fe2O3 were prepared using two different methods comprising traditional melt-quenching and twin roller fast-cooling techniques. The topography and structure of the materials obtained were characterized by X-ray powder diffraction and scanning electron microscopy. All of the materials were found to be amorphous. The topography of most of the glasses comprised...
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STRUCTURE AND MAGNETIC PROPERTIES OF Bi5Ti3FeO15 CERAMICS PREPARED BY SINTERING, MECHANICAL ACTIVATION AND EDAMM PROCESS. A COMPARATIVE STUDY
PublicationThree different methods were used to obtain Bi5Ti3FeO15 ceramics, i.e. solid-state sintering, mechanical activation (MA) with subsequent thermal treatment, and electrical discharge assisted mechanical milling (EDAMM). The structure and magnetic properties of produced Bi5Ti3FeO15 samples were characterized using X-ray diffraction and Mössbauer spectroscopy. The purest Bi5Ti3FeO15 ceramics was obtained by standard solid-state sintering...
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The impact of interactions between polyphenolic antioxidants on the redox-related chemical and biological properties of their mixtures – the extension of food synergy concept.
PublicationThe results of studies indicate that chemopreventive efficiency of isolated phytochemicals is lower than that of polyphenol-rich foods. This discrepancy has been ascribed to the food synergy concept that assumes additive or even synergistic influence of different food ingredients on human health. The results presented in the dissertation made it possible to propose an alternative and innovative explanation of these observations. The...
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Synthesis, structure and properties of poly(ester-urethane)s obtained using bio-based and petrochemical1,3-propanediol and 1,4-butanediol
PublicationIn this paper, the poly(ester-urethane)s obtained using petrochemical and bio-based chain extenders were prepared and characterized. The influence of glycols’ origin on the chemical structure, mechanical and thermal properties of the prepared polyurethanes was studied. The materials were synthesised by prepolymer method. The first step involved the reaction of α,ω-dihydroxy(ethylene-butylene adipate (POLIOS 55/20) with 4,4’-diphenylmethane...
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Investigation of poly(3,4-ethylenedioxythiophene) deposition method influence on properties of ion-selective electrodes based on bis(benzo-15-crown-5) derivatives
PublicationGlassy carbon electrodes modified by conductive polymers and membrane with derivatives of bis(benzo-15-crown-5) were tested as solid contact ion selective electrodes for K+ ions concentration determination. PEDOT with PSS, Cl- and ClO4- counter ions was electrochemically deposited onto glassy carbon substrates using four different electrochemical approaches (potentiostatic, galvanostatic, potentiodynamic and potentiostatic pulses)....
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Effect of temperature and ionic strength on volumetric and acoustic properties of solutions of urea alkil derivatives in aqueous NaCl
PublicationThe present work was undertaken to study volumetric and acoustic properties for diluted solutions of tetramethylurea in pure water and for urea, n-propylurea, n-butylurea and tetramethylurea in 0.5 or 1 moldm3 aqueous solutions of sodium chloride. This paper presents measured values of densities and sound velocities at T = (288.15, 298.15 and 308.15) K. From these data the apparent molar volumes, , adiabatic compressibilities,...
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Influence of orientational disorder on the optical absorption properties in hybrid metal‐halide perovskite CH3NH3PbI3. A combined DFT/TD‐DFT and experimental study.
PublicationAn experimental and theoretical investigation is reported to analyze the relation between the structural and absorption properties of CH3NH3PbI3 in the tetragonal phase. More than 3000 geometry optimizations were performed in order to reveal the structural disorder and to identify structures with the lowest energies. The electronic structure calculations provide an averaged band gap of 1.674 eV, which is in excellent agreement...
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Effects of Bromine Doping on the Structural Properties and Band Gap of CH3NH3Pb(I1–xBrx)3 Perovskite
PublicationAn experimental and theoretical study is reported to investigate the influence of bromine doping on CH3NH3Pb(I1−xBrx)3 perovskite for Br compositions ranging from x = 0 to x = 0.1, in which the material remains in the tetragonal phase. The experimental band gap is deduced from UV−vis absorption spectroscopy and displays a linear behavior as a function of bromine concentration. Density functional theory calculations are performed...
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Modulation of dielectric properties in low-loss polypropylene-based composites at GHz frequencies: theory and experiment
PublicationPolymer composites with high dielectric constant and low loss tangent are highly regarded as substrates for modern high-speed electronics. In this work, we analyze the high-frequency dielectric properties of two types of composites based on polypropylene infused with high-dielectric-constant microparticles. Two types of fillers are used: commercial ceramics or titanium oxide ( TiO2) with different concentrations. The key observation...
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New insights on lithium storage in silicon oxycarbide/carbon composites: Impact of microstructure on electrochemical properties
PublicationIn this work, we study the impact of the preceramic precursor vinyltriethoxysilane (VTES) on the electrochemical performance of silicon oxycarbide (SiOC) glass/graphite composites. We apply an innovative approach based on high-power ultrasounds in order to obtain highly homogenous composites with a uniform distribution of small graphitic flakes. This procedure enhances gelation and drying of VTES-based preceramic polymer/graphite...
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The assessment of microbiological antimicrobial properties of PE film loaded with nanozinc filler
Open Research DataThe dataset contains the results of a single series of determinations of the antimicrobial properties against E. coli and S. aureus of polyethylene films containing the nanozinc filler.
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The electrical properties mesurements of DIR-SOFC with Ce0.8Fe0.2O2-s functional layer
Open Research DataThe dataset includes the electrical properties mesurements of SOFC with Ce0.8Fe0.1O2-s layer. Samples were produced using aqueous soft chemistry methods (microemulsion method) and applied in form of a layer onto the anode of the commercial SOFC. The SOFC was working under biogas feeding at 750oC. The layers were sintered at 1100oC.
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The electrical properties mesurements of DIR-SOFC with Ce0.8Co0.2O2-s functional layer
Open Research DataThe dataset includes the electrical properties mesurements of SOFC with Ce0.8Co0.1O2-s layer. Samples were produced using aqueous soft chemistry methods (microemulsion method) and applied in form of a layer onto the anode of the commercial SOFC. The SOFC was working under biogas feeding at 750oC. The layers were sintered at 1100oC.
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The electrical properties mesurements of DIR-SOFC with Ce0.8Mn0.2O2-s functional layer
Open Research DataThe dataset includes the electrical properties mesurements of SOFC with Ce0.8Mn0.1O2-s layer. Samples were produced using aqueous soft chemistry methods (microemulsion method) and applied in form of a layer onto the anode of the commercial SOFC. The SOFC was working under biogas feeding at 750oC. The layers were sintered at 1100oC.
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The electrical properties mesurements of DIR-SOFC with Ce0.8Ni0.2O2-s functional layer
Open Research DataThe dataset includes the electrical properties mesurements of SOFC with Ce0.8Ni0.1O2-s layer. Samples were produced using aqueous soft chemistry methods (microemulsion method) and applied in form of a layer onto the anode of the commercial SOFC. The SOFC was working under biogas feeding at 750oC. The layers were sintered at 1100oC.
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Electrical properties of silicate-lead glasses containing nanostructures of iron oxides.
Open Research DataElectrical properties of silicate-lead glasses doped with different content of iron oxide was studied. The set of glass samples were prepared with the composition of (50 − 0.5x)SiO2–(50 − 0.5x)PbO–xFe2O3, where x = 2, 5, 10, 15, 20 and 25 (in mol%). All sampleswere prepared by the conventional melt quenching technique; the melting was conducted in...
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The electrical properties mesurements of DIR-SOFC with CeO2-s functional layer
Open Research DataThe dataset includes the electrical properties mesurements of SOFC with CeO2-s layer. Samples were produced using aqueous soft chemistry methods (microemulsion method) and applied in form of a layer onto the anode of the commercial SOFC. The SOFC was working under biogas feeding at 750oC. The layers were sintered at 1100oC.
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The electrical properties mesurements of DIR-SOFC with Ce0.8Cu0.2O2-s functional layer
Open Research DataThe dataset includes the electrical properties mesurements of SOFC with Ce0.8Cu0.1O2-s layer. Samples were produced using aqueous soft chemistry methods (microemulsion method) and applied in form of a layer onto the anode of the commercial SOFC. The SOFC was working under biogas feeding at 750oC. The layers were sintered at 1100oC.
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Acid–base properties of the crosslinked polysaccharide–polyimine layer deposited on the surface of siliceous material (acid–base properties of the polysaccharide–polyimine layer)
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Shape-Depended Biological Properties of Ag3PO4 Microparticles: Evaluation of Antimicrobial Properties and Cytotoxicity in In Vitro Model—Safety Assessment of Potential Clinical Usage
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Studies on the Combined Impact of Starch Source and Multiple Processing on Selected Properties of Thermoplastic Starch/Ethylene-Vinyl Acetate Blends
PublicationThermoplastic starch (TPS)/ethylene vinyl acetate (EVA) blends compatibilized with polyethylene-graft-maleic anhydride (PE-g-MA) were prepared from various native starches (potato, maize and waxy maize) and subjected to multiple extrusion cycles. Source of starch has significant impact on its composition, hence properties of obtained TPS and their blends with EVA. Higher content of amylopectin in waxy maize starch, comparing to...
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Sestaveni Smerne Krivky Modulu Tuhosti Pro Zkoumani Nizkotrplotnich Vlastnosti (Developing of Stiffness Master Curve for Analysis of Low Temperature Properties)
PublicationV prispevku je predstaven novy postup pro sestrojeni smernych tuhostnich krivek. Nizkoteplotni vlastnosti asfaltove smesi byly stanoveny za vyuziti zkousky dotvarovani pri tribodovem ohybu. Motivem tohoto vyzkumu je skutecnost, ze metody hodnoceni nizkoteplotniho chovani asfaltovych smesi, nove zavedenych v Polsku, nejsou dostatecne. V zaveru jsou prezentovany smerne krivky tuhosti beznych asfaltovych smesi vyuzivanych v Polsku.
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Protective and Suppressing Electromagnetic Interference Properties of Epoxy Coatings Containing Nano-Sized NiZn Ferrites
PublicationNano-crystalline ferrites with the chemical formula NixZn(1−x)Fe2O4, where x = 0, 0.2, 0.4, 0.6, 0.8, 1.0, were synthesized using a co-precipitation method. The obtained ferrites were investigated by X-ray diffraction (XRD). The corrosion inhibiting behavior of nano-sized ferrites was tested using carbon steel samples and 10% aqueous ferrite extracts. Results were compared with previous data obtained for micro-sized ceramic ferrites....
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C-1311 (Symadex), a potential anti-cancer drug, intercalates into DNA between A and G moieties. NMR-derived and MD-refined stereostructure of the d(GAGGCCTC) 2 :C-1311 complex
PublicationImidazoacridinone C-1311 (Symadex®) is an antitumor agent which has been recommended for Phase II clinical trials a few years ago. Previously, it was shown experimentally that during the initial stage of its action C-1311 forms stable intercalation complexes with DNA duplexes. Herein, a NMR-derived stereostructure of d(GAGGCCTC)2:C-1311 complex was reported. The ligand was found locating itself between A and G moieties, forming...
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The first study on the usefulness of recombinant tetravalent chimeric proteins containing fragments of SAG2, GRA1, ROP1 and AMA1 antigens in the detection of specific anti-Toxoplasma gondii antibodies in mouse and human sera
PublicationThis study presents an evaluation of four tetravalent recombinant chimeric proteins containing fragments of the Toxoplasma gondii antigens, SAG2, GRA1, ROP1 and AMA1, as potential replacements of a the soluble, whole-cell tachyzoite lysate (TLA) used in serological assays. Recombinant chimeric proteins (SAG2-GRA1-ROP1-AMA1N, AMA1N-SAG2-GRA1-ROP1, AMA1C-SAG2-GRA1-ROP1, and AMA1-SAG2-GRA1-ROP1) obtained by genetic engineering were...
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Structural and physico-mechanical properties of natural rubber/GTR composites devulcanized by microwaves: Influence of GTR source and irradiation time
PublicationGround tire rubber from car and truck was modified using microwave irradiation at variable time. The irradiated ground tire rubber was used as filler in composites based on natural rubber. The composites, with high content of ground tire rubber, were prepared using an internal batch mixer and subsequently cross-linked at 160℃. The influence of the ground tire rubber source (car/truck) and irradiation time on structure, physico-mechanical...
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Non-linear electrical properties of myocardium in computer simulation
PublicationPomiar impedancji elektrycznej jest obiecującą metodą monitorowania stanu mięśnia sercowego, szczególnie podczas niedokrwienia. Typową metodą pomiaru jest rejestrowanie odpowiedzi-napięcia na pobudzenie prądowe. Odpowiedź jest często aproksymowana jako liniowa względem pobudzenia. Artykuł jest poświęcony oszacowaniu rzędu wielkości nieliniowych komponentów w odpowiedzi.
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Emulsifying properties of surfactants and biosurfactants in the context of soil remediation
PublicationZbadano stabilność emulsji, w których fazę rozproszoną stanowił dodekan oraz bazowy olej syntetyczny typu polialfaolefin - PAO. Zbadano wpływ czasu i temperatury na stabilność emulsji zawierających różne stężenia surfaktantów (Triton X-100, biosurfaktant JBR 325) oraz różne zawartości fazy niepolarnej za pomocą aparatu Turbiscan Lab wykorzystując technikę wstecznego rozproszenia światła. We wszystkich próbkach stwierdzono niestabilności...
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Electrical properties of YSZ films prepared by netshape technology
PublicationW pracy przedstawiono wyniki badań domieszkowanego tlenku cyrkonu przygotowanego metodą net shape. Materiał został przygotowany w postaci warstwy o grubości 1-10um na szafirze oraz folii platynowej. Zbadano włąsiciwości elektryczne przygotowanych warst.
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Modeling of substrate noise block properties for early rediction.
PublicationZaproponowano nowe podejscie do modelowania zakłóceń podłozowych we wczesnym etapie projektowania systemów na wspólnym podłożu krzemowym. Modelowanie zakłóceń oparto na założeniu, że głównym źródłem zakłóceń podłożowych jest sieć zasilająca. W oparciu o przeprowadzone symulacjie wykazano słusznosć takiej metody.
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Tribological properties of tissue in biobearings and bioreactors as the histotribological parameters
PublicationReferat przedstawia stan wiedzy oraz potrzeby b+r w zakresie celów badawczych podjętych w projekcie BioBearing, finansowanym przez Komisję Europejską. Są to badania teoretyczne, numeryczne i eksperymentalne problemów tribologii tkanek jako elementów histotribologii a w szczególności smarowania stawów nienewtonowskimi cieczami synowialnymi w warunkach nieustalonych z uwzględnieniem deformacji chrząstki stawowej w opisie stochastycznym.
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Direct measurement of nonlinear properties of bipartite quantum states
PublicationNieliniowe własności stanów kwantowych, takie jak entropia, splątania, określają ilość ważnych fizycznych źródeł i są często używane w informatyce kwantowej. Na ogół są one obliczane z pełnego opisu stanu kwantowego, pomimo tego, że zależą od niewielkiej ilości parametrów opisujących dany stan. Wyciągamy nielokalną i nieliniową wielkość, mianowicie entropię Renyi, z lokalnych pomiarów dwóch par fotonów splątanych polaryzacyjnie.
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Mechanical properties of dissimilar welded joints for chemical tankers
PublicationArtykuł przedstawia właściwości mechaniczne złączy różnoimiennych stali typu duplex oraz austenitycznej typu 316L otrzymanych za pomocą spawania automatycznego łukiem krytym. Wykazano możliwość wykorzystania wysokowydajnej metody SAW w miejsce dotychczas stosowanych metod GTAW i GMAW do spawania blach zbiorników statków do przewozu chemikaliów. Pomimo obawy uzyskania nieodpowiednich struktur złączy okazało się, że spawanie stali...
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Microstructure and corrosion properties of the laser treated SUPERSTON alloy
PublicationPrzedstwiono wyniki laserowego nadtapiania powierzchni stopu SUPERSTON w warunkach kriogenicznych. Zaprezentowano obraz powierzchni stopu po badaniach korozyjnych oraz wyniki pomiarów mikrotwardości i odporności korozyjnej.
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Amino Acid Based Antimicrobial Agents – Synthesis and Properties
PublicationStructures of several dozen of known antibacterial, antifungal or antiprotozoal agents are based on the amino acid scaffold. In most of them, the amino acid skeleton is of a crucial importance for their antimicrobial activity, since very often they are structural analogs of amino acid intermediates of different microbial biosynthetic pathways. Particularly, some aminophosphonate or aminoboronate analogs of protein amino acids are...
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Dynamics of Chains as a Tool to Study Thermomechanical Properties of Proteins.
PublicationPolymer dynamics can be formulated on different levels of detail. One approach eliminates microscopic degrees of freedom and a polymer molecule is represented by a simplified structure—a chain. In the simplest case monomers of ideal chain have fixed length, and their orientation is independent of the orientations and positions of neighbouring monomers. This is reason that two monomers can co-exist at the same place. Ideal chain...
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Chromogenic azomacrocycles with imidazole residue: Structure vs. properties
PublicationNew diazo macrocycles linked by hydrocarbon chain bearing imidazole or 4-methylimidazole residue have been synthetized with satisfactory yield (24–55%). The structure of macrocycles was confirmed by X-ray analysis and spectroscopic methods (1H NMR, MS, FTIR). Metal cation complexation studies were carried out in acetonitrile and acetonitrile-water system. It was found that azomacrocyles form triple-decker complexes with lead(II)....
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Influence of ligno-cellulosic particles on tribological properties of boards
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Thermal properties of poly(vinyl chloride)/polyurethane blends
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Structure and electric properties of double magnesium zirconium orthophosphate
PublicationPublikacja przedstawia wyniki pomiarów elektrycznych i strukturalnych ortofosforanu magnezowo-cyrkonowego.
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Structural and Electrical Properties of STF Materials for SOFC Applications
PublicationW tym artykule przedstawiono badania tytanian strontu domieszkowanego żelazem. Synteza dwuetapowa była niezbędna do uzyskania czystego fazowo proszku o pożądanych właściwościach. Przewodnictwo elektryczne wykazało właściwości typu zero-TCR dla składu STF35. Poziom przewodnictwa elektrycznego różnił się o więcej niż jeden rząd wartości dla wytworzonych materiałów. Reaktywność chemiczną między YSZ i STF badano w zakresie temperatur...
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Investigation of properties of swimming pool water treatment sediments
PublicationDwa rodzaje osadów pochodzących z instalacji basenowych zostały scharakteryzowane i otrzymane wyniki przedyskutowane, w szczególności flokuły, które zatrzymały się na filtrze piaskowo-żwirowym i następnie zostały usunięte w płukaniu zwrotnym oraz osady z dna niecki basenowej zebrane tzw. odkurzaczem wodnym. Lepsze zrozumienie struktury i właściwości osadów powinno usprawnić usuwanie cyst Cryptosporidium z basenów i w efekcie podnieść...
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The properties, functions and use of selenium compounds in living organisms
PublicationSelenium occurs in the environment in inorganic and organic compounds. For many years it was regarded as a toxic element, causing numerous illnesses and diseases. But research in the last 50 years has revealed a "bright side" to this element, especially as a component of selenoproteins, selenium makes a significant contribution to the health of humans and animals. The selenium content in an organism depends on its concentration...
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The rheological properties of hydroxylated soybean oil by using bioglycols
PublicationPraca zawiera opis właściwości fizykochemicznych i reologicznych hydroksylowanych olejów sojowych zmodyfikownych przy użyciu wybranych bioglikoli.
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Labyrynths generators, their properties and practical application in computer games
Publicationthis paper presents three basic algorithms for generation of mazes, and many of their modifications and examples showing their practical application in creating random structures that resembles those from the real world. the paper highlights the difference in the labyrinths classes generated by listed algorithms and describes a specific and highly likely to occur shapes that occur in generated mazes. particular attention was paid...
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Structural and magnetic properties of Cu-alloyed FePd films
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Induction heating in estimation of thermal properties of conductive materials
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The effect of transglutaminase on the properties of salmon skin-gelatin films
PublicationCelem pracy była enzymatyczna modyfikacja folii otrzymanych z żelatyny rybnej. Źródłem żelatyny były surowe i wędzone skóry łososia. Stwierdzono, że czas żelowania roztworu żelatyny ulegał skróceniu w obecności transglutaminazy w badanym zakresie 0,1-0,2 mg/ml. Enzymatyczne modyfikacje prowadziły do obniżenia rozpuszczalności folii, jednakże w różnym stopniu zależnym od źródła białka. Obecność DTT lub cysteiny w mieszaninie reakcyjnej...
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Copper containing protein sites - structure, properties and models
PublicationEnzymy organizmów żywych katalizują wiele reakcji stosowanych w przemyśle chemicznym. Przykładem potencjalnego zastosowania enzymu w produkcji jest synteza L-Dopy przy udziale tyrozynazy. Ze względu na możliwe praktyczne zastosowanie w katalizie, otrzymano i opisano wiele prostych modeli miejsc aktywnych enzymów. W artykule opisano niektóre modele białek zawierających miedź.
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Basic properties of oil from pyrplysis of scrap tires
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DAF - and collagen-binding properties of chimeric Dr fimbriae
PublicationEkspozycja białek heterologicznych na powierzchni mikroorganizmów jest jedną z nowych strategii stosowanych w mikrobiologii, biotechnologii oraz projektowaniu nowoczesnych szczepionek. W niniejszej pracy zbadano możliwość wykorzystania białka podjednostkowego DraE fimbrii Dr uropatogennych szczepów Escherichia coli jako nośnika heterologicznych sekwencji. W rejon odpowiadający N-terminalnej domenie 2 białka DraE wprowadzono epitopową...
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Thermal properties of tetrabutylammonium bromotrichloro-, tribromochloro-and tetrabromoferrates(III)
PublicationW pracy badana jest termiczna dekompozycja związków tetrabutylammonium bromotrichloro-, tribromochloro-and tetrabromoferrates(III). Analizę termiczną (TG-MS, DTA, DTG i DSC) prowadzono w atmosferze argonu w zakresie temperatur 293-1073 K. Stałe produkty dekompozycji identyfikowano metodą dyfrakcji promieniowania rentgenowskiego.
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The morphology and mechanical properties of recyclated polyethylene/polyamide laminate
PublicationZbadano wpływ kompatybilizatorów na morfologię i właściwości mechaniczne mieszanin PE/PA. Okreslono właściwości recyklatu uzyskanego z odpadów barierowej folii wielowarstwowej zawierającej 80% PE i 20% PA. Po dodaniu kompatybilizatorów układ stał się bardziej jednorodny, zmniejszeniu uległy domeny PA oraz poprawiły się właściwości mechaniczne.
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Properties of glass-ceramic for solid oxide fuel cells
PublicationW pracy przedstawiono właściwości krystalicznych pyro- i orto- krzemowych szkieł przygotowanych dla tlenkowych ogniw paliwowych. Zbadano rozszerzalnoność, ubytek masy, zmiany widm rentgenograficznych oraz widm impedancyjnych dla szkieł narażonych przez 60 dni na atmosfere ulteniajacą i redukująca w temperaturze 800C.
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Chemical structures and physical properties of cured segmental polyurethanes
PublicationPrzedmiotem badań były poliuretany (PUR) segmentowe otrzymywane w dwuetapowej syntezie oligomerycznego α,ω-dihydroksy(adypinianu etylenowo-butylenowego) oraz dwóch różnych aromatycznych diizocyjanianów: 4,4'-diizocyjanianu difenylenometanu (MDI) albo MDI modyfikowanego diizocyjanianem karbodiimidu. Na etapie przedłużania łańcucha, oprócz typowo używanego do tego celu 1,4-butanodiolu, stosowano triol - 1,3-dihydroksy-2-(hydroksymetyleno)propan...
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The influence of preparing conditions on the properties of SrTi0.98Nb0.02O3-YSZ composite
PublicationZbadano wpływ warunków przygotowania na właściwości kompozytów SrTi0.98Nb0.02O3-YSZ jako potencjalnych warstw przejściowych między anodą a elektrolitem w tlenkowych ogniwach paliwowych SOFC. Udowodniono, że proces wstępnej obróbki temperaturowej substratów oraz sposób ich mielenia znacznie wpływa na przewodnictwo elektryczne badanych materiałów.
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Electrical and structural properties of Nb-doped SrTiO3 ceramics
PublicationPrzebadano wpływ zawartości niobu na strukturę i własności elektryczne tytanianu strontu. Zbadany został wpływ warunków redukcji i porowatości na właściwości materiału. Za optymalne uznano domieszkowanie niobem w wysokości 2% molowych.
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Wide range of properties of polyurethanes for medicine - characterization of biomaterials
PublicationW artykule opisano różnorodność poliuretanów stosowanych na polu biomedycznym. Wyrózniono mtody otrzymywania materiałów o róznych własciwościach, a tym samym zastosowaniach. Opisano 10 serii potrzymanych PU oraz wyniki charakterystyki fizycznej, powierzchniowej i biologicznej tych poliuretanów.
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Tailoring Graphene to Achieve Negative Poisson's Ratio Properties
PublicationGraphene can be made auxetic through the introduction of vacancy defects. This results in the thinnest negative Poisson's ratio material at ambient conditions known so far, an effect achieved via a nanoscale de-wrinkling mechanism that mimics the behavior at the macroscale exhibited by a crumpled sheet of paper when stretched.
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Investigation of electrocatalytic gas sensor properties in presence of chlorine
PublicationIn this paper performance of an electrocatalytic sensor in presence of chlorine is investigated. Presented studies concern sensor prepared in ceramic technology based on NASICON as a solid electrolyte with two round shaped platinum electrodes. Measurements in different temperatures have been performed in order to determine optimal sensor working temperature.
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Thin CVD diamond films - synthesis, properties, applications
PublicationThe basic model of diamond films growth, in the low pressure synthesis, deposition from the CVD gas phase, is the mixture of hydrocarbon gas in presence with activated hydrogen and its nucleation on the substrate as a result of pyrolysis reaction. It allows to cross the great energetic barrier between graphite and diamond. High pressure and temperature are replaced by change of electronic structure of atoms into gas precursors...
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How important are scaffolds and their surface properties in regenerative medicine
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Influence of bulky pyrrolyl substitent on the physicochemical properties of porphyrazines
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Synthesis and Selected Properties of Ester Elastomer Containing Sorbitol
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Heteropolyanions doped polyacetylene—Preparation, spectroscopic and catalytic properties
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Properties of Potato Starch Roasted with Apple Distillery Wastewater
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Adsorption Properties of Sepiolite in Relation to Uranium and Lanthanide Ions
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Luminescent properties of YAlO3:Mn single crystalline films
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Fracture in composite/aluminium joints of variable adhesive properties
PublicationA strain gauge technique recently developed with the wedge test, for estimating crack length and, thus, the fracture energy of structural adhesive bonding, has been employed on a system in which one adherend had two types of surface treatment. Simple polishing and polishing with subsequent sandblasting were the treatments used, with a distinct straight line, perpendicular to the sample edges, separating the two. Despite the clear-cut...
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Influence of hydrothermal synthesis parameters on the properties of hydroxyapatite nanoparticles
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The Properties, Functions, and Use of Selenium Compounds in Living Organisms
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THE TRIBOLOGICAL PROPERTIES OF LUBRICATING GREASES BASED ON RENEWABLE OILS
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Geotechnical Properties of Phosphogypsum and Its Use in Road Engineering
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Amorphous Form of Carvedilol Phosphate—The Case of Divergent Properties
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The influence of polypropylene fibres on the properties of fresh and hardened concrete
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